Ultrasonics Sonochemistry最新文献

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Impact of ultrasound-assisted single washing process on tilapia mince: Biochemical changes, structural modifications, and gel formation 超声辅助单次洗涤过程对罗非鱼肉糜的影响:生化变化、结构修饰和凝胶形成
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2026-01-01 Epub Date: 2025-12-14 DOI: 10.1016/j.ultsonch.2025.107707
Ali Hamzeh , Lobdaw Saelee , Kanjana Thumanu , Jae W. Park , Jirawat Yongsawatdigul
{"title":"Impact of ultrasound-assisted single washing process on tilapia mince: Biochemical changes, structural modifications, and gel formation","authors":"Ali Hamzeh ,&nbsp;Lobdaw Saelee ,&nbsp;Kanjana Thumanu ,&nbsp;Jae W. Park ,&nbsp;Jirawat Yongsawatdigul","doi":"10.1016/j.ultsonch.2025.107707","DOIUrl":"10.1016/j.ultsonch.2025.107707","url":null,"abstract":"<div><div>Ultrasound (US)-assisted single washing was applied to reduce water usage in tilapia mince washing during surimi production. The mince-to-water ratio of 1:2 in US-assisted washing was compared with ratios of 1:2 and 1:3 in conventional washing (CW−2 and CW−3, respectively). Screening of US power revealed the greatest effect at an intensity of 3.19 W/cm<sup>2</sup> on mince whiteness (<em>p</em> &lt; 0.05), without damage to protein polypeptide chains, and no extensive biochemical changes. Subsequently, the mince was subjected to various US exposure times of 1, 3, and 5 min (US−1, US−3, and US−5, respectively) at 3.19 W/cm<sup>2</sup>, maintaining the same total washing time of 10 min across all treatments. US-assisted washing increased myofibrillar protein loss compared with that with CW, as indicated by sodium dodecyl sulfate–polyacrylamide gel electrophoresis, and the loss increased with longer exposure time—from 7.57 % in US−1 to 12.76 % in US−5. The US−1-washed mince exhibited the highest Ca<sup>2+</sup>–ATPase activity and reactive sulfhydryl (SH) content, even higher than that of CW−3 (<em>p</em> &lt; 0.05). Random coil structures decreased in US−5, while other secondary structures did not change significantly. Tertiary structure analysis using Raman spectroscopy revealed comparable tyrosine and tryptophan exposure in US−1, US−3, and CW−3, which may contribute to the increased breaking force and distance through higher extent of hydrophobic interactions in their corresponding surimi gels compared with CW−2 and US − 5 (<em>p</em> &lt; 0.05). Oxidation of SH groups and hydrophobic interactions increased in US−3 and US−5 (<em>p</em> &lt; 0.05). US−1 was identified as the optimal condition for a single washing of tilapia mince to reduce water usage with minimal negative effects on protein.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"124 ","pages":"Article 107707"},"PeriodicalIF":9.7,"publicationDate":"2026-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145753366","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Improving amino acids and digestive peptides contents of chicken breast paste using ultrasound-assisted EGCG treatment within a complex meat matrix 超声辅助EGCG处理复合肉基质提高鸡胸肉膏氨基酸和消化肽含量
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2026-01-01 Epub Date: 2025-12-17 DOI: 10.1016/j.ultsonch.2025.107728
Jiahui Chen , Xinglian Xu
{"title":"Improving amino acids and digestive peptides contents of chicken breast paste using ultrasound-assisted EGCG treatment within a complex meat matrix","authors":"Jiahui Chen ,&nbsp;Xinglian Xu","doi":"10.1016/j.ultsonch.2025.107728","DOIUrl":"10.1016/j.ultsonch.2025.107728","url":null,"abstract":"<div><div>This study systematically investigated the unique effects of ultrasound-assisted EGCG treatment on the amino acids and digestive peptides contents of chicken breast paste. As a complex system, chicken samples exhibited distinct ultrasonic responses that cannot be extrapolated from simplified protein-based studies. To be specific, results demonstrated that ultrasound-assisted EGCG treatment significantly enhanced the essential/non-essential amino acids ratio to 41.03%, which could not be acquired through individual treatment. More so, structural analysis of meat pastes revealed that particle size was reduced by 62.72% after treatment. Furthermore, ultrasound-assisted EGCG treatment reduced total water contents by 13.65%, thereby promoting the transition of immobilized to free water. The above-mentioned changes enhanced enzymatic accessibility and increased peptide contents by 2.18%. This study innovatively highlighted the efficiency of ultrasonic-assisted EGCG treatment in enhancing nutritional features at the level of chicken matrix, offering an important advancement from theory to practice.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"124 ","pages":"Article 107728"},"PeriodicalIF":9.7,"publicationDate":"2026-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145785407","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Advances in ultrasound-enhanced recovery of marine algal polysaccharides: toward sustainable bioprocessing 海洋藻类多糖超声强化回收的研究进展:迈向可持续生物处理
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-12-01 Epub Date: 2025-11-16 DOI: 10.1016/j.ultsonch.2025.107683
Tehmina Naseem , Khushi Ali , Nisha Zahid , Syed Ali Hassan , Gholamreza Abdi , Seydi Yıkmış , Rana Muhammad Aadil
{"title":"Advances in ultrasound-enhanced recovery of marine algal polysaccharides: toward sustainable bioprocessing","authors":"Tehmina Naseem ,&nbsp;Khushi Ali ,&nbsp;Nisha Zahid ,&nbsp;Syed Ali Hassan ,&nbsp;Gholamreza Abdi ,&nbsp;Seydi Yıkmış ,&nbsp;Rana Muhammad Aadil","doi":"10.1016/j.ultsonch.2025.107683","DOIUrl":"10.1016/j.ultsonch.2025.107683","url":null,"abstract":"<div><div>The growing emphasis on environmental sustainability has intensified interest in the extraction and valorization of polysaccharides from marine algal species due to their non-toxic nature and notable bioactivities. Although various conventional extraction techniques have been employed, these often involve high energy consumption, prolonged processing times, limited selectivity, and the potential degradation of polysaccharide bioactivity. To address these limitations, a range of sustainable and cost-effective extraction methods has been developed, including enzyme-assisted extraction (EAE), supercritical fluid extraction (SFE), subcritical water extraction (SWE), microwave-assisted extraction (MAE), and ultrasound-assisted extraction (UAE). Among these, the UAE, either as a standalone method or integrated within a biorefinery framework, has emerged as a promising and green technology. It offers higher extraction efficiency with reduced time, energy, and cost requirements. Polysaccharides extracted via ultrasound (US) have demonstrated enhanced anticancer, bioactive, and rheological properties. Furthermore, integrating the UAE with green solvents, such as natural deep eutectic solvents (NaDESs), or complementary techniques, including MAE, hot water extraction (HWE), and EAE, has been shown to further improve yields by 2–6 % and enhance functional quality. This review highlights the potential of the UAE, both individually and in combination with other methods for the efficient recovery of algal polysaccharides. It also evaluates the influence of the UAE on the biofunctional properties of the extracted compounds, underscoring their applicability across diverse industrial sectors. Nonetheless, further research is warranted to optimize process parameters, ensure safety, enhance antioxidant activity (AOA), and improve purification and characterization, as well as better understand the structure–activity relationships of these valuable biopolymers.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"123 ","pages":"Article 107683"},"PeriodicalIF":9.7,"publicationDate":"2025-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145531119","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Next-generation suturing: Moisture-pressurized and ultrasonic synthesis of Cu–Ag–Al nanorods for antibacterial dental and dialysis applications 新一代缝合:用于抗菌牙科和透析应用的Cu-Ag-Al纳米棒的湿加压和超声波合成
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-12-01 Epub Date: 2025-11-08 DOI: 10.1016/j.ultsonch.2025.107672
Wenhao Tao , Yibo Wei , Zhizen Quan, Chen Li, Gang Tian , Xiaogang Xu
{"title":"Next-generation suturing: Moisture-pressurized and ultrasonic synthesis of Cu–Ag–Al nanorods for antibacterial dental and dialysis applications","authors":"Wenhao Tao ,&nbsp;Yibo Wei ,&nbsp;Zhizen Quan,&nbsp;Chen Li,&nbsp;Gang Tian ,&nbsp;Xiaogang Xu","doi":"10.1016/j.ultsonch.2025.107672","DOIUrl":"10.1016/j.ultsonch.2025.107672","url":null,"abstract":"<div><div>Cu–Ag–Al trimetallic nanorods were synthesized using a moisture-pressurized ultrasonic method and evaluated as antibacterial coatings for dental and dialysis sutures. The nanorods exhibited a mesoporous structure (surface area = 28.6 m<sup>2</sup> g<sup>−1</sup>) and strong crystalline stability confirmed by XRD, FESEM, BET, TGA, and Raman analyses. The coated sutures showed concentration-dependent antibacterial and antibiofilm activity, achieving up to 86.5 % inhibition against <em>E. coli</em> and 74.2 % against <em>S. aureus</em>, with durable adhesion after washing. Cytotoxicity assays on KB and U87 cells revealed selective anticancer potential and acceptable biocompatibility at low doses. The developed ultrasonic synthesis offers a rapid, energy-efficient, and scalable route compared with conventional hydrothermal and microwave methods. The coatings maintained high stability, reduced the risk of nanoparticle release, and exhibited environmental and clinical safety potential. The enhanced antibacterial effect is attributed to synergistic reactive oxygen species (ROS) generation and membrane disruption arising from the Cu–Ag–Al interaction. This scalable, low-cost approach demonstrates promise for next-generation infection-resistant sutures in clinical dentistry and dialysis applications.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"123 ","pages":"Article 107672"},"PeriodicalIF":9.7,"publicationDate":"2025-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145462168","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
CFD-PBM modelling for predicting the size and distribution of silica nanoparticles synthesized in an ultrasound-assisted swirling vortex flow reactor CFD-PBM模型预测超声辅助旋流反应器中合成的二氧化硅纳米颗粒的尺寸和分布
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-12-01 Epub Date: 2025-11-01 DOI: 10.1016/j.ultsonch.2025.107663
Lu Liu , Weibin Shi , Bin Li , Guichao Wang , Yanqing Guo , Xiaogang Yang , Weibiao Zhou
{"title":"CFD-PBM modelling for predicting the size and distribution of silica nanoparticles synthesized in an ultrasound-assisted swirling vortex flow reactor","authors":"Lu Liu ,&nbsp;Weibin Shi ,&nbsp;Bin Li ,&nbsp;Guichao Wang ,&nbsp;Yanqing Guo ,&nbsp;Xiaogang Yang ,&nbsp;Weibiao Zhou","doi":"10.1016/j.ultsonch.2025.107663","DOIUrl":"10.1016/j.ultsonch.2025.107663","url":null,"abstract":"<div><div>A coupled computational fluid dynamics-population balance model (CFD-PBM) framework is developed and experimentally validated to predict the size and distribution of silica nanoparticles in an ultrasound-assisted swirling vortex flow reactor (SVFR). Two key aggregation parameters (i.e., bridge strength parameter <em>A<sub>p</sub></em>, and the initial particle number coefficient <em>C</em><sub>1</sub>) are identified and corrected against experimental data, enabling accurate prediction of primary and secondary peaks in the particle size distribution. The modelling results show that increasing vortex Reynolds number promotes particle collisions, leading to a high frequency of particle collisions and thus relatively large particle sizes, while ultrasound exerts a dual effect by enhancing collisions and simultaneously suppressing excessive aggregation via turbulence-induced shear. These findings highlight the critical role of ultrasound-assisted turbulence in controlling nanoparticle formation, providing insights for reactor design and scale-up.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"123 ","pages":"Article 107663"},"PeriodicalIF":9.7,"publicationDate":"2025-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145424101","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Ultrasound-assisted extraction enhances recovery of antioxidant-rich carbohydrate fraction from mixed microalgae species 超声辅助提取提高了混合微藻中富含抗氧化剂的碳水化合物组分的回收率
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-12-01 Epub Date: 2025-10-30 DOI: 10.1016/j.ultsonch.2025.107656
Eldwin Ze Hao Ooi , Eng-Seng Chan , Cher Pin Song , Janarthanan Pushpamalar , Yee-Ying Lee
{"title":"Ultrasound-assisted extraction enhances recovery of antioxidant-rich carbohydrate fraction from mixed microalgae species","authors":"Eldwin Ze Hao Ooi ,&nbsp;Eng-Seng Chan ,&nbsp;Cher Pin Song ,&nbsp;Janarthanan Pushpamalar ,&nbsp;Yee-Ying Lee","doi":"10.1016/j.ultsonch.2025.107656","DOIUrl":"10.1016/j.ultsonch.2025.107656","url":null,"abstract":"<div><div>The effects of ultrasonic processing parameters on the functional and physicochemical properties of microalgae carbohydrates remain poorly understood, despite evidence from plant-based extractions showing that sonication conditions strongly influence bioactive compound yield and antioxidant activity from carbohydrates. This study investigated the effects of ultrasonic-assisted extraction (UAE) parameters on the yield, composition, and antioxidant activity of carbohydrates extracted from defatted mixed microalgae biomass. A single-factor approach was employed to test different extraction times (10–30 min), amplitudes (20–100 %), and solid-to-solvent ratios (1:10–1:30 g/mL). All analyses were conducted in triplicate, and statistical significance was determined at p &lt; 0.05. Results showed that processing time was the most influential factor in improving antioxidant activity. Under optimal UAE conditions (25 min, 100 % amplitude, 1:15 g/mL), the extract contained significantly higher uronic acid, sulphate, and fibre contents (p &lt; 0.05) compared to hot water extraction. These changes corresponded to stronger antioxidant activity (∼35 % increase in DPPH radical scavenging). Correlation analysis further revealed that uronic acid had the strongest positive influence on antioxidant activity. In conclusion, UAE improved both the yield and antioxidant properties of microalgae carbohydrates compared with hot water extraction. With its high fibre content and bioactivity, the extract may have potential applications as a functional food ingredient.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"123 ","pages":"Article 107656"},"PeriodicalIF":9.7,"publicationDate":"2025-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145383589","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Ultrasound-assisted hot water extraction of yellow leaves of Pu’er tea polysaccharides: Extraction process, characterization, antioxidant and hypoglycemic activity 超声辅助热水提取普洱茶黄叶多糖:提取工艺、表征及抗氧化降糖活性
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-12-01 Epub Date: 2025-10-27 DOI: 10.1016/j.ultsonch.2025.107653
Ao Zhao , Lina Sun , Fu Xu, Wendie Gan, Biaoying Guo, Lianzhou Jiang, Xia Wu
{"title":"Ultrasound-assisted hot water extraction of yellow leaves of Pu’er tea polysaccharides: Extraction process, characterization, antioxidant and hypoglycemic activity","authors":"Ao Zhao ,&nbsp;Lina Sun ,&nbsp;Fu Xu,&nbsp;Wendie Gan,&nbsp;Biaoying Guo,&nbsp;Lianzhou Jiang,&nbsp;Xia Wu","doi":"10.1016/j.ultsonch.2025.107653","DOIUrl":"10.1016/j.ultsonch.2025.107653","url":null,"abstract":"<div><div>Yellow leaves of Pu’er tea are classified as lower-grade Pu’er tea, and polysaccharides being its principal active components. Pu’er tea polysaccharides (PTPS) were optimally extracted from yellow leaves of Pu’er tea using ultrasound-assisted hot water extraction with the following parameters: solid-to-liquid ratio of 1:25 (w/v), ultrasonic temperature of 70 °C, ultrasonic power of 500 W, and ultrasonic time of 40 min. Two fractions, PTPS-4A and PTPS-5A, were clearly isolated and purified. Their antioxidant and hypoglycemic effects were compared in a lab after examining their structural features. PTPS-4A and PTPS-5A were mostly composed of fucose, rhamnose, arabinose, galactose, glucose, mannose, and glucuronic acid. They manifested as flexible chains and assumed a linear spline curve suggestive of an earthworm-like conformation. The nuclear magnetic resonance investigation found α- and β-glycosidic linkages (<em>δ</em>4.30–5.95 ppm and <em>δ</em>4.29–4.97 ppm, respectively) in PTPS-4A and PTPS-5A. PTPS-4A had enhanced DPPH and hydroxyl radical removal, with IC<sub>50</sub> values of 1.79 ± 0.07 mg/mL and 6.42 ± 0.16 mg/mL, respectively. The intermediate concentration value of 5.22 ± 0.08 mg/mL of PTPS-4A indicated a stronger inhibitory impact on α-glucosidase. PTPS-4A and PTPS-5A did not affect α-amylase in any way. The PTPS-4A fraction from this study may be further processed to create polysaccharide-based hypoglycemic and antioxidant products.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"123 ","pages":"Article 107653"},"PeriodicalIF":9.7,"publicationDate":"2025-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145396330","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Enhanced extraction of beetroot peel polyphenols using response surface methodology and their stabilization in W/O/W emulsions using whey protein isolates 响应面法提取甜菜根皮多酚及其在乳清分离蛋白W/O/W乳剂中的稳定性
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-12-01 Epub Date: 2025-10-21 DOI: 10.1016/j.ultsonch.2025.107638
Iqra Nasim , Nauman Khalid
{"title":"Enhanced extraction of beetroot peel polyphenols using response surface methodology and their stabilization in W/O/W emulsions using whey protein isolates","authors":"Iqra Nasim ,&nbsp;Nauman Khalid","doi":"10.1016/j.ultsonch.2025.107638","DOIUrl":"10.1016/j.ultsonch.2025.107638","url":null,"abstract":"<div><div>This study aims to investigate the bioactive compounds in beetroot peel and their stabilization in W/O/W emulsions for potential use in future food industrial applications. The extraction of polyphenols, flavonoids, and antioxidants from beetroot peels was performed with the green extraction method, and their effects were determined through spectrophotometric methods. Box-Behnken Design was used for optimizing extraction parameters and model validation. The design suggested a quadratic model for all the responses. The minimum and maximum coded values examined for the experimental design included extraction time (10–30 min), sample concentration (1–5 %), and operating power (10–50 W). The W/O/W emulsions were prepared with varying concentrations of whey protein isolates (WPI) (1 % (E<sub>1</sub>), 2 % (E<sub>2</sub>), and 3 % (E<sub>3</sub>) (w/w)). The emulsions were studied in terms of creaming index, viscosity, encapsulation efficiency, antioxidant determination, color analysis, droplet size distribution, and optical microscopy on samples stored for 0, 10, 20, and 30 days at 4 °C. The optimized conditions for maximum extraction of polyphenols were 21.72 min, 4.99 % sample concentration, and 49.76 W power. The yield of total polyphenols, total flavonoids, DPPH, and ABTS activity was 46.5 mg GAE/g DW, 10.9 mg QE/g, 66.3 %, and 89.6 % respectively. 3 % (w/w) WPI provided the highest color retention, oxidative and physical stability, and encapsulation efficiency. Overall, it was observed that all the independent factors played a significant role in the extraction of phytochemicals from beetroot peel extract and could be improved to maximize model responses. The formulated emulsion has potential for utilization in future food applications.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"123 ","pages":"Article 107638"},"PeriodicalIF":9.7,"publicationDate":"2025-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145450446","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Application and mechanism of ultrasonic-assisted extraction of ginkgo flavonol glycosides with natural deep eutectic solvent-based supramolecular solvents 天然深共晶溶剂基超分子溶剂超声辅助提取银杏黄酮醇苷的应用及机理研究
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-12-01 Epub Date: 2025-11-04 DOI: 10.1016/j.ultsonch.2025.107664
Han Yuan , Xiangzhou Li , Jun Zhou , Yanhong Yang , Wensheng Li , Peng Zhou
{"title":"Application and mechanism of ultrasonic-assisted extraction of ginkgo flavonol glycosides with natural deep eutectic solvent-based supramolecular solvents","authors":"Han Yuan ,&nbsp;Xiangzhou Li ,&nbsp;Jun Zhou ,&nbsp;Yanhong Yang ,&nbsp;Wensheng Li ,&nbsp;Peng Zhou","doi":"10.1016/j.ultsonch.2025.107664","DOIUrl":"10.1016/j.ultsonch.2025.107664","url":null,"abstract":"<div><div>To address potential issues such as low efficiency, prolonged processing time, the environmental friendliness deficiency of traditional extraction processes of ginkgo flavonol glycosides, this study adopted an ultrasonic-assisted extraction of Ginkgo Flavonol Glycosides with natural deep eutectic solvent-based supramolecular solvent/equilibrium solution (NADES-SUPRAS/EqS). With the assistance of ultrasound, this method achieved an efficient and green extraction process, especially demonstrating significant advantages in reducing extraction time. Through experimental optimization, the optimal conditions were determined as follows: ultrasonic power 160 W, treatment duration 15 min, solid-to-liquid ratio 40 mg/mL, and extraction temperature 30 ℃. Under these conditions, the yield of Ginkgo Flavonol Glycosides reached 8.025 mg/g. Recovery experiments confirmed excellent recyclability of the NADES-SUPRAS/EqS solvent, achieving a flavonol glycoside recovery rate of 91.3 %. This approach holds significant potential for industrial-scale production of Ginkgo Flavonol Glycosides. Microstructural analysis revealed that the NADES-SUPRAS/EqS solvent formed normal micellar vesicles with a hydrophobic core and hydrophilic corona, and the combination of ultrasonic action could effectively disrupt the cell walls of Ginkgo leaves. Density functional theory (DFT)-based molecular modeling elucidated the extraction mechanism, demonstrating strong hydrogen bonding and van der Waals interactions between the NADES-SUPRAS/EqS solvent and rutin. The significance of this research lies in offering a reference framework for green and efficient ultrasonic-assisted extraction studies of natural bioactive compounds, which may provide a feasible technical solution for production of ginkgo flavonol glycosides.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"123 ","pages":"Article 107664"},"PeriodicalIF":9.7,"publicationDate":"2025-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145441407","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Ultrasound-powered bovine bone protein hydrolysate-flaxseed gum emulsions: modulation of stability, interfacial properties, and curcumin bioaccessibility 超声驱动的牛骨蛋白水解-亚麻籽胶乳剂:稳定性、界面特性和姜黄素生物可及性的调节
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-12-01 Epub Date: 2025-10-30 DOI: 10.1016/j.ultsonch.2025.107658
Niancheng Hong , Shengnan Liu , Yueyu Bai , Yaodi Zhu , Miaoyun Li , Lijun Zhao , Gaiming Zhao , Dong Liang
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