Micron最新文献

{"title":"Microscopic chemical characterization of epoxy resin with scanning transmission electron microscopy – electron energy-loss spectroscopy","authors":"Hsin-Hui Huang ,&nbsp;Tomohiro Miyata ,&nbsp;Yohei K. Sato ,&nbsp;Teruyasu Mizoguchi ,&nbsp;Hiroshi Jinnai ,&nbsp;Kaname Yoshida","doi":"10.1016/j.micron.2024.103623","DOIUrl":"https://doi.org/10.1016/j.micron.2024.103623","url":null,"abstract":"<div><p>The structural characterization of epoxy resins is essential to improve the understanding on their structure–property relationship for promising high-performance applications. Among all analytical techniques, scanning transmission electron microscopy–electron energy-loss spectroscopy (STEM–EELS) is a powerful tool for probing the chemical and structural information of various materials at a high spatial resolution. However, for sensitive materials, such as epoxy resins, the structural damage induced by electron-beam irradiation limits the spatial resolution in the STEM–EELS analysis. In this study, we demonstrated the extraction of the intrinsic features and structural characteristics of epoxy resins by STEM–EELS under electron doses below 1 e^–/Ų at room temperature. The reliability of the STEM–EELS analysis was confirmed by X-ray absorption spectroscopy and spectrum simulation as low- or non-damaged reference data. The investigation of the dependence of the epoxy resin on the electron dose and exposure time revealed the structural degradation associated with electron-beam irradiation, exploring the prospect of EELS for examining epoxy resin at low doses. Furthermore, the degradation mechanisms in the epoxy resin owing to electron-beam irradiation were revealed. These findings can promote the structural characterization of epoxy-resin-based composites and other soft materials.</p></div>","PeriodicalId":18501,"journal":{"name":"Micron","volume":null,"pages":null},"PeriodicalIF":2.4,"publicationDate":"2024-03-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140069506","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Orientation-dependent oxidation behavior of Cu under In-situ E-Beam irradiation","authors":"Weiwei Xia ,&nbsp;Quan An ,&nbsp;Lianyang Chen ,&nbsp;Ran Cai","doi":"10.1016/j.micron.2024.103622","DOIUrl":"10.1016/j.micron.2024.103622","url":null,"abstract":"<div><p>Herein, we present an atomic <em>in-situ</em> investigation of Cu oxidation along different orientations stimulated by high-energy electron beams (E-Beam) in transmission electron microscopy (TEM). By following the microstructural evolution of the Cu substrate in real time, high-resolution TEM (HRTEM) images reveal an orientation-dependent oxidation mechanism, whereby Cu along [110] zone axis migrates onto the surface and be oxidized while Cu along [100] zone axis is oxidized completely both in bulk and at the surface. The different oxidation mechanisms can be attributed to the differing diffusion rates of oxygen in Cu structures along directions. Moreover, the growth of Cu oxides is found to follow a layer-by-layer mechanism, where Cu mostly migrates onto nanocrystal {110} planes. This behavior would lead to the oxides wider in geometric shape and therefore promote the aggregation of adjacent oxides. These findings have important implications for the practical use of copper-based materials in oxidizing environments.</p></div>","PeriodicalId":18501,"journal":{"name":"Micron","volume":null,"pages":null},"PeriodicalIF":2.4,"publicationDate":"2024-03-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140044684","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Propionic acid affects the synaptic architecture of rat hippocampus and prefrontal cortex","authors":"Mzia G. Zhvania ,&nbsp;Giorgi Lobzhanidze ,&nbsp;Nino Pochkhidze ,&nbsp;Nadezhda Japaridze ,&nbsp;Pavel Tchelidze ,&nbsp;Fuad Rzayev ,&nbsp;Eldar Gasimov","doi":"10.1016/j.micron.2024.103624","DOIUrl":"10.1016/j.micron.2024.103624","url":null,"abstract":"<div><p>It is well documented that propionic acid (PPA) produces behavioral, morphological, molecular and immune responses in rats that are characteristic of autism spectrum disorder in humans. However, whether PPA affects the ultrastructure and synaptic architecture of regions of autistic brain has not been adequately addressed. Earlier we show that single intraperitoneal (IP) injection of PPA (175 mg/kg) produces superficial changes in the spatial memory and learning of adolescent male Wistar rats. However, in neurons, synapses and glial cells of hippocampal CA1 area and medial prefrontal cortex transient (mainly) or enduring alterations were detected. In this study, we used electron microscopic morphometric analysis to test the effect of PPA on different structural parameters of axodendritic synapses of the hippocampus and prefrontal cortex. The animals were treated with a single IP injection of PPA (175 mg/kg). The length and width of synaptic active zone, the area of presynaptic and postsynaptic mitochondria, the distance between presynaptic mitochondria and the synapse active zone, the distance between postsynaptic mitochondria and postsynaptic density and the depth and opening diameter of neuronal porosome complex were evaluated. Our results show that synaptic mitochondria of the hippocampus and prefrontal cortex are the most vulnerable to PPA treatment: in both regions, the area of postsynaptic mitochondria were increased. In general, our results show that even small dose of PPA, which produces only superficial effects on spatial memory and learning is able to alter the synapse architecture in brain regions involved in cognition and autism pathogenesis. Therefore, the microbiome may be involved in the control of neurotransmission in these regions.</p></div>","PeriodicalId":18501,"journal":{"name":"Micron","volume":null,"pages":null},"PeriodicalIF":2.4,"publicationDate":"2024-03-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140044690","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Recent developments in denoising medical images using deep learning: An overview of models, techniques, and challenges","authors":"Nahida Nazir ,&nbsp;Abid Sarwar ,&nbsp;Baljit Singh Saini","doi":"10.1016/j.micron.2024.103615","DOIUrl":"10.1016/j.micron.2024.103615","url":null,"abstract":"<div><p>Medical imaging plays a critical role in diagnosing and treating various medical conditions. However, interpreting medical images can be challenging even for expert clinicians, as they are often degraded by noise and artifacts that can hinder the accurate identification and analysis of diseases, leading to severe consequences such as patient misdiagnosis or mortality. Various types of noise, including Gaussian, Rician, and Salt-pepper noise, can corrupt the area of interest, limiting the precision and accuracy of algorithms. Denoising algorithms have shown the potential in improving the quality of medical images by removing noise and other artifacts that obscure essential information. Deep learning has emerged as a powerful tool for image analysis and has demonstrated promising results in denoising different medical images such as MRIs, CT scans, PET scans, etc. This review paper provides a comprehensive overview of state-of-the-art deep learning algorithms used for denoising medical images. A total of 120 relevant papers were reviewed, and after screening with specific inclusion and exclusion criteria, 104 papers were selected for analysis. This study aims to provide a thorough understanding for researchers in the field of intelligent denoising by presenting an extensive survey of current techniques and highlighting significant challenges that remain to be addressed. The findings of this review are expected to contribute to the development of intelligent models that enable timely and accurate diagnoses of medical disorders. It was found that 40% of the researchers used models based on Deep convolutional neural networks to denoise the images, followed by encoder-decoder (18%) and other artificial intelligence-based techniques (15%) (Like DIP, etc.). Generative adversarial network was used by 12%, transformer-based approaches (13%) and multilayer perceptron was used by 2% of the researchers. Moreover, Gaussian noise was present in 35% of the images, followed by speckle noise (16%), poisson noise (14%), artifacts (10%), rician noise (7%), Salt-pepper noise (6%), Impulse noise (3%) and other types of noise (9%). While the progress in developing novel models for the denoising of medical images is evident, significant work remains to be done in creating standardized denoising models that perform well across a wide spectrum of medical images. Overall, this review highlights the importance of denoising medical images and provides a comprehensive understanding of the current state-of-the-art deep learning algorithms in this field.</p></div>","PeriodicalId":18501,"journal":{"name":"Micron","volume":null,"pages":null},"PeriodicalIF":2.4,"publicationDate":"2024-03-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140035554","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Examining cut mark residue with SEM to identify metal tool use: An experimental study","authors":"Francesc Marginedas ,&nbsp;Josep Maria Vergès ,&nbsp;Palmira Saladié ,&nbsp;Antonio Rodríguez-Hidalgo","doi":"10.1016/j.micron.2024.103614","DOIUrl":"10.1016/j.micron.2024.103614","url":null,"abstract":"<div><p>In this manuscript, we explore the potential of studying metal residues in cut marks generated by copper and bronze knives. The method was developed in the forensic sciences for use with modern metals in order to identify microscopic particles of metal tools on bone surfaces. However, the study of residues in archaeological materials can be challenging due to the ways in which the bone remains may have been manipulated, both in the past and in more recent times. Using a scanning electron microscope (SEM), we detected microscopic fragments of bronze and copper knives along with contamination both inside and outside of the cut marks made by those knives. Copper and bronze residues were identified embedded in the bone inside the incisions and, in two cases, they left greenish stains caused by metal oxidation. In contrast, modern contamination of undetermined origin was found unattached to the bone and had a chemical composition not compatible with that of the knives. The amount of residue was influenced by the quantity of soft tissue between the bone and the knife during the butchering tasks. Bone cooking does not seem to influence the preservation of the residues. We anticipate that the approach used in this first exploratory study will emerge as a promising method for identifying the use of metal tools in archaeological bone remains.</p></div>","PeriodicalId":18501,"journal":{"name":"Micron","volume":null,"pages":null},"PeriodicalIF":2.4,"publicationDate":"2024-02-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.sciencedirect.com/science/article/pii/S0968432824000313/pdfft?md5=7e4e9dd19856cfc4a4d5a2d824bb134b&pid=1-s2.0-S0968432824000313-main.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139981127","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"EBSD investigation of microstructure and microtexture evolution on additively manufactured TiC-Fe based cermets—Influence of multiple laser scanning","authors":"H.S. Maurya ,&nbsp;R.J. Vikram ,&nbsp;R. Kumar ,&nbsp;R. Rahmani ,&nbsp;K. Juhani ,&nbsp;F. Sergejev ,&nbsp;K.G. Prashanth","doi":"10.1016/j.micron.2024.103613","DOIUrl":"10.1016/j.micron.2024.103613","url":null,"abstract":"<div><p>Sustainable TiC-Fe-based cermets have been fabricated by adopting an Additive Manufacturing route based on laser powder bed fusion technology (L-PBF). The objective is to produce crack-free cermet components by employing novel multiple laser scanning techniques with variations in laser process parameters. Electron backscatter diffraction analysis (EBSD) was used to study the microstructure and microtexture evolution with variations in laser process parameters. The investigation revealed that adjusting the preheating scan speed (PHS) and melting scan speed (MS) influenced the growth and nucleation of TiC phases. Lowering these speeds resulted in grain coarsening, while higher scan speeds led to grain refinement with larger sub-grain boundaries. Moreover, a high scanning speed increases the degree of dislocation density and internal stress in the fabricated cermet parts. Notably, it is revealed that decreasing the laser scan speed enhanced the proportion of high-angle grain boundaries in the cermet components, signifying an increase in material ductility.</p></div>","PeriodicalId":18501,"journal":{"name":"Micron","volume":null,"pages":null},"PeriodicalIF":2.4,"publicationDate":"2024-02-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139952588","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Structural and mechanical characterization of the hoof in Mongolian equids","authors":"Nuo Chen ,&nbsp;Xin Yang ,&nbsp;Shucai Xu ,&nbsp;Jiafeng Song","doi":"10.1016/j.micron.2024.103609","DOIUrl":"10.1016/j.micron.2024.103609","url":null,"abstract":"<div><p>In this paper, the microstructure and mechanical properties (including nanoindentation, tensile test, and compression test) of Mongolian horse hooves were investigated. Many tubules and Intermediate Filaments (IF) were distributed longitudinally in the hoof of Mongolian horses, which could better help the hoof cushioning. The hardness and modulus of the hoof wall of Mongolian horses varied at different water contents. The hardness and modulus decreased with the increase in water content. The modulus of elasticity of the hoof wall decreased from 16.3% to 25.4%, and the hardness decreased from 17.8% to 29.3% from 10% to 20% water content. At 20–30% water content, the horseshoe wall modulus decreased by 3.5%−4.8%, and the hardness reduced by 4.1%−7.3%. The results of the tensile and compression experiments showed that the compression properties of Mongolian horse hooves were better than their tensile properties; their longitudinal compression energy absorption was better than their transverse compression properties; and Young's modulus and yield strength of the hoof wall increased as the compression rate increased. Finally, comparing the experiments belonging to this paper with hooves from other papers, it was found that the hardness of the tubular region and the intertubular region of Mongolian horse hooves was 17.7% and 39.4% higher than that of the hooves from the current study, respectively. The microstructural features of Mongolian horse-like hooves with superior mechanical properties provide a promising inspiration for the bionic design of lightweight and high-strength composites in engineering.</p></div>","PeriodicalId":18501,"journal":{"name":"Micron","volume":null,"pages":null},"PeriodicalIF":2.4,"publicationDate":"2024-02-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139922167","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Comparative study of ion milling techniques for the preparation of ceramic fibers in transmission electron microscopy","authors":"Clémentine Fellah ,&nbsp;Bérangère Lesaint","doi":"10.1016/j.micron.2024.103612","DOIUrl":"10.1016/j.micron.2024.103612","url":null,"abstract":"<div><p>Sample preparation, essential to any analysis, remains an under-documented step. Preparation methods for transmission electron microscopy (TEM) are complex and lead to artifacts that need to be identified to avoid wrong conclusions about the sample's microstructure. Ion milling techniques are increasingly becoming the reference techniques to prepare thin foils. The possibilities of different ion beam processes for milling samples will be shown and compared, using ceramic carbon/carbide fibers, a material applied in many industrial applications, as a test specimen. This overview of ion milling preparation techniques will enable us to identify the advantages, disadvantages and parameters in order to best prepare these thin samples. It will be carried out for the community, and will also highlight a new preparation method for ceramic fibers to minimize the artefacts inherent in these techniques.</p></div>","PeriodicalId":18501,"journal":{"name":"Micron","volume":null,"pages":null},"PeriodicalIF":2.4,"publicationDate":"2024-02-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139922080","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"A comparative approach employing microCT for the analysis of Cenozoic foraminifera from the Brazilian carbonate equatorial platform","authors":"Olga Oliveira De Araújo ,&nbsp;Orangel Aguilera ,&nbsp;Dayana Alvarado Sierra ,&nbsp;Beatriz Teixeira Guimarães ,&nbsp;Vinicius Kutter ,&nbsp;Ana Paula Linhares ,&nbsp;Daniel Lima ,&nbsp;Julianny Dos Santos Silva ,&nbsp;Ricardo Tadeu Lopes","doi":"10.1016/j.micron.2024.103611","DOIUrl":"10.1016/j.micron.2024.103611","url":null,"abstract":"<div><p>Worldwide, some of the largest hydrocarbon reservoirs are located in tropical neritic carbonate deposits. Biostratigraphic and paleoenvironmental analyzes of these sedimentary records are often based on the study of foraminiferal assemblage. Foraminifera-based biozones are widely employed in the oil industry to support drilling processes that, alongside petrophysical prospecting, define interval favorable for exploiting hydrocarbon resources. Both scientific research and the petroleum industry, however, usually apply traditional petrographical and paleontological methods to analyze microfossil assemblages, especially for large benthic foraminifera. New, faster, and more accurate methods based on microCT analyzes have emerged as a valuable high-output tool to obtain high-resolution microfossil records for biostratigraphy and paleoenvironmental reconstructions. This method is also useful for the development of digital databases for artificial intelligence applications. MicroCT analyzes, therefore, lead to faster identification of foraminifera assemblage and support digital access to international foraminifera repositories and reference collections, introducing a new dimension in micropaleontological research.</p></div>","PeriodicalId":18501,"journal":{"name":"Micron","volume":null,"pages":null},"PeriodicalIF":2.4,"publicationDate":"2024-02-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139825037","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Novel technology for controlled fabrication of aperture cantilever sensors for scanning near-field optical microscopy","authors":"A.S. Kolomiytsev ,&nbsp;A.V. Kotosonova ,&nbsp;O.I. Il’in ,&nbsp;A.V. Saenko ,&nbsp;A.V. Shelaev ,&nbsp;A.V. Baryshev","doi":"10.1016/j.micron.2024.103610","DOIUrl":"https://doi.org/10.1016/j.micron.2024.103610","url":null,"abstract":"<div><p>This paper presents a new technique for forming SNOM (Scanning Near-Field Optical Microscopy) cantilevers. The technique is based on the continuous growth of a conical hollow tip using local ion-induced carbon deposition on standard tipless cantilever chips. This method offers precise control of the geometric parameters of the cantilever's tip, including the angle of the tip, the probe's curvature radius, and the input and output aperture diameter. Such control allows to optimize the probe for specific tasks. The use of local structure methods based on FIB (Focused Ion Beam) enables the production of SNOM cantilevers with high radiation transmittance, tip robustness, and the capability to measure sample topography in semi-contact AFM (Atomic Force Microscopy) mode. The research focused on optimizing the technology for manufacturing tips with specific geometric characteristics, facilitating accurate navigation and positioning in the area of interest. The manufactured probe samples being tested demonstrate sufficient accuracy and mechanical durability of the tip. Overall, this technique offers a novel approach to forming SNOM cantilevers, providing precise control over geometric parameters and promising enhanced performance in various applications.</p></div>","PeriodicalId":18501,"journal":{"name":"Micron","volume":null,"pages":null},"PeriodicalIF":2.4,"publicationDate":"2024-02-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139749584","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}