Advanced Engineering Materials最新文献

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Antimicrobial Nano-Ag/Cu Composite Coatings on Pure Ti Implants by Magnetron Sputtering Following Pretreatment for Dental Applications 磁控溅射预处理纳米银/铜抗菌复合涂层在纯钛种植体上的应用
IF 3.4 3区 材料科学
Advanced Engineering Materials Pub Date : 2025-03-28 DOI: 10.1002/adem.202402437
Xun Ma, Leilei Yu, Peixu Cheng, Ping Liu, Sergey Karpushenkov, Jiannan Liu, Wei Li
{"title":"Antimicrobial Nano-Ag/Cu Composite Coatings on Pure Ti Implants by Magnetron Sputtering Following Pretreatment for Dental Applications","authors":"Xun Ma,&nbsp;Leilei Yu,&nbsp;Peixu Cheng,&nbsp;Ping Liu,&nbsp;Sergey Karpushenkov,&nbsp;Jiannan Liu,&nbsp;Wei Li","doi":"10.1002/adem.202402437","DOIUrl":"https://doi.org/10.1002/adem.202402437","url":null,"abstract":"<p>Pure Ti is widely utilized in dental implant applications due to its exceptional biocompatibility. However, its lack of antibacterial properties poses a limitation. To address this constraint, nanocomposite coatings with novel topographic microstructure and Ag, Cu nanoparticles are introduced onto the surface of pure Ti implants through sandblasting, acid etching, and hydrothermal treatment and magnetron sputtering. In addition, polished Ti substrates, Ti substrates subjected to sandblasting, acid etching, and hydrothermal treatment, as well as Ti samples individually magnetron sputtered with Ag and Cu, are fabricated and investigated. A systematic comparison between those samples is performed to investigate the influence of substrate surface microstructure and element composition on physicochemical characteristics and antibacterial performance of Ti implants. The results demonstrate that sandblasting, acid etching, and alkali heat treatment significantly enhance the surface roughness of pure Ti, thereby improving its wettability. Nano-Ag and nano-Cu particles are deposited via magnetron sputtering technology, resulting in excellent antibacterial properties. Compared to the single-layer coating, the nano-composite coating exhibited superior antibacterial activity despite releasing lower concentrations of Ag<sup>+</sup> and Cu<sup>2+</sup>. Therefore, nanocomposite Ag- and Cu-based coatings fabricated by sandblasting, acid etching, hydrothermal treatment, and magnetron sputtering, effectively enhance the antibacterial properties of Ti implants for dental applications.</p>","PeriodicalId":7275,"journal":{"name":"Advanced Engineering Materials","volume":"27 9","pages":""},"PeriodicalIF":3.4,"publicationDate":"2025-03-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143909623","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Superior Shock Resistance of Magnesium and Magnesium–Aluminum Alloys with Cerium Addition 添加铈的镁及镁铝合金具有优异的抗冲击性
IF 3.4 3区 材料科学
Advanced Engineering Materials Pub Date : 2025-03-28 DOI: 10.1002/adem.202402488
Maadhav Anand, Shreshtha Ranjan, Shubham Sisodia, Gopalan Jagadeesh, Satyam Suwas, Ankur Chauhan
{"title":"Superior Shock Resistance of Magnesium and Magnesium–Aluminum Alloys with Cerium Addition","authors":"Maadhav Anand,&nbsp;Shreshtha Ranjan,&nbsp;Shubham Sisodia,&nbsp;Gopalan Jagadeesh,&nbsp;Satyam Suwas,&nbsp;Ankur Chauhan","doi":"10.1002/adem.202402488","DOIUrl":"https://doi.org/10.1002/adem.202402488","url":null,"abstract":"<p>This study investigates the shock response of forged and annealed commercially pure magnesium (Cp<b>–</b>Mg) and its cerium (Ce)-alloyed variants (Mg<b>–</b>0.5Ce and Mg<b>–</b>3Al<b>–</b>0.5Ce). Shock loading is performed using a conventional shock tube setup at two pressure levels along the forging direction (FD). Under low-pressure conditions, all materials deform without fracturing, with Cp<b>–</b>Mg exhibiting the highest deflection. However, at higher pressure, Cp<b>–</b>Mg discs fracture, displaying brittle cleavage, whereas Mg<b>–</b>0.5Ce and Mg<b>–</b>3Al<b>–</b>0.5Ce absorb impact energy without failure due to their superior strength–ductility balance. Among the Ce-alloyed variants, Mg<b>–</b>3Al<b>–</b>0.5Ce demonstrates slightly better shock resistance, exhibiting lower deflection and effective strain. Shock loading does not alter the grain size but results in a high density of predominantly extension twins that complements slip activity in all materials, particularly at higher pressures and in Cp<b>–</b>Mg. Post-shock analysis reveals the greatest reduction in basal texture intensity in Cp<b>–</b>Mg, while Mg<b>–</b>0.5Ce and Mg<b>–</b>3Al<b>–</b>0.5Ce show a moderate decrease. This reduction is attributed to slip and twinning, with Cp<b>–</b>Mg displaying the highest twinning activity. Local misorientation analysis indicates strain localization and stress concentrations at twin–matrix interfaces. Overall, Mg<b>–</b>0.5Ce and Mg<b>–</b>3Al<b>–</b>0.5Ce exhibit superior shock resistance compared to Cp<b>–</b>Mg, owing to their higher toughness, lower twin density, and increased non-basal slip activity.</p>","PeriodicalId":7275,"journal":{"name":"Advanced Engineering Materials","volume":"27 9","pages":""},"PeriodicalIF":3.4,"publicationDate":"2025-03-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143909622","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
β-Ga4GeO8 Stability Under Extreme Conditions (up to 600 °C and 30 GPa) β-Ga4GeO8在极端条件下的稳定性(高达600°C和30 GPa)
IF 3.4 3区 材料科学
Advanced Engineering Materials Pub Date : 2025-03-26 DOI: 10.1002/adem.202402347
Anna V. Spivak, Tatiana V. Setkova, Ludmila A. Gorelova, Oleg S. Vereshchagin, Valentin N. Kovalev, Egor S. Zakharchenko, Sergey N. Britvin, Vladimir N. Bocharov
{"title":"β-Ga4GeO8 Stability Under Extreme Conditions (up to 600 °C and 30 GPa)","authors":"Anna V. Spivak,&nbsp;Tatiana V. Setkova,&nbsp;Ludmila A. Gorelova,&nbsp;Oleg S. Vereshchagin,&nbsp;Valentin N. Kovalev,&nbsp;Egor S. Zakharchenko,&nbsp;Sergey N. Britvin,&nbsp;Vladimir N. Bocharov","doi":"10.1002/adem.202402347","DOIUrl":"https://doi.org/10.1002/adem.202402347","url":null,"abstract":"<p>\u0000The Ga<sub>4</sub>GeO<sub>8</sub> compound has attracted sufficient attention as an advanced optical material and host matrix material for near-infrared phosphors. A complex study (scanning electron microscopy, energy dispersive X-Ray spectroscopy, powder X-Ray diffraction, lattice dynamics calculations, and Raman spectroscopy up to 600 °C and 30 GPa) is presented on the synthetic <i>β</i>-Ga<sub>4</sub>GeO<sub>8</sub> compound. The <i>β</i>-Ga<sub>4</sub>GeO<sub>8</sub> crystals (up to 200 μm in size) are synthesized under hydrothermal conditions (600/650 °C, 100 MPa) at temperatures sufficiently lower than previously reported. The unit cell parameters are: <i>a</i> = 8.2701(2), <i>b</i> = 8.2392(2), <i>c</i> = 9.0886(2) Å, <i>β</i> = 117.674(1)°, <i>V</i> = 548.45(2) Å<sup>3</sup>, space group <i>P</i>2<sub>1</sub>/<i>c</i>. The obtained structural data are used for the lattice dynamics calculations. The assignment of <i>A</i><sub>g</sub> and <i>B</i><sub>g</sub> bands (cm<sup>−1</sup>) in calculated and experimental non-polarized Raman spectra at the ambient conditions is carried out. No significant changes are observed in the Raman spectra up to ≈600 °C. <i>In situ</i> Raman spectroscopy indicates that the structural integrity of the material is well preserved up to ≈11 GPa. Thus, <i>β</i>-Ga<sub>4</sub>GeO<sub>8</sub> is stable at least up to ≈600 °C and ≈11 GPa, which may indicate its potential applications under extreme conditions.</p>","PeriodicalId":7275,"journal":{"name":"Advanced Engineering Materials","volume":"27 9","pages":""},"PeriodicalIF":3.4,"publicationDate":"2025-03-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143908882","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
The Atomic Segregation and Ordered Stacking Fault Phase Transformation Along the Superlattice Stacking Fault During Creep in a Novel Powder Metallurgy Ni-Based Superalloy 一种新型粉末冶金镍基高温合金蠕变过程中沿超晶格层错的原子偏析和有序层错相变
IF 3.4 3区 材料科学
Advanced Engineering Materials Pub Date : 2025-03-21 DOI: 10.1002/adem.202401530
Xinyu Li, Haopeng Zhang, Xiaokun Li, Jian Jia, Changsheng Liu, Jiantao Liu, Yiwen Zhang
{"title":"The Atomic Segregation and Ordered Stacking Fault Phase Transformation Along the Superlattice Stacking Fault During Creep in a Novel Powder Metallurgy Ni-Based Superalloy","authors":"Xinyu Li,&nbsp;Haopeng Zhang,&nbsp;Xiaokun Li,&nbsp;Jian Jia,&nbsp;Changsheng Liu,&nbsp;Jiantao Liu,&nbsp;Yiwen Zhang","doi":"10.1002/adem.202401530","DOIUrl":"https://doi.org/10.1002/adem.202401530","url":null,"abstract":"<p>Superlattice stacking faults (SSFs) in the γ′ precipitate of a novel powder metallurgy (PM) Ni-based superalloy after creep rupture at 760 °C/552 MPa are analyzed through atomic-level characterization. The results show that the Cottrell atmosphere formed by the segregation of γ formers Cr, Co, and Mo near the leading partial dislocation drives the extension of SSFs. Co, Cr, Mo, and W segregate along the superlattice intrinsic stacking fault and lead to the formation of the ordered stacking fault phase ε-D0<sub>19</sub>. Meanwhile, Co, Ti, W, and Nb segregate along the superlattice extrinsic stacking fault and promote the formation of the ordered phase η-D0<sub>24</sub>. In addition, the formation process diagram of the SSF with ordered phase under the aid of segregation is drawn. The transformation of the ordered stacking fault phase can be evaluated by the atomic ratios of Al over the stacking fault phase formers.</p>","PeriodicalId":7275,"journal":{"name":"Advanced Engineering Materials","volume":"27 9","pages":""},"PeriodicalIF":3.4,"publicationDate":"2025-03-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143909638","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effects of Preoxidation on Microstructure and Characteristics of Carbon/Carbon Composite–Ti3Al Joints Prepared by Transient Liquid Phase Diffusion Bonding 预氧化对瞬态液相扩散连接制备碳/碳复合材料- ti3al接头组织和性能的影响
IF 3.4 3区 材料科学
Advanced Engineering Materials Pub Date : 2025-03-20 DOI: 10.1002/adem.202401985
Jie Wang, Wanru Shen, Jin Yang, Yang Feng, Zhe Zhou, Yaoji Yin
{"title":"Effects of Preoxidation on Microstructure and Characteristics of Carbon/Carbon Composite–Ti3Al Joints Prepared by Transient Liquid Phase Diffusion Bonding","authors":"Jie Wang,&nbsp;Wanru Shen,&nbsp;Jin Yang,&nbsp;Yang Feng,&nbsp;Zhe Zhou,&nbsp;Yaoji Yin","doi":"10.1002/adem.202401985","DOIUrl":"https://doi.org/10.1002/adem.202401985","url":null,"abstract":"<p>In order to promote the molten metal penetration into the carbon/carbon (C/C) composite, a sequence of annular gaps is designed and prepared on the C/C surface. These gaps are created on the C/C surface under preoxidation conditions at 600–660 °C. The oxidized C/C composite is joined to Ti<sub>3</sub>Al via transient liquid phase (TLP) diffusion bonding at 880 °C with AgCuNiLi foil as an intermediate layer. The study investigates the effects of preoxidation temperature on the microstructure and characteristics of C/C composite and C/C–Ti<sub>3</sub>Al joints. The results show that a sequence of annular gaps with appropriate size can be established between the carbon fiber and pyrolytic carbon layer, while carbon fiber is barely oxidized after oxidation at 630 °C for 30 min. During the bonding process, the molten metal seeps through the C/C gaps, and a permeation layer composed of TiC, Ag (s, s), and C/C composite can be formed. The production of a permeation layer can enhance the bonding strength of the C/C–Ti<sub>3</sub>Al joint, and the maximum shear strength (42.12 MPa) of the joint can be 22% greater than the initial C/C–Ti<sub>3</sub>Al joint.</p>","PeriodicalId":7275,"journal":{"name":"Advanced Engineering Materials","volume":"27 9","pages":""},"PeriodicalIF":3.4,"publicationDate":"2025-03-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143909482","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Celebrating Excellence in Materials Science: Prof. Suryanarayana Challapalli 庆祝材料科学的卓越成就:Suryanarayana Challapalli教授
IF 3.4 3区 材料科学
Advanced Engineering Materials Pub Date : 2025-03-18 DOI: 10.1002/adem.202500288
Enrique J. Lavernia, B. S. Murty
{"title":"Celebrating Excellence in Materials Science: Prof. Suryanarayana Challapalli","authors":"Enrique J. Lavernia,&nbsp;B. S. Murty","doi":"10.1002/adem.202500288","DOIUrl":"https://doi.org/10.1002/adem.202500288","url":null,"abstract":"&lt;p&gt;On the occasion of Prof. Suryanarayana's 80th birthday, it is our profound honour to organize and dedicate this special issue to an esteemed colleague whose remarkable contributions have profoundly enriched our understanding of materials science and engineering. In the realm of materials science and engineering, few individuals have contributed as profoundly as Prof. Suryanarayana, Ph.D., FASM, FIMMM, FEMSI, FAPAS, FTAS. With an illustrious academic and research career, spanning decades, Prof. Suryanarayana continues to inspire the global scientific community as Professor Emeritus at the University of Central Florida.&lt;/p&gt;&lt;p&gt;Prof. Suryanarayana's educational journey is a testament to his dedication and intellect. Starting with a Bachelor of Science degree from Andhra University, where he graduated as the top student in his college, he advanced to earn a Bachelor of Engineering in Metallurgy from the Indian Institute of Science, Bangalore, with distinction. His academic achievements culminated in a Ph.D. in Metallurgical Engineering from Banaras Hindu University, India. His doctoral thesis, focusing on the constitution, structure and energetics of splat-cooled alloys, laid the foundation for a groundbreaking career in materials science.&lt;/p&gt;&lt;p&gt;Throughout his career, Prof. Suryanarayana has explored the frontiers of materials research, contributing extensively to the fields of nanomaterials and advanced materials processing. His primary research interests include synthesizing and characterizing nanomaterials, mechanical alloying, rapid solidification of metallic glasses and coatings for turbine materials. These pursuits have enriched the field and advanced technological applications in diverse industries.&lt;/p&gt;&lt;p&gt;Beyond research, Prof. Suryanarayana has been a dedicated educator, shaping the minds of countless students and professionals in materials science. At the University of Central Florida, he taught an impressive range of graduate and undergraduate courses, including advanced topics such as “Nanostructured Materials,” “Phase Transformations in Metals and Alloys,” and “X-Ray Diffraction and Crystallography.” His undergraduate courses included critical areas like “Emerging Materials” and “Structure and Properties of Materials.” Prof. Surynarayana also played a pivotal role in modernizing the undergraduate materials laboratory by securing funding for essential equipment and enhancing hands-on learning experiences for students.&lt;/p&gt;&lt;p&gt;Prof. Surynarayana's impact extended beyond the classroom. Recognizing the need for specialized resources in graduate-level teaching and research, he authored and edited several key textbooks, including &lt;i&gt;Experimental Techniques in Materials and Mechanics&lt;/i&gt; and &lt;i&gt;X-Ray Diffraction: A Practical Approach&lt;/i&gt;. These works have become invaluable references for both students and professionals in the field, underscoring his commitment to advancing education in materials science.&lt;/p&gt;&lt;p&gt;Prof. Surynarayana's influence is n","PeriodicalId":7275,"journal":{"name":"Advanced Engineering Materials","volume":"27 6","pages":""},"PeriodicalIF":3.4,"publicationDate":"2025-03-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://onlinelibrary.wiley.com/doi/epdf/10.1002/adem.202500288","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143646062","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Principles and Mechanisms of Cryomilling of Metallic Materials: Insights from Recent Studies 金属材料低温铣削的原理和机理:最新研究的见解
IF 3.4 3区 材料科学
Advanced Engineering Materials Pub Date : 2025-03-18 DOI: 10.1002/adem.202570017
Felipe Gutierrez-Morales, Enrique J. Lavernia
{"title":"Principles and Mechanisms of Cryomilling of Metallic Materials: Insights from Recent Studies","authors":"Felipe Gutierrez-Morales,&nbsp;Enrique J. Lavernia","doi":"10.1002/adem.202570017","DOIUrl":"https://doi.org/10.1002/adem.202570017","url":null,"abstract":"<p><b>Cryomilling</b>\u0000 </p><p>Materials with improved properties and functionalities are increasingly essential across various industries. In article number 2402172, Enrique J. Lavernia and Felipe Gutierrez-Morales discuss cryomilling, a top-down technique for producing nanomaterials by pulverizing powder materials within a cryogenic environment that impedes dislocation recovery and promotes grain stability. This process minimizes contamination and achieves finer particles compared to room temperature mechanical alloying.\u0000 <figure>\u0000 <div><picture>\u0000 <source></source></picture><p></p>\u0000 </div>\u0000 </figure></p>","PeriodicalId":7275,"journal":{"name":"Advanced Engineering Materials","volume":"27 6","pages":""},"PeriodicalIF":3.4,"publicationDate":"2025-03-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://onlinelibrary.wiley.com/doi/epdf/10.1002/adem.202570017","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143645999","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Dynamic Deformation Mechanisms and Mechanical Properties of Additively Manufactured Closed-Cell Foams of Various Topologies 增材制造不同拓扑结构闭孔泡沫的动态变形机理和力学性能
IF 3.4 3区 材料科学
Advanced Engineering Materials Pub Date : 2025-03-17 DOI: 10.1002/adem.202401892
Md Abdul Kader, Md Abdul Wares, Md Ashraful Islam, Paul Jonathan Hazell, Juan Pablo Escobedo, Mohammad Saadatfar
{"title":"Dynamic Deformation Mechanisms and Mechanical Properties of Additively Manufactured Closed-Cell Foams of Various Topologies","authors":"Md Abdul Kader,&nbsp;Md Abdul Wares,&nbsp;Md Ashraful Islam,&nbsp;Paul Jonathan Hazell,&nbsp;Juan Pablo Escobedo,&nbsp;Mohammad Saadatfar","doi":"10.1002/adem.202401892","DOIUrl":"https://doi.org/10.1002/adem.202401892","url":null,"abstract":"<p>Closed-cell foams are widely used in energy absorption and load-bearing applications. Herein, four lightweight closed-cell foam topologies—tetrakaidecahedron, octet, spherical, and reverse hexagonal—are designed, manufactured, and mechanically tested. The structures are fabricated from acrylonitrile butadiene styrene using fused deposition modeling and subjected to low-velocity impact to investigate their elastic, plastic, and energy absorption behavior under dynamic loading. Deformation mechanisms are investigated to explore the role of topological architectures on mechanical response. Among the structures, the reverse hexagonal topology exhibits the highest yield strength and elastic stiffness, making it suitable for load-bearing applications. However, it demonstrates poor energy absorption due to its inability to utilize joints as plastic hinges during impact. In contrast, the octet structure exhibits superior energy absorption through a layer-by-layer collapse mechanism but offers limited elastic properties. The formation of shear bands in tetrakaidecahedron structure leads to midrange elastic properties. The spherical structure, however, shows poor energy absorption due to its unsystematic deformation and cell-wall distortion. The tetrakaidecahedron foam shows increased strength but reduced energy absorption during impact compared to quasi-static compression. These findings highlight the importance of considering dynamic mechanical properties when designing structures for impact-prone applications throughout their service life.</p>","PeriodicalId":7275,"journal":{"name":"Advanced Engineering Materials","volume":"27 9","pages":""},"PeriodicalIF":3.4,"publicationDate":"2025-03-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143909459","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
High Repetition Rate Laser-Induced Printing of Bioink with Picosecond Pulse Durations: Optimization of the Printing Process 皮秒脉冲高重复率激光诱导生物墨水打印:打印工艺的优化
IF 3.4 3区 材料科学
Advanced Engineering Materials Pub Date : 2025-03-17 DOI: 10.1002/adem.202402478
Lucas Duvert, Adrien Casanova, Ahmed Al-Kattan, Stefano Testa, Frédérique Magdinier, Anne-Patricia Alloncle
{"title":"High Repetition Rate Laser-Induced Printing of Bioink with Picosecond Pulse Durations: Optimization of the Printing Process","authors":"Lucas Duvert,&nbsp;Adrien Casanova,&nbsp;Ahmed Al-Kattan,&nbsp;Stefano Testa,&nbsp;Frédérique Magdinier,&nbsp;Anne-Patricia Alloncle","doi":"10.1002/adem.202402478","DOIUrl":"https://doi.org/10.1002/adem.202402478","url":null,"abstract":"<p>It has been more than two decades since laser-induced forward transfer (LIFT) was studied on a laboratory scale for its ability to print biomaterials. Most of the published works in this field are focused on the use of nanosecond lasers. Our final objective is to use the LIFT technique in a picosecond regime to create in vitro biomodels for tissue engineering and regenerative medicine applications. But in a first approach, the work presented here focuses on hydrodynamics and rheological studies for the optimization of the process for bioapplications. In order to precisely control the amount and position of the deposited material, it is necessary to carefully investigate the jetting dynamics as a function of various parameters, including the laser fluence and the rheological properties of the bioink. In this study, time-resolved fast imaging is used to investigate the hydrodynamics of the transfer of successive jets at a high pulse repetition rate. Different conditions have been determined (bioink viscosity, specific jetting dynamic associated with a precise distance for printing, and laser parameters) for precise control of the quantity of ink and number of cells deposited per droplet associated with high accuracy on their location and good reproducibility of the printing process.</p>","PeriodicalId":7275,"journal":{"name":"Advanced Engineering Materials","volume":"27 9","pages":""},"PeriodicalIF":3.4,"publicationDate":"2025-03-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://onlinelibrary.wiley.com/doi/epdf/10.1002/adem.202402478","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143909461","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Fly Ash, TiO2, hBN, and B4C Nanoparticle Reinforcement: A Novel Approach to Magnesium Metal via Powder Metallurgy 粉煤灰、TiO2、hBN和B4C纳米颗粒增强:粉末冶金制备金属镁的新方法
IF 3.4 3区 材料科学
Advanced Engineering Materials Pub Date : 2025-03-17 DOI: 10.1002/adem.202402261
Essam B. Moustafa, Abdulraheem H. Alyoubi, Mahmoud A. Alzahrani, Ahmed O. Mosleh, Asmaa M. Khalil
{"title":"Fly Ash, TiO2, hBN, and B4C Nanoparticle Reinforcement: A Novel Approach to Magnesium Metal via Powder Metallurgy","authors":"Essam B. Moustafa,&nbsp;Abdulraheem H. Alyoubi,&nbsp;Mahmoud A. Alzahrani,&nbsp;Ahmed O. Mosleh,&nbsp;Asmaa M. Khalil","doi":"10.1002/adem.202402261","DOIUrl":"https://doi.org/10.1002/adem.202402261","url":null,"abstract":"<p>\u0000The study explores the impact of fly ash and nanoparticle reinforcements (TiO<sub>2</sub>, hBN, B<sub>4</sub>C) on magnesium alloy properties. Fly ash increases porosity and reduces density. All reinforcements reduce conductivity, and B<sub>4</sub>C significantly decrease thermal expansion. This decrease is attributed to the particles' barrier effect, lower CTEs, and ability to promote uniform particle dispersion. The distribution of reinforcing particles varies, with B<sub>4</sub>C and hBN showing the most even dispersion. All reinforcements improve particle homogeneity, enhancing microhardness, with B<sub>4</sub>C exhibiting the most significant enhancement of 72%. All composite materials show increased compression strength, with B<sub>4</sub>C showing the most significant improvement of over 50%. The Mg hybrid composites display higher longitudinal and shear velocities than pure Mg. B<sub>4</sub>C shows the most substantial increase, with a 30% rise in longitudinal velocity and a 22% increase in shear velocity. Moreover, all composite materials exhibit larger Young's and shear moduli than pure Mg. B<sub>4</sub>C demonstrates the most notable enhancement, with a 50% increase in Young's modulus and a 45% increase in shear modulus. These enhancements result from the composites' heightened rigidity and decreased mass caused by the reinforcements, further amplified by the optimized spatial distribution of particles.</p>","PeriodicalId":7275,"journal":{"name":"Advanced Engineering Materials","volume":"27 9","pages":""},"PeriodicalIF":3.4,"publicationDate":"2025-03-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143909460","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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