Journal of Materials Science: Materials in Electronics最新文献

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Influence of BaTiO3 substitution on structural and thermal response of lead borosilicate glass for ultrasonic applications 取代 BaTiO3 对超声波应用硼硅酸铅玻璃结构和热响应的影响
IF 2.8 4区 工程技术
Journal of Materials Science: Materials in Electronics Pub Date : 2024-08-07 DOI: 10.1007/s10854-024-13246-4
M. Salah, El Sayed Moustafa, A. A. Showahy
{"title":"Influence of BaTiO3 substitution on structural and thermal response of lead borosilicate glass for ultrasonic applications","authors":"M. Salah, El Sayed Moustafa, A. A. Showahy","doi":"10.1007/s10854-024-13246-4","DOIUrl":"https://doi.org/10.1007/s10854-024-13246-4","url":null,"abstract":"<p>An extensive examination of the impact of BaTiO<sub>3</sub> doping on the mechanical and thermal characteristics of lead-borosilicate glasses is provided in this work. The glass density increases noticeably (from 6020 for BaTiO<sub>3</sub> to 2533 kg/m<sup>3</sup> for SiO<sub>2</sub>), and the molar volume decreases, suggesting a denser and more compact structural arrangement. The mechanical properties exhibited a notable improvement upon the addition of BaTiO<sub>3</sub>. Specifically, the longitudinal ultrasonic velocity (<i>V</i><sub><i>L</i></sub>) increased from 3927 to 4458 m/s, and the shear velocity (<i>V</i><sub><i>S</i></sub>) increased from 2317 to 2630 m/s, indicating a reinforced glass network. The bulk modulus increased from 35.71 to 58.06 GPa, and Young’s modulus increased from 57.2 to 92.98 GPa. These significant increases in elastic moduli were attributed to tighter atom packing and higher levels of cross-linking within the glass matrix. Furthermore, the glass structure’s increased rigidity and connectedness were further indicated by the Debye temperature (<i>θ</i><sub><i>D</i></sub>), which increased from 296.8 to 347.3 K. The influence of BaTiO<sub>3</sub> on the thermal analysis is demonstrated, which revealed that increasing BaTiO<sub>3</sub> content raises both the glass transition and crystallization temperatures. The results of the experiment demonstrate how much BaTiO<sub>3</sub> doping can improve the physical characteristics of lead-borosilicate glasses, enabling them to be used in sophisticated optical and structural applications.</p>","PeriodicalId":646,"journal":{"name":"Journal of Materials Science: Materials in Electronics","volume":null,"pages":null},"PeriodicalIF":2.8,"publicationDate":"2024-08-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141935065","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Development of the BiVO4/ZnFe2O4 heterostructure for solar water splitting 开发用于太阳能水分离的 BiVO4/ZnFe2O4 异质结构
IF 2.8 4区 工程技术
Journal of Materials Science: Materials in Electronics Pub Date : 2024-08-07 DOI: 10.1007/s10854-024-13315-8
R. M. Sánchez-Albores, Odín Reyes-Vallejo, F. Pola-Albores, A. Fernández-Madrigal, Andrés López-López, E. Ríos-Valdovinos
{"title":"Development of the BiVO4/ZnFe2O4 heterostructure for solar water splitting","authors":"R. M. Sánchez-Albores, Odín Reyes-Vallejo, F. Pola-Albores, A. Fernández-Madrigal, Andrés López-López, E. Ríos-Valdovinos","doi":"10.1007/s10854-024-13315-8","DOIUrl":"https://doi.org/10.1007/s10854-024-13315-8","url":null,"abstract":"<p>In this study, we report the development of a BiVO<sub>4</sub>/ZnFe<sub>2</sub>O<sub>4</sub> heterostructure and its characterization as a photoanode in solar water splitting. ZnFe<sub>2</sub>O<sub>4</sub> was deposited on a BiVO<sub>4</sub> thin film after electrodepositing varying charges of FeOOH (50, 100, and 250 mC), which were then thermally oxidized in the presence of air and a zinc source. Structural characterization via XRD and profilometry indicated an increase in film thickness with higher deposited charges. The analysis revealed a decrease in strain and Urbach energy, indicative of reduced structural defects and an increase in the bandgap. SEM images illustrated the porous nature of the film surfaces, with elongated 2D structures enhancing light absorption through multiple reflectance effects. However, increased charge deposition led to particle agglomeration, reducing light absorption efficiency and active surface area, thus diminishing photogenerated charge generation. Electrochemical and photoelectrochemical characterization confirmed the n-type nature of all films, with carrier concentration increasing with film thickness. Nevertheless, the thinnest film (50 mC) exhibited the highest photocurrent, attributed to reduced particle agglomeration, enhanced light absorption, greater charge transport capacity, and superior electrocatalytic behavior, thereby minimizing recombination effects. Overall, the heterostructure demonstrated suitability as a photoanode for oxygen evolution reaction, supported by correct band alignment as determined from flat band potentials.</p>","PeriodicalId":646,"journal":{"name":"Journal of Materials Science: Materials in Electronics","volume":null,"pages":null},"PeriodicalIF":2.8,"publicationDate":"2024-08-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141935054","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Influence of annealing on the optoelectronic properties of sprayed p-NiO/n-CdS 退火对喷涂 p-NiO/n-CdS 光电特性的影响
IF 2.8 4区 工程技术
Journal of Materials Science: Materials in Electronics Pub Date : 2024-08-07 DOI: 10.1007/s10854-024-13259-z
Mohammed Hamid Mustafa, Hiba M. Ali, Nadir F. Habubi, B. H. Hussein
{"title":"Influence of annealing on the optoelectronic properties of sprayed p-NiO/n-CdS","authors":"Mohammed Hamid Mustafa, Hiba M. Ali, Nadir F. Habubi, B. H. Hussein","doi":"10.1007/s10854-024-13259-z","DOIUrl":"https://doi.org/10.1007/s10854-024-13259-z","url":null,"abstract":"<p>The chemical spray pyrolysis was utilized to deposit nickel oxide with a thickness of 250 nm on both glass and FTO substrates. Its characteristics were examined at a range of annealing temperatures, including 523, 623, and 723 K for one hour. Based on X-ray diffraction tests, The X-ray pattern data indicated that nickel oxide had a cubic polycrystalline structure with a favored orientation (012). The films have very smooth surfaces, and nanoscale structures were revealed using atomic force microscope measurements. Field-emission scanning electron microscope shows roughly spherical-shaped particles with granulation and an agglomeration tendency with uniformly dispersed size morphology for the deposited films. The deposited films’ transmittance spectrum of wavelengths between 400 and 1100 nm was included in the investigation of optical characteristics. The lowered absorption spectrum rate leads to the optical spectrum’s bandgap (300–700 nm) rise by (3.21,3.28,3.31,3.35) eV. Analysis of the current–voltage characteristics of heterojunctions fabricated at various annealing temperatures showed an increase in the conversion efficiency of the optoelectronic devices from 1.9 to 3.8% as the annealing temperature increased to 723 K.</p>","PeriodicalId":646,"journal":{"name":"Journal of Materials Science: Materials in Electronics","volume":null,"pages":null},"PeriodicalIF":2.8,"publicationDate":"2024-08-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141935066","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Electrochromic performance of Pt-embedded porous alumina thick films via interface engineering with low-temperature volatile organic compound based gas sensors 通过与基于低温挥发性有机化合物的气体传感器的界面工程实现铂嵌入多孔氧化铝厚膜的电致变色性能
IF 2.8 4区 工程技术
Journal of Materials Science: Materials in Electronics Pub Date : 2024-08-07 DOI: 10.1007/s10854-024-13260-6
Baliram Nadekar, Chandrakant Ghuge, Yogesh Khollam, Kiran Sonawane, Mohd Abul Kalam, Sanjay Gadakh, Vijay Pawar, Shoyebmohamad F. Shaikh, Pravin S. More
{"title":"Electrochromic performance of Pt-embedded porous alumina thick films via interface engineering with low-temperature volatile organic compound based gas sensors","authors":"Baliram Nadekar, Chandrakant Ghuge, Yogesh Khollam, Kiran Sonawane, Mohd Abul Kalam, Sanjay Gadakh, Vijay Pawar, Shoyebmohamad F. Shaikh, Pravin S. More","doi":"10.1007/s10854-024-13260-6","DOIUrl":"https://doi.org/10.1007/s10854-024-13260-6","url":null,"abstract":"<p>Low-temperature volatile gas sensors are essential tools for many different applications, such as industrial safety and environmental monitoring. The low-temperature volatile gas sensor based on porous alumina thick films embedded with platinum (Pt) is demonstrated in this study. The thick layers of porous alumina on the aluminum substrates were produced by an electrochemical anodization process that was done in the dark. The semitransparent Pt coatings were deposited using the simple chemical bath deposition method to an anodized porous alumina sample. The films were characterized using both scanning electron microscopy (SEM) and energy-dispersive X-ray analysis (EDAX). The EDAX studies’ findings demonstrated the formation of a pure Pt phase and validated the purity of the Pt-embedded porous alumina films. A static gas-sensing system was used to measure the maximum sensitivity factor for methanol (5.5 × 10<sup>5</sup>), ethanol (4.5 × 10<sup>5</sup>), and acetone (~950) at the optimal operating temperature of 40 °C and carbon dioxide (~250) at the optimal operating temperature of 80 °C, respectively, using Pt-embedded porous alumina film at 1000 ppm. In addition, our synthesized Pt-embedded porous alumina film demonstrates constant cyclic repeatability. The results of this work indicate that Pt-embedded porous alumina films have a great deal of potential for use in a wide range of gas-sensing applications in various domains.</p>","PeriodicalId":646,"journal":{"name":"Journal of Materials Science: Materials in Electronics","volume":null,"pages":null},"PeriodicalIF":2.8,"publicationDate":"2024-08-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141935052","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Feasibility and performance of TiCN-based patch antennas for microwave antenna applications 微波天线应用中基于 TiCN 的贴片天线的可行性和性能
IF 2.8 4区 工程技术
Journal of Materials Science: Materials in Electronics Pub Date : 2024-08-06 DOI: 10.1007/s10854-024-13283-z
M. A. Jusoh, N. I. E. Pamin, N. I. Z. Azman, R. Nazlan, S. A. Harun
{"title":"Feasibility and performance of TiCN-based patch antennas for microwave antenna applications","authors":"M. A. Jusoh, N. I. E. Pamin, N. I. Z. Azman, R. Nazlan, S. A. Harun","doi":"10.1007/s10854-024-13283-z","DOIUrl":"https://doi.org/10.1007/s10854-024-13283-z","url":null,"abstract":"<p>Titanium Carbonitride (TiCN) offers a wide range of advantages due to its distinctive characteristics. This study investigates the feasibility of utilizing TiCN for microwave antenna applications. This paper describes the whole process, starting with the synthesizing of materials until the fabricating and testing of TiCN-based patch antenna. The TiCN paste was prepared using a hydrothermal method, and its crystallinity was analyzed using X-ray diffraction. The functional group of the TiCN paste was determined through FTIR analysis, while the morphology of the paste was examined using FESEM/EDX. The TiCN paste was applied onto an RT duroid 5880 substrate using screen-printing techniques, resulting in a strong bond between the paste and substrate as confirmed by the adhesion test. The antenna’s performance was evaluated using the Vector Network Analyzer, revealing two resonant frequencies at 9.08 GHz and 16.96 GHz. The return loss values for these frequencies are − 12.10 dB and − 16.25 dB, respectively. A calculated bandwidth of 950 MHz at − 10.00 dB was found for resonant frequency of 16.96 GHz. This performance indicates the promise of TiCN-based patch antennas for wireless communication technologies.</p>","PeriodicalId":646,"journal":{"name":"Journal of Materials Science: Materials in Electronics","volume":null,"pages":null},"PeriodicalIF":2.8,"publicationDate":"2024-08-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141935063","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Evaluation of the effect of low additive V2O5/ZnO on the structural, physical, and radiation attenuation performance of borate glasses 评估低添加剂 V2O5/ZnO 对硼酸盐玻璃的结构、物理和辐射衰减性能的影响
IF 2.8 4区 工程技术
Journal of Materials Science: Materials in Electronics Pub Date : 2024-08-06 DOI: 10.1007/s10854-024-13244-6
Islam M. Nabil, Ahmed T. Mosleh, Fawaz F. Alqahtani, Ahmad S. Alzoubi, Mohammed S. Alqahtani, H. Y. Zahran, I. S. Yahia, El Sayed Yousef, Rehab M. El-Sharkawy
{"title":"Evaluation of the effect of low additive V2O5/ZnO on the structural, physical, and radiation attenuation performance of borate glasses","authors":"Islam M. Nabil, Ahmed T. Mosleh, Fawaz F. Alqahtani, Ahmad S. Alzoubi, Mohammed S. Alqahtani, H. Y. Zahran, I. S. Yahia, El Sayed Yousef, Rehab M. El-Sharkawy","doi":"10.1007/s10854-024-13244-6","DOIUrl":"https://doi.org/10.1007/s10854-024-13244-6","url":null,"abstract":"<p>In this work, new glass systems with composition <i>x</i>V<sub>2</sub>O<sub>5</sub>–20CuO–60B<sub>2</sub>O<sub>3</sub>–15CaO–(5−<i>x</i>)ZnO which is coded as BCuCa–(5−<i>x</i>)Zn:xV where (0, 1, 2.5 mol.%) were fabricated using the melt-quenching technique with melting temperature 1200 °C to serve as competitive candidates for γ-ray and neutron shielding. XRD and FT-IR were used to characterize the assembled glass samples. The density values of synthesized glasses were increased almost linearly from 2.807 to 2.834 g cm<sup>−3</sup>, whereas molar volume decreased from 54.894 to 54.174 cm<sup>3</sup> mol<sup>−1</sup>, depending on the addition of V<sub>2</sub>O<sub>5</sub>. The γ-ray shielding properties of the prepared glass samples were tested experimentally using P-type HPGe detector in the photon energy range of 0.356–1.332 MeV and theoretically with the help of Monte Carlo (MC) simulations and Phy-X/PSD software in the photon energy range of 0.015–15 MeV. Various nuclear radiation shielding parameters such as linear attenuation coefficient (<i>µ</i>), half value layer (HVL), tenth value layer (TVL), mean free path (MFP), effective atomic number (Z<sub>eff</sub>), radiation protection efficiency (RPE), and fast neutron removal cross-section (FNRCS) for the prepared glasses have been evaluated at the selected range of photon energies. The experimental data of <i>μ</i> for all the tested glass systems is comparable to that obtained from a theoretical calculation. Also, Monte Carlo calculations were in a fairly good agreement with the Phy-X/PSD data, so that the maximum difference between them was about 2.716%. The outlined results indicated that the glass sample with 2.5-mol % V<sub>2</sub>O<sub>5</sub> (BCuCa–2.5Zn:2.5V) exhibits optimal <i>µ</i>, Z<sub>eff</sub>, HVL, TVL, and MFP values. BCuCa–2.5Zn:2.5V was also found to have the best value of the FNRCS (about 0.1 cm<sup>−1</sup>).</p>","PeriodicalId":646,"journal":{"name":"Journal of Materials Science: Materials in Electronics","volume":null,"pages":null},"PeriodicalIF":2.8,"publicationDate":"2024-08-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141935246","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Structural, magnetic, electrical, and magneto-conductivity of LiZCdYZnXNi1−(X+Y+Z)Fe2O4 cathode materials for energy storage device applications 用于储能设备应用的 LiZCdYZnXNi1-(X+Y+Z)Fe2O4 阴极材料的结构、磁性、电性和磁导率
IF 2.8 4区 工程技术
Journal of Materials Science: Materials in Electronics Pub Date : 2024-08-06 DOI: 10.1007/s10854-024-13234-8
N. R. Rethi, J. Johnson, R. Sankaranarayanan
{"title":"Structural, magnetic, electrical, and magneto-conductivity of LiZCdYZnXNi1−(X+Y+Z)Fe2O4 cathode materials for energy storage device applications","authors":"N. R. Rethi, J. Johnson, R. Sankaranarayanan","doi":"10.1007/s10854-024-13234-8","DOIUrl":"https://doi.org/10.1007/s10854-024-13234-8","url":null,"abstract":"<p>Herein, Li, Cd and Zn substituted spinel nickel ferrites Li<sub><i>Z</i></sub>Cd<sub><i>Y</i></sub>Zn<sub><i>X</i></sub>Ni<sub>1−(<i>X+Y+Z</i>)</sub>Fe<sub>2</sub>O<sub>4</sub> with different (<i>x</i> + <i>y</i> + <i>z</i> = 0.15, 0.3, 0.45, 0.6 and 0.75) compositions were fabricated by using sol–gel method followed by sintering treatment at 1050 °C. Single-phase cubic spinel structure of nickel ferrite compound was identified through X-ray diffraction analysis. The replacement of Cd<sup>2+</sup>, Zn<sup>2+</sup> and Ni<sup>2+</sup> cations toward tetrahedral A-site and Li<sup>+</sup> and Fe<sup>3+</sup> ions over octahedral B-site. From the variations in lattice parameter (8.3399–8.4380 Å), crystallite size (94.32–69.92 nm) and ionic jump length (3.611–3.653 Å), considerable enhancement in saturation magnetization (39.38–58.65 emu/g) at room temperature was obtained in the ferrimagnetic nanocomposite with increase in Li<sup>+</sup>, Cd<sup>2+</sup>, and Zn<sup>2+</sup> ion concentrations. The electrical responses revealed that the better capacitance behavior of Li<sub><i>Z</i></sub>Cd<sub><i>Y</i></sub>Zn<sub><i>X</i></sub>Ni<sub>1−(<i>X+Y+Z</i>)</sub>Fe<sub>2</sub>O<sub>4</sub> based cathode materials. Further, the electric properties of materials depend on the external magnetic field (0.1, 0.2 and 0.3 Tesla) which exhibits the variation in impedance (<i>Z</i>′ and <i>Z</i>″), dielectric (<i>ε</i>′ and <i>ε</i>″) and ac-conductivity (<i>σ</i><sub>ac</sub>) responses due to the magneto-electric coupling effect. The enhancement in all the electric and magneto-electric results represent that the prepared novel magnetic specimens could be a promising character in energy conversion and energy storage applications. Therefore, it can be utilized in the development of novel cathodes for energy storage and GMR sensor applications.</p>","PeriodicalId":646,"journal":{"name":"Journal of Materials Science: Materials in Electronics","volume":null,"pages":null},"PeriodicalIF":2.8,"publicationDate":"2024-08-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141935245","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
High-performance self-powered electrochemical photodetectors based on co-precipitation and hydrothermally synthesized HgS nanoparticles 基于共沉淀和水热合成 HgS 纳米粒子的高性能自供电电化学光电探测器
IF 2.8 4区 工程技术
Journal of Materials Science: Materials in Electronics Pub Date : 2024-08-05 DOI: 10.1007/s10854-024-13299-5
Peeyush Phogat, Soumya Rai, Shreya, Ranjana Jha, Sukhvir Singh
{"title":"High-performance self-powered electrochemical photodetectors based on co-precipitation and hydrothermally synthesized HgS nanoparticles","authors":"Peeyush Phogat, Soumya Rai, Shreya, Ranjana Jha, Sukhvir Singh","doi":"10.1007/s10854-024-13299-5","DOIUrl":"https://doi.org/10.1007/s10854-024-13299-5","url":null,"abstract":"<p>In the realm of current technological advancements, the development of efficient materials for diverse applications is paramount. Photodetectors are crucial components in applications, such as optical communication systems, sensing devices, and imaging technologies, driving extensive research efforts to enhance their performance. This study presents a comprehensive exploration of mercury sulfide synthesized via two distinct methods, co-precipitation (HS) and hydrothermal method (HSA), focusing on their applicability as thin films for photodetectors. XRD analysis confirmed the crystalline nature of both samples, with HS exhibiting a cubic structure and HSA displaying a combination of cubic and hexagonal structures. UV–Visible spectra indicated absorbance in both the visible and UV regions for the samples, with HSA showing a higher number of absorbance peaks compared to HS. FESEM analysis revealed agglomerated spherical morphologies for both HS and HSA. Electrochemical analysis demonstrated a diffusion-controlled behavior for both samples. Moreover, self-powered electrochemical photodetectors (ECPD) based on synthesized HgS thin films were fabricated and characterized. The ECPD devices exhibited remarkable performance metrics underscoring superior values of responsivity (0.00329 ± 0.00012 mA/W) and rise time (0.07 ± 0.002 secs) of HSA at 0 V bias. The comprehensive analysis using various techniques provides valuable insights into the properties of the synthesized mercury sulfide samples, highlighting the enhanced photodetector capabilities of HSA over HS, paving the way for its application in advanced self-powered optoelectronic devices.</p>","PeriodicalId":646,"journal":{"name":"Journal of Materials Science: Materials in Electronics","volume":null,"pages":null},"PeriodicalIF":2.8,"publicationDate":"2024-08-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141935249","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
The substantial role of TiO2 in bimetallic alloy nanoparticle arrangement: electrocatalytic determination of glucose at Ni-Co@TiO2@GCE TiO2 在双金属合金纳米粒子排列中的重要作用:Ni-Co@TiO2@GCE 对葡萄糖的电催化测定
IF 2.8 4区 工程技术
Journal of Materials Science: Materials in Electronics Pub Date : 2024-08-05 DOI: 10.1007/s10854-024-13272-2
Muhammad Tariq, Muhammad Saqib, Abdur Rahim, Duncan S. Sutherland
{"title":"The substantial role of TiO2 in bimetallic alloy nanoparticle arrangement: electrocatalytic determination of glucose at Ni-Co@TiO2@GCE","authors":"Muhammad Tariq, Muhammad Saqib, Abdur Rahim, Duncan S. Sutherland","doi":"10.1007/s10854-024-13272-2","DOIUrl":"https://doi.org/10.1007/s10854-024-13272-2","url":null,"abstract":"<p>Herein, we investigate glucose detection on Ni-Co supported on TiO<sub>2</sub>. The polyol method is used for the synthesis of Ni-Co@TiO<sub>2</sub> nanocomposites (NCs). The morphological and structural properties of Ni-Co@TiO<sub>2</sub> NCs is examined by TEM, SEM, EDX, XRD, while the electrocatalytic properties of Ni-Co@TiO<sub>2</sub>@GCE is monitored using voltammetry and amperometry. The Ni-Co@TiO<sub>2</sub>@GCE exhibts tremendous electrocatalytic activity towards glucose at a working potential of + 0.45 V. The Ni-Co@TiO<sub>2</sub>@GCE shows an excellent response in a wide linear range (0.2–12 mM) with a low limit of detection (0.044 µM), superior sensitivity (2950 µA/mM cm<sup>−2</sup>), stable, and selective response in the presence of interfering species (such as ascorbic acid, uric acid, acetaminophen, NaClz, fructose, xylose, lactose and maltose) within short time o (&lt; 2 s). The Ni-Co@TiO<sub>2</sub>@GCE is also applied for determination of glucose in a real blood sample of a diabetic patient.</p>","PeriodicalId":646,"journal":{"name":"Journal of Materials Science: Materials in Electronics","volume":null,"pages":null},"PeriodicalIF":2.8,"publicationDate":"2024-08-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141935239","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Tuning sensitivity of surface plasmon resonance sensor based on ZnO layer and CaF2 prism for the recognition of SARS-CoV-2 基于氧化锌层和 CaF2 棱镜的表面等离子体共振传感器在识别 SARS-CoV-2 时的灵敏度调节
IF 2.8 4区 工程技术
Journal of Materials Science: Materials in Electronics Pub Date : 2024-08-05 DOI: 10.1007/s10854-024-13287-9
Amrindra Pal, Youssef Trabelsi, Partha Sarkar, Manoj Sharma, Manoj Kumar, Arun Uniyal
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