Ultrasonics Sonochemistry最新文献

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Flow field regulation and sediment particle flocculation mechanisms in ultrasound-assisted electrocoagulation intervention 超声辅助电絮凝干预中的流场调节和沉积物颗粒絮凝机理
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-09-10 DOI: 10.1016/j.ultsonch.2025.107558
Yifeng Liu , Wenwen Bai , Jiahua Wei , Zhen Qiao , Shangyao Du
{"title":"Flow field regulation and sediment particle flocculation mechanisms in ultrasound-assisted electrocoagulation intervention","authors":"Yifeng Liu ,&nbsp;Wenwen Bai ,&nbsp;Jiahua Wei ,&nbsp;Zhen Qiao ,&nbsp;Shangyao Du","doi":"10.1016/j.ultsonch.2025.107558","DOIUrl":"10.1016/j.ultsonch.2025.107558","url":null,"abstract":"<div><div>Ultrasound-assisted electrocoagulation (US-EC) shows promise in improving flocculation through cavitation and flow field regulation, yet the mechanisms of flow field evolution and particle size control under acoustic-electric coupling remain underexplored. In this study, an acoustic-electric coupling observation platform for suspended sediment flocculation was established. The motion response characteristics of gas–solid and mixed phases under the intervention of acoustic-electric coupling were observed by employing Particle Image Velocimetry (PIV). Then, the effects of different ultrasonic frequencies and current densities on flow field characteristics, particle size distribution, and flocculation behavior were systematically explored, and ultimately, the synergistic mechanism of US-EC in particle fragmentation and aggregation was revealed. According to the experimental results, low-frequency (28 kHz) ultrasound, owing to a strong cavitation effect, can effectively fragment medium-sized particles while enhancing the specific surface area and fluid disturbances. Meanwhile, high current density (40 A/m<sup>2</sup>) can accelerate electrolytic reactions and promote rapid reduction of Zeta potential, thereby promoting efficient particle aggregation. Under the operating condition of 28 kHz + 40 A/m<sup>2</sup>, the fluid system maintained a moderate flow velocity (11.01 mm/s) with uniform vorticity distribution, leading to a dynamic balance between disturbance intensity and floc structural stability (15 ≤ <em>η/D</em> &lt; 25, 10<sup>−6</sup> ≲ <em>ε</em> ≲ 10<sup>−4</sup> m<sup>2</sup> s<sup>−3</sup>), which significantly enhanced flocculation efficiency. Accordingly, the average particle size increased from 18.89 μm to 60.98 μm, with a sedimentation rate of 87.96 %. Overall, the US-EC process follows a three-phase evolution path: “ultrasound-induced fragmentation, EC-driven aggregation, gravity-induced sedimentation”. The flow velocity and vorticity collaboratively regulate the particle migration paths, collision efficiency, and floc stability, while Zeta potential exhibits a control effect on particle aggregation rate. These mechanisms complement each other temporally to enhance the overall treatment performance.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"121 ","pages":"Article 107558"},"PeriodicalIF":9.7,"publicationDate":"2025-09-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145045618","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Sonochemical synthesis of nanoparticles from bioactive compounds: advances, challenges, and future perspectives 生物活性化合物声化学合成纳米颗粒:进展、挑战和未来展望
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-09-10 DOI: 10.1016/j.ultsonch.2025.107559
Gabriela Jajko-Liberka , Anagha M.G. , Paulina Chytrosz-Wróbel , Piotr Kubisiak , Waldemar Kulig , Lukasz Cwiklik , Andrzej Kotarba
{"title":"Sonochemical synthesis of nanoparticles from bioactive compounds: advances, challenges, and future perspectives","authors":"Gabriela Jajko-Liberka ,&nbsp;Anagha M.G. ,&nbsp;Paulina Chytrosz-Wróbel ,&nbsp;Piotr Kubisiak ,&nbsp;Waldemar Kulig ,&nbsp;Lukasz Cwiklik ,&nbsp;Andrzej Kotarba","doi":"10.1016/j.ultsonch.2025.107559","DOIUrl":"10.1016/j.ultsonch.2025.107559","url":null,"abstract":"<div><div>Sonochemical synthesis, driven by acoustic cavitation, has emerged over the past two decades as a powerful and versatile method for producing nanoparticles of bioactive substances with enhanced physicochemical and biological properties. The extreme conditions generated by the collapse of cavitation bubbles – such as transient high temperatures and pressures – facilitate molecular fragmentation, nucleation, and controlled nanoparticle growth. These characteristics make sonochemistry particularly well suited for nanosizing pharmaceuticals, enzymes, and natural bioactive compounds. In addition to a wide range of experimental techniques, recent advances in molecular dynamics simulations have offered critical insights into the molecular-level mechanisms underlying sonochemical processes, revealing the roles of solvent interactions and interfacial dynamics in determining nanoparticle size and stability. This deeper understanding has enabled more precise tuning of synthesis parameters to achieve desired nanoparticle characteristics. Sonochemically synthesized nanoparticles have demonstrated significant potential in diverse biomedical fields, including targeted drug delivery, sonodynamic therapy, regenerative medicine, and antimicrobial coatings. This minireview consolidates two decades of research, highlighting key advancements in the sonochemical synthesis of nanoparticles of bioactive substances, with a focus on molecular-level insights, biomedical applications, future research directions, ongoing challenges, and future perspectives.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"121 ","pages":"Article 107559"},"PeriodicalIF":9.7,"publicationDate":"2025-09-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145095586","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Microstructure and cavitation erosion behavior in overlapping vs. substrate areas of WAAM NAB WAAM NAB叠合与衬底区域的微观结构及空化侵蚀行为
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-09-10 DOI: 10.1016/j.ultsonch.2025.107562
Xiang Cai , Shuo Wang , Dun Miao , Shujun Li , Ruimin Gao , Yanxin Qiao , Mengmeng Yang , Jian Zhou , Qichao Zhang , Feng Xue
{"title":"Microstructure and cavitation erosion behavior in overlapping vs. substrate areas of WAAM NAB","authors":"Xiang Cai ,&nbsp;Shuo Wang ,&nbsp;Dun Miao ,&nbsp;Shujun Li ,&nbsp;Ruimin Gao ,&nbsp;Yanxin Qiao ,&nbsp;Mengmeng Yang ,&nbsp;Jian Zhou ,&nbsp;Qichao Zhang ,&nbsp;Feng Xue","doi":"10.1016/j.ultsonch.2025.107562","DOIUrl":"10.1016/j.ultsonch.2025.107562","url":null,"abstract":"<div><div>This study investigated the mechanism of influence of the microstructure of nickel-aluminum bronze (NAB) alloy prepared by wire-arc additive manufacturing (WAAM) on cavitation erosion (CE) and the synergistic effect of CE and corrosion. Microstructural analysis revealed that the earlier-deposited area in the overlapping area exhibited finer grain size (6.8 µm), higher β’ phase content (34.6 %), and dominant κ<sub>Ⅲ</sub>/κ<sub>Ⅳ</sub> precipitates, while the substrate featured coarser grain size (13.6 µm) and lower β’ phase content (23.2 %) featured coarser grain size (13.6 µm) and lower β’ phase content (23.2 %). CE testing indicated that in synthetic seawater, the cumulative mass loss in the overlapping area (75.2 mg) is lower than that in the substrate (82.32 mg), but the initial mass loss rate is faster. After CE, the alloy develops a 140 µm work-hardening layer, with peak hardness occurring at a depth of 20 µm. The synergistic effects of CE-corrosion accounted for 52 % of the total mass loss, with corrosion-promoted CE (34 %) exceeding CE-promoted corrosion.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"121 ","pages":"Article 107562"},"PeriodicalIF":9.7,"publicationDate":"2025-09-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145045591","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
The mouse motor cortex stimulation via non-invasive temporal interference transcranial focused ultrasound with microbubbles 无创颞叶干扰经颅聚焦超声微泡对小鼠运动皮层的刺激
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-09-10 DOI: 10.1016/j.ultsonch.2025.107561
Jie Jin , Xinze Liu , Zhenxiang Ji , Chenxuan Wu , Yuting Han , Quanrong Jing , Jian Zhang , Wei Li , Tianyi Yan , Hui Jing , Dingjie Suo
{"title":"The mouse motor cortex stimulation via non-invasive temporal interference transcranial focused ultrasound with microbubbles","authors":"Jie Jin ,&nbsp;Xinze Liu ,&nbsp;Zhenxiang Ji ,&nbsp;Chenxuan Wu ,&nbsp;Yuting Han ,&nbsp;Quanrong Jing ,&nbsp;Jian Zhang ,&nbsp;Wei Li ,&nbsp;Tianyi Yan ,&nbsp;Hui Jing ,&nbsp;Dingjie Suo","doi":"10.1016/j.ultsonch.2025.107561","DOIUrl":"10.1016/j.ultsonch.2025.107561","url":null,"abstract":"<div><div>Transcranial focused ultrasound (tFUS) has emerged as an innovative brain stimulation technology that uniquely integrates three characteristics: (a) non-invasive energy delivery, (b) submillimeter-scale spatial precision, and (c) effective penetration through cranial barriers to reach subcortical structures. Previous studies have shown that microbubbles (MBs) could amplify the mechanical effects of ultrasound, and the utilization of temporal interference ultrasound excitation effectively lowers cavitation thresholds. In this study, tFUS is applied to the motor cortex of both normal mice and MB-injected mice. Electromyography (EMG) recordings are utilized to analyze the effects of temporal interference (TI) ultrasound and single-frequency ultrasound stimulation on contralateral limb movements in mice. A hybrid model integrating the Gilmore-Akulichev-Zener (GAZ) model with nonlinear lipid membrane dynamics is developed, and numerical simulations of microbubble (MB) dynamics are performed to calculate the scattered pressure exerted by MBs on neurons. The study demonstrated that temporal interference ultrasound combined with MBs could increase the success rate of motor responses. The potential mechanism could be temporal interference ultrasound combined with MBs generate higher scattered pressures. The results demonstrated that temporal interference ultrasound combined with MBs could enhance neuronal activity in the Central Nervous System, enabling a highly specific method to increase the efficiency of tFUS stimulation.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"121 ","pages":"Article 107561"},"PeriodicalIF":9.7,"publicationDate":"2025-09-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145045607","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Emerging frontiers in juice processing: The role of ultrasonication and other non-thermal technologies in enhancing antioxidant capacity and quality of fruit and vegetable juices 果汁加工的新前沿:超声波和其他非热技术在提高果蔬汁的抗氧化能力和质量中的作用
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-09-09 DOI: 10.1016/j.ultsonch.2025.107554
Muhammad Umair , Muhammad Abid , Mishal Mumraiz , Saqib Jabbar , Song Xun , Kashif Ameer , Muhammad Shahid Riaz Rajoka , He Zhendan , Saqer S. Alotaibi , Robert Mugabi , Gulzar Ahmad Nayik
{"title":"Emerging frontiers in juice processing: The role of ultrasonication and other non-thermal technologies in enhancing antioxidant capacity and quality of fruit and vegetable juices","authors":"Muhammad Umair ,&nbsp;Muhammad Abid ,&nbsp;Mishal Mumraiz ,&nbsp;Saqib Jabbar ,&nbsp;Song Xun ,&nbsp;Kashif Ameer ,&nbsp;Muhammad Shahid Riaz Rajoka ,&nbsp;He Zhendan ,&nbsp;Saqer S. Alotaibi ,&nbsp;Robert Mugabi ,&nbsp;Gulzar Ahmad Nayik","doi":"10.1016/j.ultsonch.2025.107554","DOIUrl":"10.1016/j.ultsonch.2025.107554","url":null,"abstract":"<div><div>Fruit and vegetable juices (FVJs) are widely consumed due to their rich profile of vitamins, minerals, and bioactive compounds, particularly antioxidants, which play a critical role in mitigating non-communicable diseases. However, conventional thermal processing methods, while effective in microbial inactivation, significantly compromise the antioxidant capacity (AC), sensory attributes, and nutritional quality of FVJs. In response to growing consumer demand for minimally processed and functionally enriched juices, non-thermal technologies (NTTs) have emerged as promising alternatives. This review comprehensively evaluates recent advancements (2015–2024) in non-thermal processing methods—including ultrasonication, cold plasma, irradiation, and pulsed electric fields—and their influence on the AC and overall quality of FVJs.</div><div>NTTs enhance juice quality by inducing abiotic stress, activating antioxidant biosynthesis pathways, inactivating spoilage enzymes, and facilitating the release of bound phytochemicals. The review highlights the mechanistic insights, optimal processing parameters, and synergistic effects of combined NTT approaches on juice matrix, antioxidant retention, and enzymatic stability. Furthermore, it discusses the scalability, energy efficiency, and environmental sustainability of these technologies in comparison to traditional thermal methods. Despite promising outcomes at the laboratory scale, commercial adaptation of NTTs faces challenges such as equipment cost, process optimization for diverse juice matrices, regulatory acceptance, and consumer perception. Future directions emphasize the need for multidisciplinary collaborations to decode antioxidant metabolism, validate safety parameters (e.g., ROS/RNS residues), and develop industry-ready, cost-effective, and safe processing units. This review stands out by providing mechanistic insights, comparative efficacy, and optimization strategies of various NTTs specifically aimed at enhancing antioxidant capacity in fruit and vegetable juices. It also integrates a critical discussion on industrial scalability, regulatory challenges, and future biosynthetic pathway investigations, distinguishing it from prior reviews.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"122 ","pages":"Article 107554"},"PeriodicalIF":9.7,"publicationDate":"2025-09-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145157016","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Sonication-assisted emulsification: Analyzing different polymers in aqueous systems for microparticle preparation by the double emulsion technique 超声辅助乳化:用双乳液技术分析水体系中不同聚合物的微颗粒制备
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-09-08 DOI: 10.1016/j.ultsonch.2025.107555
Muhaimin Muhaimin , Anis Yohana Chaerunisaa , Roland Bodmeier
{"title":"Sonication-assisted emulsification: Analyzing different polymers in aqueous systems for microparticle preparation by the double emulsion technique","authors":"Muhaimin Muhaimin ,&nbsp;Anis Yohana Chaerunisaa ,&nbsp;Roland Bodmeier","doi":"10.1016/j.ultsonch.2025.107555","DOIUrl":"10.1016/j.ultsonch.2025.107555","url":null,"abstract":"<div><div>Sonication-assisted emulsification has emerged as a powerful technique for the preparation of microparticles in various fields, including pharmaceuticals, cosmetics, and food science. This study aims to investigate the impact of different polymers in an aqueous system on the preparation of microparticles by the double emulsion technique. By understanding the factors that affect emulsification and stability, we can optimize the production of microparticles with desired characteristics. This study discusses the mechanism behind sonication-assisted emulsification, the various polymers used, and the analysis of particle size, morphology, and stability. The microparticle were prepared with a water-in-oil-in-water (W/O/W) solvent evaporation method, for various polymers (including EC 4 cp, Eudragit® RS 100, Eudragit® RL 100, PLGA (RG503H) and PCL) that solvent used dichloromethane. The particle size/distribution of the emulsion droplets/hardened microparticles was monitored using FBRM. The morphology of polymeric microparticles was characterized using scanning electron microscopy (SEM). The transformation of the emulsion droplets into solid microparticles occured within the first 11.5, 20, 26, 30.5 and 56 min when EC 4 cp, Eudragit® RS 100, Eudragit® RL 100, PLGA (RG503H) and PCL were used respectively. The square weighted mean chord length of PCL microparticles was smallest, but the chord count was not the highest. The chord length distribution (CLD) measured by FBRM showed that a larger mean particle size gave longer CLD and a lower peak of particle number. SEM data revealed that the morphology of microparticles was influenced by the type of polymer. Sonicator helped in emulsification of polymeric system in aquous. FBRM can be employed for online monitoring of the shift in the microparticle CLD and detect transformation of emulsion droplets into solid microparticles during the solvent evaporation process. The microparticle CLD and transformation process were strongly influenced by polymer type.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"121 ","pages":"Article 107555"},"PeriodicalIF":9.7,"publicationDate":"2025-09-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145045617","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Optimization of astaxanthin extraction from red (Gracilaria corticata) and brown (Sargassum polycystum) macroalgae through ultrasonication and microwave processing 超声波和微波工艺优化红、褐大藻虾青素提取工艺
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-09-08 DOI: 10.1016/j.ultsonch.2025.107556
Parisa Feizi , Seid Mahdi Jafari
{"title":"Optimization of astaxanthin extraction from red (Gracilaria corticata) and brown (Sargassum polycystum) macroalgae through ultrasonication and microwave processing","authors":"Parisa Feizi ,&nbsp;Seid Mahdi Jafari","doi":"10.1016/j.ultsonch.2025.107556","DOIUrl":"10.1016/j.ultsonch.2025.107556","url":null,"abstract":"<div><div>This study aimed at optimizing the extraction of astaxanthin (ASX) by microwave- and ultrasound-assisted methods through an organic solvent (a mixture of ethanol and ethyl acetate), a green solvent (a microemulsion (MEL) of tributyloctylphosphonium bromide ionic liquid in water), and a vegetable oil (sunflower oil) from red (<em>Gracilaria corticate</em>/<em>GC</em>) and brown (<em>Sargassum polycystum</em>/<em>SP</em>) macroalgae. First, MELs were evaluated in terms of density, particle size and conductivity. Then, total carotenoids, ASX content, ASX extraction efficiency and DPPH scavenging activity were measured to evaluate the performance of different extraction methods. According to the results, the density of MEL was 0.97 g/cm<sup>3</sup>, its diameter was 15.80 nm and the conductivity was 312 µS/cm at 27.1 °C. Based on our findings, the optimal conditions for the extraction of ASX from <em>SP</em> and <em>GC</em> by sonication were the solvent to sample ratio of 20:1, power of 200 W and time of 30 min; for microwave processing, the solvent to sample ratio of 20:1, power of 100 W and time of 5 s. The results showed that in both methods, the ionic MEL solvent showed better performance in terms of ASX extraction, and <em>SP</em> resulted in more total carotenoids compared to <em>GC</em>. Microwave treatment was more effective for extracting ASX from brown algae due to its ability to rapidly disrupt cells from the inside, improve solute–solvent interactions, and overcome structural resistance of algal tissues more efficiently than sonication. Based on the results, red (<em>GC</em>) and brown (<em>SP</em>) macroalgae can be suggested as accessible and inexpensive sources for extracting valuable compounds such as bioactives and the natural pigment astaxanthin.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"121 ","pages":"Article 107556"},"PeriodicalIF":9.7,"publicationDate":"2025-09-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145045616","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of ultrasound pretreatment on the drying characteristics and quality of Tremella fuciformis under heat pump drying 超声预处理对银耳热泵干燥特性及品质的影响
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-09-07 DOI: 10.1016/j.ultsonch.2025.107553
Yuping Cao , Li Wu , Jinxuan Liu , Qing Xia , Wei Deng , Yunzhe Guo , Yibin Li
{"title":"Effect of ultrasound pretreatment on the drying characteristics and quality of Tremella fuciformis under heat pump drying","authors":"Yuping Cao ,&nbsp;Li Wu ,&nbsp;Jinxuan Liu ,&nbsp;Qing Xia ,&nbsp;Wei Deng ,&nbsp;Yunzhe Guo ,&nbsp;Yibin Li","doi":"10.1016/j.ultsonch.2025.107553","DOIUrl":"10.1016/j.ultsonch.2025.107553","url":null,"abstract":"<div><div>To enhance the heat pump drying (HPD) efficiency and quality of <em>Tremella fuciformis</em> (<em>T. fuciformis</em>), this study employed ultrasound pretreatment and evaluated its effects on drying behavior and product attributes at various ultrasound intensities [0.00 (the control group, CK), 0.20, 0.34, 0.54, and 0.74 W/g]. The results showed that ultrasound pretreatment significantly accelerated the drying process. The 0.34 W/g pretreatment group achieved the shortest drying time (855 min), which was 9.52% shorter than the CK group (945 min) (<em>p</em> &lt;0.05), and improved the rehydration rate by 7.25% (1220.50 ± 24.75%) compared to the CK group (1138.00 ± 1.41%) (<em>p</em> &lt;0.05). The polysaccharide content reached a maximum value of 24.80 ± 0.25 % at 0.54 W/g, which was 14.44% higher than that of the CK group (21.67 ± 0.26%) (<em>p</em> &lt;0.05). The chromatism remained stable. The microstructure and moisture migration analysis showed that ultrasound pretreatment promotes the formation of porous and loose microstructures in <em>T. fuciformis</em>, which homogenizes the spatial distribution of moisture inside the tissue and enhances moisture diffusion during the HPD process. However, the soluble protein content showed a reduction. Based on a comprehensive evaluation, ultrasound intensities of 0.34 ∼ 0.54 W/g are recommended as the optimal pretreatment range. This study provides theoretical guidance and practical data support for optimizing the drying process and promoting industrial application of <em>T</em>. <em>fuciformis</em>.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"121 ","pages":"Article 107553"},"PeriodicalIF":9.7,"publicationDate":"2025-09-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145026652","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Ultrasound-assisted extraction of naringin from Exocarpium Citri Grandis using a novel ternary natural deep eutectic solvent based on glycerol: Process optimization using ANN-GA, extraction mechanism and biological activity 基于甘油的新型三元天然深共熔溶剂超声辅助提取柑桔皮苷:ANN-GA工艺优化、提取机理及生物活性研究
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-09-07 DOI: 10.1016/j.ultsonch.2025.107551
Hailin Ran , Xuxiang Zhang , Jiafei Long , Zhijia Wang , Shengyi Zhuang , Xin Zhang , Yongmei Jiang , Jianyong Zhang , Gang Wang
{"title":"Ultrasound-assisted extraction of naringin from Exocarpium Citri Grandis using a novel ternary natural deep eutectic solvent based on glycerol: Process optimization using ANN-GA, extraction mechanism and biological activity","authors":"Hailin Ran ,&nbsp;Xuxiang Zhang ,&nbsp;Jiafei Long ,&nbsp;Zhijia Wang ,&nbsp;Shengyi Zhuang ,&nbsp;Xin Zhang ,&nbsp;Yongmei Jiang ,&nbsp;Jianyong Zhang ,&nbsp;Gang Wang","doi":"10.1016/j.ultsonch.2025.107551","DOIUrl":"10.1016/j.ultsonch.2025.107551","url":null,"abstract":"<div><div>This study aimed to develop an efficient green ultrasound-assisted extraction (UAE) method for naringin (Nar) from <em>Exocarpium Citri Grandis</em> (ECG) using a glycerol-based ternary natural deep eutectic solvent (NADES) and explore its biofunctional relevance. After screening and single-factor optimization, the optimal NADES was identified as glycerol:malic acid:propanedioic acid (1:1:2 M ratio, 30 % water content). Extraction conditions (liquid–solid ratio, temperature, time) were optimized via response surface methodology (RSM) and an artificial neural network-genetic algorithm (ANN-GA), with ANN-GA demonstrating superior predictive capability. Optimal parameters (57 °C, 25.9 mL/g, 24.4 min) yielded a high Nar extraction yield of 175.30 ± 2.94 mg/g. Scanning electron microscopy (SEM) revealed structural changes in ECG, while extraction kinetics indicated an activation energy of 40.45 kJ/mol and molecular dynamics simulations elucidated improved solvation mechanisms. NADES was reusable for at least three cycles before efficiency decreased significantly at the fourth reuse. Furthermore, the extracted Nar showed significant inhibitory activity against key enzymes, with IC<sub>50</sub> values of 19.6 μg/mL (α-glucosidase), 2.73 mg/mL (pancreatic lipase), and 1,086 μg/mL (acetylcholinesterase). These results indicate its potential for hypoglycemic, hypolipidemic, and anti-Alzheimer’s therapeutic effects. This work establishes a sustainable strategy for efficient Nar extraction, integrating green solvent technology with bioactivity assessment to advance its therapeutic potential.</div></div>","PeriodicalId":442,"journal":{"name":"Ultrasonics Sonochemistry","volume":"121 ","pages":"Article 107551"},"PeriodicalIF":9.7,"publicationDate":"2025-09-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145019361","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Comprehensive analysis of ultrasound-assisted electrohydrodynamic technology on drying characteristics, quality attributes, and volatile profiles of yam (Dioscorea opposita) 超声辅助电流体动力技术对山药干燥特性、品质属性及挥发性特征的综合分析
IF 9.7 1区 化学
Ultrasonics Sonochemistry Pub Date : 2025-09-06 DOI: 10.1016/j.ultsonch.2025.107548
Wurile Bai , Changjiang Ding , Jingli Lu , Chunxu Qin , Junyi Wang , Zhiqing Song , Chuanqiang Che , Hao Chen
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