Journal of Food Composition and Analysis最新文献

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Sensory directed analysis for key odor-active compounds in by-products flavorings enhanced by enzymatic hydrolysis and Maillard reaction
IF 4 2区 农林科学
Journal of Food Composition and Analysis Pub Date : 2025-03-15 DOI: 10.1016/j.jfca.2025.107487
Xiaomo Han , Xing Gao , Mingguang Yu , Rui Xu , Huanlu Song , Wenqing Pan , Wanying Chen , Wen Xiong , Li Yang , Zijian Huang
{"title":"Sensory directed analysis for key odor-active compounds in by-products flavorings enhanced by enzymatic hydrolysis and Maillard reaction","authors":"Xiaomo Han ,&nbsp;Xing Gao ,&nbsp;Mingguang Yu ,&nbsp;Rui Xu ,&nbsp;Huanlu Song ,&nbsp;Wenqing Pan ,&nbsp;Wanying Chen ,&nbsp;Wen Xiong ,&nbsp;Li Yang ,&nbsp;Zijian Huang","doi":"10.1016/j.jfca.2025.107487","DOIUrl":"10.1016/j.jfca.2025.107487","url":null,"abstract":"<div><div>This study explores the enhancement of chicken bone flavor through enzymatic hydrolysis and the Maillard reaction, providing insights into the formation and characterization of key aroma compounds. Chicken bone extract was hydrolyzed using Protamex™ and Flavourzyme™ to obtain chicken bone enzymatic hydrolysate (CBEE), which was subjected to the Maillard reaction to produce Maillard reaction chicken flavoring (MRCF). The volatile compounds in CBEE and MRCF were comprehensively analyzed using solvent-assisted flavor evaporation (SAFE) and solid-phase microextraction (SPME) combined with two-dimensional gas chromatography–olfactometry–mass spectrometry (GC×GC-O-MS). A total of 40 odor active compounds were identified and their odor activity values (OAV) were calculated. Among them, 11 compounds contributed significantly to the overall aroma (OAV ≥ 1). Key contributors, including 2-methyl-3-furanethiol, furaneol, 5-(2-hydroxyethyl)-4-methylthiazole, and maltol, were confirmed through aroma recombination and omission experiments. The results highlight that the Maillard reaction significantly enhances the richness and complexity of the meaty and roasted aromas, driven primarily by the increased levels of sulfur-containing and heterocyclic compounds. This research provides a scientific foundation for the industrial development of meat flavorings from chicken bone by-products and offers valuable guidance for flavor optimization.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"142 ","pages":"Article 107487"},"PeriodicalIF":4.0,"publicationDate":"2025-03-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143680274","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Heavy metal(loid)s contamination assessment in jhum soil-rice system, Arunachal Pradesh, Northeast India
IF 4 2区 农林科学
Journal of Food Composition and Analysis Pub Date : 2025-03-13 DOI: 10.1016/j.jfca.2025.107478
Sunitee Gohain Baruah, Mayuri Chabukdhara
{"title":"Heavy metal(loid)s contamination assessment in jhum soil-rice system, Arunachal Pradesh, Northeast India","authors":"Sunitee Gohain Baruah,&nbsp;Mayuri Chabukdhara","doi":"10.1016/j.jfca.2025.107478","DOIUrl":"10.1016/j.jfca.2025.107478","url":null,"abstract":"<div><div>The metal(loid)s accumulation in rice grain poses a significant global concern, particularly because rice is widely consumed food in the world. In this study, concentration of lead (Pb), cadmium (Cd), iron (Fe), nickel (Ni), and arsenic (As) was assessed in paddy soil and four different local rice varieties under Jhum Farming (JF) system in the then Lower Subansiri (now Keyi Panyor) district of Arunachal Pradesh, northeast India. Nemerow’s Pollution Index (PI<sub>N</sub>) in Jhum farming (JF) soils ranges from 0.9 to 1.9, with an average of 1.4, indicating 'clean' to 'slight' pollution. Except for two sites, others were classified as pollution-free based on PLI (Pollution Load index). The mean hazard quotient (HQ) for non-carcinogenic risks from heavy metals through rice intake was within safe limit (HQ&lt;1) for all local rice varieties (Amo, Baede, Lemeh and Riyu). Overall, no significant non-carcinogenic health risks due to studied metals including arsenic under traditional Jhum Farming (JF) system. Regular monitoring of heavy metal(loid)s in soil-rice system is important to ensure the safety of rice production and take suitable management options.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"142 ","pages":"Article 107478"},"PeriodicalIF":4.0,"publicationDate":"2025-03-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143628245","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Metabolomic profiling of novel muskmelon cultigens reveals regional variation in fruit composition across four U.S. growing locations
IF 4 2区 农林科学
Journal of Food Composition and Analysis Pub Date : 2025-03-13 DOI: 10.1016/j.jfca.2025.107470
Jashbir Singh , Rita Metrani , Deepak Kumar Jha , Kevin M. Crosby , John L. Jifon , Sadhana Ravishankar , Paul Brierley , Daniel I. Leskovar , Thomas A. Turini , Wenjing Guan , Devanand L. Luthria , Bhimanagouda S. Patil
{"title":"Metabolomic profiling of novel muskmelon cultigens reveals regional variation in fruit composition across four U.S. growing locations","authors":"Jashbir Singh ,&nbsp;Rita Metrani ,&nbsp;Deepak Kumar Jha ,&nbsp;Kevin M. Crosby ,&nbsp;John L. Jifon ,&nbsp;Sadhana Ravishankar ,&nbsp;Paul Brierley ,&nbsp;Daniel I. Leskovar ,&nbsp;Thomas A. Turini ,&nbsp;Wenjing Guan ,&nbsp;Devanand L. Luthria ,&nbsp;Bhimanagouda S. Patil","doi":"10.1016/j.jfca.2025.107470","DOIUrl":"10.1016/j.jfca.2025.107470","url":null,"abstract":"<div><div>Understanding the role of crop management, environmental conditions, and genotypes is critical for improving the yield and quality of agricultural products. Here, we evaluated the phytochemical compositions of eight newly developed muskmelon (<em>Cucumis melo</em>) cultigens grown at four locations (Texas, California, Arizona, and Indiana) in the United States. All the cultigens had total soluble solids contents higher than 10 °Brix, except for fruits grown in Indiana. The soluble sugars (glucose, fructose, and sucrose) among the samples averaged 22.6 %, 35.7 %, and 41.7 %, respectively. β-carotene was the prominent carotenoid, and its content ranged between 13.4 ± 1.1–37.6 ± 3.8 µg/g FW. Lower levels of colorless carotenoids phytoene and phytofluene were also quantified. The four most prominent amino acids were glutamine, glutamic acid, aspartic acid, and γ-aminobutyric acid, which were present in higher concentrations compared with other amino acids in all cultigens. A principal component analysis of studied quality attributes differentiated two muskmelon cultigens (TH1 and TH6) by growing location. This information will be important for researchers and breeders to develop better yield and quality of muskmelon.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"142 ","pages":"Article 107470"},"PeriodicalIF":4.0,"publicationDate":"2025-03-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143680870","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Isolation and characterization of novel umami peptides from dried-salted large yellow croaker (Larimichthys crocea) and molecular docking to the T1R1/T1R3 taste receptor
IF 4 2区 农林科学
Journal of Food Composition and Analysis Pub Date : 2025-03-13 DOI: 10.1016/j.jfca.2025.107484
Haoran Lv , Shanshan Jiang , Xiaoqi Liu , Chuandong Fang , Shucheng Liu , Chuan Li , Soottawat Benjakul , Huimin Lin , Bin Zhang
{"title":"Isolation and characterization of novel umami peptides from dried-salted large yellow croaker (Larimichthys crocea) and molecular docking to the T1R1/T1R3 taste receptor","authors":"Haoran Lv ,&nbsp;Shanshan Jiang ,&nbsp;Xiaoqi Liu ,&nbsp;Chuandong Fang ,&nbsp;Shucheng Liu ,&nbsp;Chuan Li ,&nbsp;Soottawat Benjakul ,&nbsp;Huimin Lin ,&nbsp;Bin Zhang","doi":"10.1016/j.jfca.2025.107484","DOIUrl":"10.1016/j.jfca.2025.107484","url":null,"abstract":"<div><div>This study aimed to extract umami peptides from East China dried-salted yellow croaker (<em>Larimichthys crocea</em>) and explore their flavor properties and binding mechanisms. Using ultrafiltration, gel column chromatography, and reverse-phase high-performance liquid chromatography, twelve peptide components were identified, with five selected for further analysis: Asp-Leu-Tyr-Glu (DLYE), Glu-Pro-Arg-His-Thr (EPRHT), Leu-Glu-Asn-Ser (LENS), Leu-Pro-Ile-Glu-Asp (LPIED), and Ser-Phe-Arg-Ala-Asn (SFRAN). Sensory evaluation confirmed that all five peptides enhanced freshness in taste. Computational analysis, including Modeller10.2 and ZDock, revealed a high-quality model of the T1R1/T1R3 receptor, with 97.7 % of the amino acid residues within the allowable range, thereby verifying model accuracy. Usually, T1R1 and T1R3 have different conformations, and the Venus flytrap domain (VFTD) in the cavity of T1R3 is beneficial for binding umami peptides. Key binding sites (Glu65, Arg393, and Gly389) were identified in the T1R1 subunit. These findings provide insight into the flavor characteristics and binding mechanisms of umami peptides from yellow croaker, offering a theoretical foundation for their application in flavor enhancement.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"142 ","pages":"Article 107484"},"PeriodicalIF":4.0,"publicationDate":"2025-03-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143680869","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Distribution and risk assessment of phthalate esters in different types of royal jelly products based on modified QuEChERS combined with GC-MS/MS
IF 4 2区 农林科学
Journal of Food Composition and Analysis Pub Date : 2025-03-13 DOI: 10.1016/j.jfca.2025.107473
Haitao Xu , Yuzhe Yuan , Guodong Mu , Sha Yan , Xiaofeng Xue
{"title":"Distribution and risk assessment of phthalate esters in different types of royal jelly products based on modified QuEChERS combined with GC-MS/MS","authors":"Haitao Xu ,&nbsp;Yuzhe Yuan ,&nbsp;Guodong Mu ,&nbsp;Sha Yan ,&nbsp;Xiaofeng Xue","doi":"10.1016/j.jfca.2025.107473","DOIUrl":"10.1016/j.jfca.2025.107473","url":null,"abstract":"<div><div>Phthalate esters (PAEs) are common environmental pollutants found in food samples, demanding accurate detection for risk assessment and remediation. In this study, a modified QuEChERS combined with GC-MS/MS was developed to detect phthalate esters (PAEs) in different types of royal jelly products. This newly developed method for fresh royal jelly exhibited excellent performance: it demonstrated a 2–500 µg/L linear range, 4.3–15.2 µg/kg limit of detection, 11.2–31.3 µg/kg limit of quantification, and 84.2 %–108.1 % recovery. Sample analysis disclosed the existence of di-(2-ehtylhexyl) phthalate (DEHP), di-n-butyl phthalate (DBP), diethyl phthalate (DEP), and dimethyl phthalate (DMP) in all three types of royal jelly products, and the detection rates of DBP and DEHP were 100 %. Higher levels of PAEs were present in processed royal jelly products (lyophilized royal jelly and royal jelly in capsule) than in fresh royal jelly samples. Given the restricted PAEs intake doses, royal jelly products are safe for human consumption. This work offers a novel perspective on controlling the quality of different types of royal jelly products.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"142 ","pages":"Article 107473"},"PeriodicalIF":4.0,"publicationDate":"2025-03-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143680871","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Analysis of microorganisms of rotting rose hips by high-throughput sequencing and MALDI-TOF-MS
IF 4 2区 农林科学
Journal of Food Composition and Analysis Pub Date : 2025-03-12 DOI: 10.1016/j.jfca.2025.107471
Ling-Li Meng , Chao Ma , Fu-Rong Wang , Ling-Xiao Liu , Gui-Zhi Dong , Yun-Guo Liu
{"title":"Analysis of microorganisms of rotting rose hips by high-throughput sequencing and MALDI-TOF-MS","authors":"Ling-Li Meng ,&nbsp;Chao Ma ,&nbsp;Fu-Rong Wang ,&nbsp;Ling-Xiao Liu ,&nbsp;Gui-Zhi Dong ,&nbsp;Yun-Guo Liu","doi":"10.1016/j.jfca.2025.107471","DOIUrl":"10.1016/j.jfca.2025.107471","url":null,"abstract":"<div><div>Rose hips (<em>Rosa rugosa</em>), a rich source of bioactive compounds such as phenols, carotenoids, and vitamins, are increasingly recognized for their nutritional and medicinal value. However, the high nutrient content and moisture levels in fresh rose hips make them highly susceptible to microbial spoilage, which significantly reduces their shelf life and increases food waste. Despite the importance of understanding the microbial communities responsible for spoilage, limited research has focused on this aspect of rose hip preservation. This study aims to bridge this gap by investigating the microbial communities involved in the spoilage of four varieties of Rosa rugosa from Pingyin, Shandong Province, using high-throughput sequencing, MALDI-TOF-MS, and gas chromatography-mass spectrometry (GC-MS) for microbial and volatile organic compound analysis. High-throughput sequencing of 16S rRNA and ITS genes identified a diverse microbial community consisting of both bacteria and fungi, including spoilage-associated species such as Bacillus, Pantoea, Rahnella, Alternaria, and Aspergillus. MALDI-TOF-MS further confirmed these findings, revealing a broader range of microbial species. GC-MS analysis of volatile organic compounds (VOCs) identified key spoilage-related compounds, such as alcohols, ketones, and esters, with correlations between specific VOCs and microbial populations. This study provides valuable insights into the microbial dynamics of rose hip spoilage and offers potential markers for spoilage detection. The integration of high-throughput sequencing, MALDI-TOF-MS, and GC-MS sets a new benchmark for food preservation research, enhancing our ability to monitor and control microbial contamination in fresh fruits.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"142 ","pages":"Article 107471"},"PeriodicalIF":4.0,"publicationDate":"2025-03-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143680868","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
A spray assisted droplet formation-liquid phase microextraction procedure for the quantification of trace levels of manganese in French Lavender Tea Infusions with flame atomic absorption spectrometry
IF 4 2区 农林科学
Journal of Food Composition and Analysis Pub Date : 2025-03-12 DOI: 10.1016/j.jfca.2025.107479
Melike Atakol , Vedat Yıldırım , Arda ATAKOL , Hilal Akbıyık , Buse Tuğba Zaman , Orhan Atakol , Sezgin Bakırdere
{"title":"A spray assisted droplet formation-liquid phase microextraction procedure for the quantification of trace levels of manganese in French Lavender Tea Infusions with flame atomic absorption spectrometry","authors":"Melike Atakol ,&nbsp;Vedat Yıldırım ,&nbsp;Arda ATAKOL ,&nbsp;Hilal Akbıyık ,&nbsp;Buse Tuğba Zaman ,&nbsp;Orhan Atakol ,&nbsp;Sezgin Bakırdere","doi":"10.1016/j.jfca.2025.107479","DOIUrl":"10.1016/j.jfca.2025.107479","url":null,"abstract":"<div><div>In this study, an easy and effective analytical preconcentration method for accurately measuring the trace levels of manganese in <em>Lavandula stoechas</em> tea infusions using flame atomic absorption spectrometry was developed. N,N′-bis(salicylidene)-2,2’-dimethyl-1,3-propanediamine was utilized as the complexing agent. The approach eliminated the need for a dispersing solvent by employing a basic spraying mechanism to form and distribute miniscule droplets of the extraction solvent. The effects of the experimental parameters that influence the extraction efficiency were carefully examined one at a time approach to acquire a well optimized procedure. The limits of detection and quantification of the system developed were found as 4.1 and 13.7 μg/L, respectively. A linear working range spanning from 10.0 to 500 μg/L was achieved. The accuracy and applicability of the proposed method were demonstrated in French lavender tea infusions by the percent recoveries ranging from 80 % to 117 % obtained by embracing the matrix matching calibration strategy.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"142 ","pages":"Article 107479"},"PeriodicalIF":4.0,"publicationDate":"2025-03-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143628249","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Exploring the power of advanced spectral imaging and multivariate analysis for distinguishing similar carrot cultivars
IF 4 2区 农林科学
Journal of Food Composition and Analysis Pub Date : 2025-03-12 DOI: 10.1016/j.jfca.2025.107456
Mulowayi Mutombo Arcel , Chen Long Bin , Zhen Hui Shen , Witness Joseph Nyimbo , Mark Bayo Turay , Shu He Zheng
{"title":"Exploring the power of advanced spectral imaging and multivariate analysis for distinguishing similar carrot cultivars","authors":"Mulowayi Mutombo Arcel ,&nbsp;Chen Long Bin ,&nbsp;Zhen Hui Shen ,&nbsp;Witness Joseph Nyimbo ,&nbsp;Mark Bayo Turay ,&nbsp;Shu He Zheng","doi":"10.1016/j.jfca.2025.107456","DOIUrl":"10.1016/j.jfca.2025.107456","url":null,"abstract":"<div><div>Carrots are a widely consumed vegetable around the world. They come in several varieties, each with their distinct quality traits. This study uses hyperspectral imaging to identify and predict soluble solids content (SSC) in three carrot cultivars using machine learning-based spectral analysis. After preprocessing the raw spectra, we constructed a partial least squares regression (PLSR) model to predict SSC using the preprocessed full spectra. iPLS and competitive adaptive reweighted sampling (CARS) methods were compared for variable selection. To differentiate carrots from three orchards, we developed four classification models: CARS-LDA, iPLS-LDA, iPLS-KNN, and CARS-KNN. Results indicated that both CARS-LDA and iPLS achieved effective wavelength selection for the Fuzhou A carrot cultivar, with the CARS-LDA model demonstrating the highest predictive capability, reflected by a relative prediction deviation (RPD) value of 2.72. In terms of accuracy, specificity, sensitivity, and precision, the CARS-KNN model was the best. This study underscores the potential of hyperspectral imaging coupled with machine learning methodologies to reliably predict and distinguish between various carrot cultivars, thereby contributing significantly to improvements in food safety and quality control standards in the agricultural sector.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"142 ","pages":"Article 107456"},"PeriodicalIF":4.0,"publicationDate":"2025-03-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143680280","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
High-performance liquid chromatography (HPLC) method for standardization and quantitative analysis of naringin in interspecific citrus hybrids
IF 4 2区 农林科学
Journal of Food Composition and Analysis Pub Date : 2025-03-11 DOI: 10.1016/j.jfca.2025.107467
Dhrumeshkumar Chavda , Nimisha Sharma , R M Sharma , Vandana Tripathy , Nilesh Joshi , Hatkari Vittal , Nirmal Kumar , A K Dubey
{"title":"High-performance liquid chromatography (HPLC) method for standardization and quantitative analysis of naringin in interspecific citrus hybrids","authors":"Dhrumeshkumar Chavda ,&nbsp;Nimisha Sharma ,&nbsp;R M Sharma ,&nbsp;Vandana Tripathy ,&nbsp;Nilesh Joshi ,&nbsp;Hatkari Vittal ,&nbsp;Nirmal Kumar ,&nbsp;A K Dubey","doi":"10.1016/j.jfca.2025.107467","DOIUrl":"10.1016/j.jfca.2025.107467","url":null,"abstract":"<div><div>Naringin is a prominent flavonoid found in various citrus fruits, widely recognized for its antibacterial, anti-inflammatory, and antioxidant properties, which contribute to its potential health benefits. This study aimed to develop and validate an HPLC-PDA method for quantifying naringin in juice from interspecific citrus hybrids, while also assessing the sensory attributes of the juice. Two reversed-phase high-performance chromatographic methods were developed for the simultaneous determination of naringin in the juice, utilizing both isocratic and gradient elution on a C18 column. The method was validated for naringin quantification, demonstrating a wide linear range, high accuracy and precision, low detection and quantification limits, and overall robustness. Consumer tests revealed significant variation in naringin content (0.1–44 mg/L) and sensory attributes (3–9 points on a hedonic scale) across the hybrids and parent varieties. Descriptive flavour analysis, conducted by a trained sensory panel, indicated that the six hybrids had good sensory quality along with optimal naringin levels. Principal component analysis (PCA) differentiated naringin content and sensory attributes, and a heatmap with hierarchical data analysis suggested that over 90 % heritability was observed for both traits.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"142 ","pages":"Article 107467"},"PeriodicalIF":4.0,"publicationDate":"2025-03-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143628246","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
A novel naphthol-malononitrile-based fluorescent dye capable of imaging amines in living cells and its polyvinyl alcohol film for real-time visual monitoring of fish freshness
IF 4 2区 农林科学
Journal of Food Composition and Analysis Pub Date : 2025-03-11 DOI: 10.1016/j.jfca.2025.107477
Yaxin Yang , Lina Hu , Yuan Yao , Keli Zhong , Xiaomei Yan , Lijun Tang
{"title":"A novel naphthol-malononitrile-based fluorescent dye capable of imaging amines in living cells and its polyvinyl alcohol film for real-time visual monitoring of fish freshness","authors":"Yaxin Yang ,&nbsp;Lina Hu ,&nbsp;Yuan Yao ,&nbsp;Keli Zhong ,&nbsp;Xiaomei Yan ,&nbsp;Lijun Tang","doi":"10.1016/j.jfca.2025.107477","DOIUrl":"10.1016/j.jfca.2025.107477","url":null,"abstract":"<div><div>The traditional evaluation method of fish freshness requires a tedious operation process and is time-consuming. In this work, a fluorescent probe <strong>HYM</strong> composition of 6-naphthol linked by vinyl with 2-(5, 5-dimethylcyclohex-2-en-1-ylidene) malononitrile was synthesized. <strong>HYM</strong> can respond with 10 amines by colorimetric and fluorescence channel in DMSO/H<sub>2</sub>O (4/6, v/v, pH=7. 4) solution. <strong>HYM</strong> exhibits an ultrafast response (3 s), a detection limit of 4.23 μM for putrescine, and can image n-propylamine in living cells. <strong>HYM</strong> can also be used as a fluorescent ink to develop invisible materials. In addition, a polyvinyl alcohol sensing film <strong>HYMPF</strong> loaded with <strong>HYM</strong> was developed. When the color of <strong>HYMPF</strong> changed from faint yellow to colorless, and the fluorescence of the film changed from light yellow to no fluorescence, it indicated the grade of fish changed from qualified to spoiled state. This sensing film evaluating fish freshness by colorimetric and fluorescence channels increases the accuracy of the results and makes it suitable for applications in the fields of food safety and intelligent packaging.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"142 ","pages":"Article 107477"},"PeriodicalIF":4.0,"publicationDate":"2025-03-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143680867","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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