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Transition-metal-free K2S2O8-promoted oxidative C-C triple bond cleavage and esterification leading to α-ketoesters. 无过渡金属的k2s2o8促进氧化C-C三键的裂解和酯化反应，生成α-酮酯。
IF 2.9 3区 化学
Organic & Biomolecular Chemistry Pub Date : 2025-07-04 DOI: 10.1039/d5ob00892a
Jin-Xin Lan, Yu Shu, Yang Zhou, Liu-Yu Shen, Fei Meng, Wen-Chao Yang
{"title":"Transition-metal-free K<sub>2</sub>S<sub>2</sub>O<sub>8</sub>-promoted oxidative C-C triple bond cleavage and esterification leading to α-ketoesters.","authors":"Jin-Xin Lan, Yu Shu, Yang Zhou, Liu-Yu Shen, Fei Meng, Wen-Chao Yang","doi":"10.1039/d5ob00892a","DOIUrl":"https://doi.org/10.1039/d5ob00892a","url":null,"abstract":"<p><p>A sustainable method for converting alkynes into α-ketoesters is reported through K<sub>2</sub>S<sub>2</sub>O<sub>8</sub>-promoted oxidative C-C triple bond cleavage and esterification. This approach avoids transition metal catalysis, photocatalysts, and pure oxygen conditions, making it both efficient and more convenient.</p>","PeriodicalId":96,"journal":{"name":"Organic & Biomolecular Chemistry","volume":" ","pages":""},"PeriodicalIF":2.9,"publicationDate":"2025-07-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144558557","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Supramolecular assembly properties of a mixed-sequence recognition-encoded melamine oligomer. 混合序列识别编码的三聚氰胺低聚物的超分子组装性质。
IF 2.9 3区 化学
Organic & Biomolecular Chemistry Pub Date : 2025-07-04 DOI: 10.1039/d5ob00769k
Mohit Dhiman, Joseph T Smith, Christopher A Hunter
{"title":"Supramolecular assembly properties of a mixed-sequence recognition-encoded melamine oligomer.","authors":"Mohit Dhiman, Joseph T Smith, Christopher A Hunter","doi":"10.1039/d5ob00769k","DOIUrl":"10.1039/d5ob00769k","url":null,"abstract":"<p><p>Recognition-encoded melamine oligomers (REMO) are composed of an alternating piperazine-triazine backbone and side-chains equipped with either a H-bond donor (phenol, D) or a H-bond acceptor (phosphine oxide, A). Complementary homo-oligomers form stable duplexes in organic solvents, due to intermolecular base-pairing interactions between the phenol and phosphine oxide side-chains. For mixed-sequence oligomers, the major pathway that competes with duplex formation is folding due to intramolecular base-pairing interactions. Automated solid phase synthesis was used to prepare the self-complementary REMO DADA, and this oligomer was used to investigate the competition between intermolecular and intramolecular H-bonding interactions. Isothermal titration calorimetry in chloroform showed that DADA forms a dimeric complex, but with reduced stability compared with the duplexes formed by shorter oligomers. The results indicate that a folded state with intramolecular interactions between the two terminal recognition units is significantly populated. The dimeric complex formed at higher concentrations could involve the interaction of two folded oligomers in a kissing stem-loops structure, or the oligomer could unfold to give the duplex with four intermolecular base-pairs. One end of the oligomer was equipped with an azide and the other with an alkyne, so that the dimeric complex could be covalently trapped using copper-catalysed azide-alkyne cycloaddition reactions. The major product was the macrocyclic duplex with small amounts of the macrocyclic single-strand, which shows that the DADA·DADA duplex dominates at millimolar concentrations. Understanding the propensity of the REMO architecture to fold will help guide the future design principles for synthesis of more complex functional assemblies.</p>","PeriodicalId":96,"journal":{"name":"Organic & Biomolecular Chemistry","volume":" ","pages":""},"PeriodicalIF":2.9,"publicationDate":"2025-07-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144558547","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Mild and efficient construction of nitrogen-containing heterocycles from ortho-ethynylbenzaldehydes and anilines. 邻乙基苯甲醛和苯胺温和高效地构建含氮杂环。
IF 2.9 3区 化学
Organic & Biomolecular Chemistry Pub Date : 2025-07-04 DOI: 10.1039/d5ob00634a
Juan Zhao, Hui-Min Qian, You Zi, Shun-Jun Ji, Xiao-Ping Xu
{"title":"Mild and efficient construction of nitrogen-containing heterocycles from <i>ortho</i>-ethynylbenzaldehydes and anilines.","authors":"Juan Zhao, Hui-Min Qian, You Zi, Shun-Jun Ji, Xiao-Ping Xu","doi":"10.1039/d5ob00634a","DOIUrl":"https://doi.org/10.1039/d5ob00634a","url":null,"abstract":"<p><p>A mild and transition-metal-free strategy for the synthesis of isoindolin-1-imines and isoquinolinium salts has been developed using <i>ortho</i>-ethynylbenzaldehydes and anilines. HFIP was employed as an effective promoter, facilitating nucleophilic addition and annulation to afford diverse isoindolin-1-imines in good yields. Alternatively, isoquinolinium salts were obtained by addition of ammonium iodide. Both reactions exhibited broad functional group tolerance and were successfully applied on gram scales as well as for further transformation, providing a practical strategy in pharmaceutical development and organic synthesis.</p>","PeriodicalId":96,"journal":{"name":"Organic & Biomolecular Chemistry","volume":" ","pages":""},"PeriodicalIF":2.9,"publicationDate":"2025-07-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144558546","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Ruthenium-catalysed isomerisation-methylenation of allyl alcohols with methanol: a one-pot synthesis of substituted pyridines. 钌催化烯丙醇与甲醇的异构甲基化：取代吡啶的一锅合成。
IF 2.9 3区 化学
Organic & Biomolecular Chemistry Pub Date : 2025-07-03 DOI: 10.1039/d5ob00881f
Priyabrata Biswal, Sanu Siyad Pullarat, Shaikh Samser, Basava Punna Rao Aradhyula, Vadapalli Chandrasekhar, Krishnan Venkatasubbaiah
{"title":"Ruthenium-catalysed isomerisation-methylenation of allyl alcohols with methanol: a one-pot synthesis of substituted pyridines.","authors":"Priyabrata Biswal, Sanu Siyad Pullarat, Shaikh Samser, Basava Punna Rao Aradhyula, Vadapalli Chandrasekhar, Krishnan Venkatasubbaiah","doi":"10.1039/d5ob00881f","DOIUrl":"https://doi.org/10.1039/d5ob00881f","url":null,"abstract":"<p><p>A simple bench-stable ruthenium complex facilitates the synthesis of tetra-substituted pyridines in one pot <i>via</i> isomerisation-methylenation of allyl alcohol using methanol as a C1 source. This methodology is applicable to a broad range of electronically diverse diaryl and monoaryl allyl alcohols, making it highly robust for synthesising substituted pyridines. Mechanistic investigations, including control experiments and isotope labelling studies, demonstrate the involvement of metal hydride species in the isomerisation-methylenation of allyl alcohol. Additionally, many of the tetra-substituted pyridines synthesised using this methodology exhibited good photophysical properties, illustrating its potential to generate interesting materials with applicability in organic electronics.</p>","PeriodicalId":96,"journal":{"name":"Organic & Biomolecular Chemistry","volume":" ","pages":""},"PeriodicalIF":2.9,"publicationDate":"2025-07-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144551468","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Improvement of N-benzoylation catalysis driven by an amyloid-substrate complex. 淀粉样蛋白-底物复合物驱动n -苯甲酰化催化的改进。
IF 2.9 3区 化学
Organic & Biomolecular Chemistry Pub Date : 2025-07-02 DOI: 10.1039/d5ob00593k
Kai Yamamoto, Taka Sawazaki, Youhei Sohma
{"title":"Improvement of <i>N</i>-benzoylation catalysis driven by an amyloid-substrate complex.","authors":"Kai Yamamoto, Taka Sawazaki, Youhei Sohma","doi":"10.1039/d5ob00593k","DOIUrl":"https://doi.org/10.1039/d5ob00593k","url":null,"abstract":"<p><p>Nucleophilic reactions of amines are important chemical transformations, but the reactions are incompatible with acidic buffer conditions. Azo-stilbene is a motif that binds to amyloids formed by accumulation of β-sheet peptides. We previously reported that the amino group attached to azo-stilbene is activated by proximity to an amyloid catalyst, promoting nucleophilic reactions in acidic buffers. Here, we show that we could improve the <i>N</i>-benzoylation yield for what was previously a difficult substrate by (1) derivatizing an amyloid catalyst, (2) modulating the amyloid morphology with His, and (3) adding thioflavin-T as a reaction additive. These results are predicted to accelerate the application of the amine modification catalysis system driven by the amyloid-substrate complex and to advance research on functional molecules containing an azo-stilbene motif.</p>","PeriodicalId":96,"journal":{"name":"Organic & Biomolecular Chemistry","volume":" ","pages":""},"PeriodicalIF":2.9,"publicationDate":"2025-07-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144537475","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Production of subtilosin A in E. coli: insights into the head-to-tail macrocyclization. 大肠杆菌中subtilosin A的产生：对首尾大环化的洞察。
IF 2.9 3区 化学
Organic & Biomolecular Chemistry Pub Date : 2025-07-02 DOI: 10.1039/d4ob01816h
Yifei Jia, Yuanjun Han, Wenning Wang, Qi Zhang
{"title":"Production of subtilosin A in <i>E. coli</i>: insights into the head-to-tail macrocyclization.","authors":"Yifei Jia, Yuanjun Han, Wenning Wang, Qi Zhang","doi":"10.1039/d4ob01816h","DOIUrl":"https://doi.org/10.1039/d4ob01816h","url":null,"abstract":"<p><p>Subtilosin A is the canonical member of the sactipeptide family with significant antimicrobial properties. In this study, we successfully produced subtilosin A in <i>Escherichia coli</i> by coexpressing the precursor peptide SboA with the radical SAM enzyme AlbA, and the metalloenzymes AlbE and AlbF. Our findings demonstrate that both AlbE and AlbF are essential for the head-to-tail macrocyclization of subtilosin A. We also identified an open-chain analog of subtilosin A, subtilosin A<sub>OC</sub>, which retains the thioether crosslinks but lacks the macrocyclic structure. Subtilosin A<sub>OC</sub> is likely a biosynthetic intermediate of subtilosin A, which exhibits observable but significantly decreased antibacterial activity compared to subtilosin A. These results provide valuable insights into the biosynthesis of subtilosin A and pave the way for future research on the sactipeptide family of natural products.</p>","PeriodicalId":96,"journal":{"name":"Organic & Biomolecular Chemistry","volume":" ","pages":""},"PeriodicalIF":2.9,"publicationDate":"2025-07-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144537478","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Antiadhesive glycoconjugate metal complexes targeting pathogens Pseudomonas aeruginosa and Candida albicans. 针对病原菌铜绿假单胞菌和白色念珠菌的抗粘附糖结合金属配合物。
IF 2.9 3区 化学
Organic & Biomolecular Chemistry Pub Date : 2025-07-02 DOI: 10.1039/d5ob00970g
Karolina Wojtczak, Emilie Gillon, Diana Bura, Karen Richmond, Megan Joyce, Emma Caraher, Keela Kessie, Trinidad Velasco-Torrijos, Cristina Trujillo, Anne Imberty, Kevin Kavanagh, Gordon Cooke, Joseph P Byrne
{"title":"Antiadhesive glycoconjugate metal complexes targeting pathogens <i>Pseudomonas aeruginosa</i> and <i>Candida albicans</i>.","authors":"Karolina Wojtczak, Emilie Gillon, Diana Bura, Karen Richmond, Megan Joyce, Emma Caraher, Keela Kessie, Trinidad Velasco-Torrijos, Cristina Trujillo, Anne Imberty, Kevin Kavanagh, Gordon Cooke, Joseph P Byrne","doi":"10.1039/d5ob00970g","DOIUrl":"https://doi.org/10.1039/d5ob00970g","url":null,"abstract":"<p><p>Glycoconjugates are known to interact with carbohydrate-binding proteins involved in adhesion by pathogens, and offer opportunities to design antimicrobial agents. Metal complexes with Eu(III), Ni(II) and Zn(II) were prepared from glycoconjugate ligand 1Gal, which binds to <i>P. aeruginosa</i>'s lectin LecA (<i>K</i><sub>d</sub> 9.6 ± 0.7 μM). <i>In vitro</i> anti-adhesive activity of these compounds was evaluated for both <i>P. aeruginosa</i> and <i>C. albicans</i>. Choice of metal ion played a crucial role in modulating anti-adhesive activity, with Eu(III) complexes most effective: [Eu·(1Gal)(H<sub>2</sub>O)<sub>6</sub>](CF<sub>3</sub>SO<sub>3</sub>)<sub>3</sub> inhibits 60% biofilm formation by <i>P. aeruginosa</i> and [Eu·(1Gal)<sub>3</sub>](CF<sub>3</sub>SO<sub>3</sub>)<sub>3</sub> inhibits 62% of <i>C. albicans</i> adhesion to buccal epithelial cells (both at 0.1 mM). The results presented demonstrate the potential for metal coordination to significantly enhance biological activity of glycoconjugates, surpassing the effect of the ligand's modest lectin-binding affinity alone.</p>","PeriodicalId":96,"journal":{"name":"Organic & Biomolecular Chemistry","volume":" ","pages":""},"PeriodicalIF":2.9,"publicationDate":"2025-07-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144537471","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Efficient homogeneous-like enantioselective catalysis of a bulky chiral catalyst: covalent immobilization of chiral spirocyclic phosphoric acid onto polystyrene brushes grafted on SiO2 nanospheres. 大体积手性催化剂的高效类均相对映选择性催化：手性螺旋环磷酸共价固定在SiO2纳米球接枝的聚苯乙烯刷上。
IF 2.9 3区 化学
Organic & Biomolecular Chemistry Pub Date : 2025-07-02 DOI: 10.1039/d5ob00641d
Yongyue Luo, Wenyan Tian, Yang Zhou, Chuangchuang He, Xuebing Ma
{"title":"Efficient homogeneous-like enantioselective catalysis of a bulky chiral catalyst: covalent immobilization of chiral spirocyclic phosphoric acid onto polystyrene brushes grafted on SiO<sub>2</sub> nanospheres.","authors":"Yongyue Luo, Wenyan Tian, Yang Zhou, Chuangchuang He, Xuebing Ma","doi":"10.1039/d5ob00641d","DOIUrl":"https://doi.org/10.1039/d5ob00641d","url":null,"abstract":"<p><p>To solve the mass transfer limitation and multi-step immobilization of bulky chiral phosphoric acids in heterogeneous asymmetric catalysis, this paper develops a direct immobilization of (<i>R</i>)-6,6'-di(9-anthryl)spirobiindane phosphoric acid ((<i>R</i>)-AnSPA) <i>via</i> Friedel-Crafts alkylation onto SiO<sub>2</sub>-grafted poly(<i>p</i>-vinylbenzyl chloride) (PVBC) brushes (PVBC@SiO<sub>2</sub>) and hollow mesoporous PVBC nanospheres (HMPNs), affording supported organocatalysts (AnSPA#PVBC@SiO<sub>2</sub> and AnSPA@HMPNs), respectively. Owing to the good dispersibility of PVBC brushes in organic solvents, the PVBC brush-anchored (<i>R</i>)-AnSPA with an open-ended structure enables the enantioselective desymmetrization of oxetanes with mercaptobenzothiazoles to proceed in a homogeneous-like manner, leading to the improved mass transfer of reactants due to alleviative steric hindrance. Compared to the homogeneous (<i>R</i>)-AnSPA, the PVBC brush-anchored (<i>R</i>)-AnSPA shows decrements in yield and enantioselectivity below 2%. However, the HMPN-anchored (<i>R</i>)-AnSPA shows larger decrements in yields (3-6%) and enantioselectivities (3-7% ee). Furthermore, AnSPA#PVBC@SiO<sub>2</sub> exhibits good reusability in enantioselective desymmetrization with no significant decreases in yield and enantioselectivity. Particularly, the deactivated AnSPA#PVBC@SiO<sub>2</sub>, caused by the hydrolysis of phosphate ester in (<i>R</i>)-AnSPA, can be easily renovated to its fresh state by dealing with POCl<sub>3</sub>. Overall, the direct immobilization of (<i>R</i>)-AnSPA onto PVBC brushes and renovation of deactivated (<i>R</i>)-AnSPA provide an effective strategy for achieving high sustainability of expensive chiral spirocyclic phosphoric acids in large-scale synthesis.</p>","PeriodicalId":96,"journal":{"name":"Organic & Biomolecular Chemistry","volume":" ","pages":""},"PeriodicalIF":2.9,"publicationDate":"2025-07-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144537474","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
One-pot synthesis of trans-2,3-diaminoindolines through 2,3-diamination of electrophilic indolines. 亲电吲哚二胺化一锅法合成反式-2,3-二氨基吲哚。
IF 2.9 3区 化学
Organic & Biomolecular Chemistry Pub Date : 2025-07-02 DOI: 10.1039/d5ob00877h
Yuito Kobori, Keisuke Tokushige, Takumi Abe
{"title":"One-pot synthesis of <i>trans</i>-2,3-diaminoindolines through 2,3-diamination of electrophilic indolines.","authors":"Yuito Kobori, Keisuke Tokushige, Takumi Abe","doi":"10.1039/d5ob00877h","DOIUrl":"https://doi.org/10.1039/d5ob00877h","url":null,"abstract":"<p><p>Despite recent advances in the synthesis of 2,3-diaminoindole derivatives, construction of 2,3-diaminoindolines, whose two amine moieties on each molecule differ from one another has yet to be achieved. In this work, we developed a concise one-pot protocol for differentiated diamination involving reacting a C2,C3-electrophilic indole reagent with amines to access a variety of previously inaccessible 2,3-diaminoindolines. Furthermore, the synthetic utility of this protocol was demonstrated by a successful gram-scale reaction and further transformation of the 2,3-diaminoindolines.</p>","PeriodicalId":96,"journal":{"name":"Organic & Biomolecular Chemistry","volume":" ","pages":""},"PeriodicalIF":2.9,"publicationDate":"2025-07-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144537477","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Ni-Catalyzed intramolecular cyclization of Baylis-Hillman adducts of 2-cyanoaniline towards 2,3-dihydroquinolin-4(1H)-ones. ni催化2-氰苯胺Baylis-Hillman加合物分子内环化2,3-二氢喹啉-4(1H)- 1。
IF 2.9 3区 化学
Organic & Biomolecular Chemistry Pub Date : 2025-07-02 DOI: 10.1039/d5ob00778j
Min Yang, Xuanfeng Li, Tingxi Lai, Jian Xiao, Minghui Xu, Bin Chen, Hai-Liang Ni, Bi-Qin Wang, Ping Hu, Peng Cao
{"title":"Ni-Catalyzed intramolecular cyclization of Baylis-Hillman adducts of 2-cyanoaniline towards 2,3-dihydroquinolin-4(1<i>H</i>)-ones.","authors":"Min Yang, Xuanfeng Li, Tingxi Lai, Jian Xiao, Minghui Xu, Bin Chen, Hai-Liang Ni, Bi-Qin Wang, Ping Hu, Peng Cao","doi":"10.1039/d5ob00778j","DOIUrl":"https://doi.org/10.1039/d5ob00778j","url":null,"abstract":"<p><p>A Ni-catalyzed reductive cyclization of Baylis-Hillman adducts of 2-cyanoaniline is presented. A novel class of quinolin-4-ones containing a quaternary carbon center were synthesized in moderate to good yields. With <sup>i</sup>Pr-PyBOX as a chiral ligand, the catalytic enantioselective cyclization gave a moderate yield and ee.</p>","PeriodicalId":96,"journal":{"name":"Organic & Biomolecular Chemistry","volume":" ","pages":""},"PeriodicalIF":2.9,"publicationDate":"2025-07-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144537476","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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