{"title":"Effect of Isothermal Treatment and Rolling on the Microstructure and Properties of Low Carbon Manganese Steel","authors":"Rendong Liu, Xiaonan Wang, Xin Xu, Chenshuo Cui, Dong Lv, Qian Sun, Zheng Cao, Lijia He, Fei Teng, Wenlu Fan, Zhu Chen, Rong Wang, Jianxia Lin, Tinting Wang, Minfu Xia","doi":"10.1007/s11665-024-10626-z","DOIUrl":"10.1007/s11665-024-10626-z","url":null,"abstract":"<div><p>The effects of isothermal treatment and rolling on the microstructure and mechanical properties of low carbon manganese steel were investigated using optical microscopy, scanning electron microscopy and transmission electron microscopy. The isothermal temperature affects the precipitation particle size, morphology, quantity and distribution characteristics. As the isothermal temperature increases from 500 to 700 °C, the microstructure was gradually transformed from bainite and ferrite to ferrite and pearlite, and further transformed to ferrite and martensite. The contribution of precipitation strengthening exceeds 120 MPa at an isothermal temperature of 600 °C. With the increase in the cooling rate, the lath characteristics of bainite becomes more obvious, and the transformation of granular bainite to lath bainite is accelerated. Under a certain rolling process, the strength of the high nitrogen steel is 10-50 MPa higher than that of the low-nitrogen steel. 180° cold bending test results show that there is no crack on the surface and sides of the specimen, indicating good cold work formability.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"34 17","pages":"18389 - 18401"},"PeriodicalIF":2.0,"publicationDate":"2025-02-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://link.springer.com/content/pdf/10.1007/s11665-024-10626-z.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145011473","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Mahshid Hafezi, Jack Allen, Andrew P. Abbott, Andrew Feeney
{"title":"Tribological Characterization of Friction-induced Phase Transformations in Binary Nitinol","authors":"Mahshid Hafezi, Jack Allen, Andrew P. Abbott, Andrew Feeney","doi":"10.1007/s11665-025-10782-w","DOIUrl":"10.1007/s11665-025-10782-w","url":null,"abstract":"<div><p>The binary alloy of nickel and titanium, commonly known as Nitinol, is widespread in the biomedical industry such as vascular stents. Recently, Nitinol’s application potential has expanded, including as actuating materials in ultrasonic transducers and robotic systems. In such cases, the temperature-dependent elastic moduli of Nitinol can be controlled via mechanical load or temperature triggers, between those for compliant martensite and stiff austenite. However, we have limited the understanding of the contact mechanics, predominantly the surface reactions and wear rate, of binary Nitinol in contact with other materials. The importance of this is understanding how Nitinol can be integrated in a wider range of industrial applications. Here, tribological investigations are undertaken to assess the phase transformation and contact mechanics of Nitinol under friction conditions, for stainless steel and titanium, chosen as common interfacing materials in actuation systems such as ultrasonic transducers. Experimental results demonstrate the phase transition from martensite to austenite via changes of elasticity in shape memory Nitinol rubbing against stainless steel under a dry condition. During these interactions, Nitinol exhibits a mass reduction of 0.00091 g, with a wear depth of 1.7 µm. Thermal analysis revealed that the austenite start temperature (As) is very close to ambient room temperature, at 25ºC. A multiple-load cycle indentation using a three-sided diamond tip was employed to evaluate the response of Nitinol to localized applied forces, where martensitic Nitinol has experienced a maximum force of 490 mN. Microscopic observations confirm the formation of oxide layers on Nitinol’s surface resulting from titanium exposure to oxygen. Meanwhile, the nonlinear hardness for martensitic Nitinol has been exhibited with increasing depth of penetration, exhibiting a maximum of 4.5 GPa. The novelty of the research is centered on both the tribological and mechanical performance of Nitinol-based actuating systems for a wide range of medical and industrial applications.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"34 9","pages":"7534 - 7546"},"PeriodicalIF":2.0,"publicationDate":"2025-02-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://link.springer.com/content/pdf/10.1007/s11665-025-10782-w.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145143182","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Microstructure and Mechanical Properties of Extruded Mg-2Sn-1.8Li-2Al-1Ag-0.5Zn Alloys","authors":"Zhichao Xu, Yancheng Zhu, Jie Song, Wei Liu, Jingren Li, Hongliang Zhao, Chang Zhu, Hucheng Pan, Gaowu Qin","doi":"10.1007/s11665-025-10727-3","DOIUrl":"10.1007/s11665-025-10727-3","url":null,"abstract":"<div><p>In this work, the microstructure and mechanical properties of as-extruded Mg-2Sn-1.8Li-2Al-1Ag-0.5Zn alloy (TLAQZ22211) were investigated, and it is found that the TLAQZ22211 alloy exhibited a bimodal grain structure after hot extrusion processing, with coarse elongated grains parallel to extrusion direction and fine grains surrounded. The yield strength (YS), ultimate tensile strength (UTS), and elongation (EL) of the TLAQZ22211 alloy extruded at 200 °C were measured at 295, 343 MPa, and 12.5%, respectively. The evolution of microstructure, changes in mechanical properties, and the influence of precipitation phase and dislocation on the properties of the alloy during deformation were discussed. The influence of dislocation-precipitation phase-interface synergistic strengthening effect on mechanical properties was compared and analyzed. The results showed that the high strength was mainly derived from the grain boundaries, nano-precipitations, and residual dislocations. And the good ductility can be attributed to the optimized bimodal grain structure and profuse low-angle grain boundaries (LAGBs) formed inside the elongated grains. The implementation of this work can provide guidance for the design and deformation of lightweight and high-strength magnesium alloys.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"34 18","pages":"20364 - 20375"},"PeriodicalIF":2.0,"publicationDate":"2025-02-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145090578","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Maraboina Raju, Mehdi Tlija, Jaber Abu Qudeiri, Vamsi Krishna Pasam, Venkatesh Gudipadu, Vishal Naranje
{"title":"Parametric Analysis for Ultrasonic-Assisted Magnetic Abrasive Finishing of AlSi12Mg Alloy Fabricated through Selective Laser Melting","authors":"Maraboina Raju, Mehdi Tlija, Jaber Abu Qudeiri, Vamsi Krishna Pasam, Venkatesh Gudipadu, Vishal Naranje","doi":"10.1007/s11665-025-10735-3","DOIUrl":"10.1007/s11665-025-10735-3","url":null,"abstract":"<div><p>The present work concentrates on the finishing of AlSi12Mg components, fabricated via selective laser melting (SLM), using a novel ultrasonic-assisted magnetic abrasive finishing process, marking its first application to 3D printed materials. The research examines the impact of varying process parameters including input voltage, rotational speed, abrasive weight percentage, abrasive grit size, and ultrasonic power intensity on surface finish (<i>R</i><sub><i>a</i></sub>), cutting force (<i>F</i><sub>c</sub>), microstructure, and residual stresses. Results indicate that increasing voltage, abrasive weight percentage, and ultrasonic power intensity enhance surface quality by reducing roughness. Rotational speed improves surface finish up to a certain limit, beyond which quality deteriorates. Finer grit sizes also contribute to better surface finishes. The optimal condition is found to be a rotational speed of 1400 rpm, a voltage of 50 V, 90% ultrasonic power intensity, 25% abrasive percentage, and 180 grit size, achieving a surface roughness of 0.179 µm, representing a 92.2% reduction from the initial SLM component. Additionally, residual stresses are increased with higher voltage, ultrasonic power intensity, and abrasive percentage, with finer grit sizes. Under these optimal conditions, a compressive residual stress of 30.3 MPa is achieved.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"34 18","pages":"20181 - 20196"},"PeriodicalIF":2.0,"publicationDate":"2025-02-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145090574","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Song Longfei, Hu Wenbin, Li Xingxing, Zeng Cheng, Liao Bokai, Wan Shan, Guo Xingpeng
{"title":"Comparison of Electrochemical Characteristics and Passive Behavior of As-Cast and Heat-Treated AlCoCrFeNi2.1 Eutectic High-Entropy Alloys in Cl−Containing Sulfuric Acid Solution","authors":"Song Longfei, Hu Wenbin, Li Xingxing, Zeng Cheng, Liao Bokai, Wan Shan, Guo Xingpeng","doi":"10.1007/s11665-025-10771-z","DOIUrl":"10.1007/s11665-025-10771-z","url":null,"abstract":"<div><p>AlCoCrFeNi<sub>2.1</sub> eutectic high-entropy alloys with excellent mechanical properties have received increasing attention in recent years, while the corrosion resistance of the alloy is rarely reported. This work investigated the corrosion and passive behaviors of as-cast and heat-treated (maintain at 1200 °C for 3 h and then quenched in water) AlCoCrFeNi<sub>2.1</sub> eutectic high-entropy alloys by electrochemical tests, as well as some surface characterizations, including scanning electron microscopy, energy-dispersive spectroscopy, atomic force microscopy, and x-ray photoelectron spectroscopy. Results showed that the heat-treat method was beneficial to the corrosion resistance of the alloy. The local contact potential difference (<i>V</i><sub>CPD</sub>) between the FCC and B2 phases of heat-treated alloy was less than that of as-cast alloy. Mott–Schottky curve measurement illustrated that the heat-treatments did not alert the semiconducting types of the passive films formed on the AlCoCrFeNi<sub>2.1</sub> EHEAs, but reduced the defect concentration in the films. Changes in chromium oxide content, aluminum oxide content and O<sup>2−</sup>/OH<sup>−</sup> ratio were one of the reasons that heat-treatment affecting the passive film property.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"34 18","pages":"19855 - 19867"},"PeriodicalIF":2.0,"publicationDate":"2025-02-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145090496","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Study of a Glass Foam Composite Loaded with Carbon Materials for Electromagnetic Wave Absorption Applications","authors":"Younes Lamri, Ratiba Benzerga, Laurent Le Gendre, Fayrouz Benhaoua, Azzedine Ayadi","doi":"10.1007/s11665-025-10773-x","DOIUrl":"10.1007/s11665-025-10773-x","url":null,"abstract":"<div><p>Glass foam composites have been fabricated and characterized for electromagnetic wave absorption application. The cullet based on recycling glass waste was used as a raw material for the manufacture of foams. Carbonic fillers of rubber powder and carbon fibers were utilized with different amounts to test the absorption efficiency of electromagnetic waves. The composites show a relatively homogeneous porous structure. The density of the produced composites varies between 213 and 347 kg/m3. Observation by scanning electron microscope shows significant degradation of rubber powders unlike carbon fibers. Gravimetric thermal analysis reveals a mass loss of 62.06% of rubber powders and 1.71% of carbon fibers during heat treatment. The dielectric characterization results exhibit an evolution of the dielectric properties (permittivity and dielectric losses) as a function of the carbon charges. Glass foam composites filled with carbon fibers have a permittivity (ε’) between 1.78 and 3.72 and high dielectric losses (tanδ) between 0.32 and 0.46 at 10 GHz. The dielectric properties of glass foam filled with rubber powders are marginally lower compared to those loaded with carbon fibers. The reflection loss measurements indicate significant absorption performance for the samples. The foam containing 6% carbon fibers recorded a reflection loss of − 35.97 dB at 11.44 GHz, accompanied by a broad absorption bandwidth of 2.48 GHz, indicating absorption greater than 90%.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"34 18","pages":"20355 - 20363"},"PeriodicalIF":2.0,"publicationDate":"2025-02-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145090495","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Assessment of Corrosion and Macrostructural Behavior of Ti6321/SS 310 Butt Joints: In Situ Study of Similar and Dissimilar Joints via Friction Stir Welding Technique","authors":"K. Sai Sujith, S. Ravi","doi":"10.1007/s11665-025-10758-w","DOIUrl":"10.1007/s11665-025-10758-w","url":null,"abstract":"<div><p>Among all other alloys, titanium alloys have demanding applications in aerospace, automobiles, and defense due to their superior properties to monolithic ones. The similar and dissimilar Ti-6Al-3Nb-2Zr-1Mo (Ti6321) and stainless steel (SS 310) joints are performed through friction stir welding. This work investigates the mechanical and corrosion behavior of FSW joints. Significant efforts have been made in research and development to create titanium alloys that possess both high strength and low weight in response to their increasing demand in industrial and orthopedic applications where durability and efficiency are crucial. The three microscopically distinct regions of the weld nugget and heat-affected zone on the advancing and retreating sides for welds made with different tool pin profiles are carried out. Tensile, microhardness, and compression tests are conducted on all five plates. The macrostructure, including an analysis of the corrosion test, is performed. It is observed that the similar Ti6321 joint with a 6 mm pin diameter, 60 mm transverse speed, 900 mm rotational speed, and a constant axial force of 1 KN exhibits a maximum compression strength of 1037 MPa and microhardness of 362 HV when compared to other joints. The results identified that similar joints significantly affect the microstructure, mechanical properties, and corrosion resistance.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"34 17","pages":"18620 - 18633"},"PeriodicalIF":2.0,"publicationDate":"2025-02-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145011658","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Adjusting Stress-Relief Annealing: Enhancing the Fatigue Performance of Hoop in High-Strength Thin-Walled Steel Tubes","authors":"Junfeng Wu, Yukui Gao","doi":"10.1007/s11665-025-10790-w","DOIUrl":"10.1007/s11665-025-10790-w","url":null,"abstract":"<div><p>The bulging process of high-strength thin-walled tubes is an effective alternative to traditional tube sheet welding. However, the fatigue damage at the bulges of the thin-walled tubes seriously affects the safe service of the components. A stress-relief annealing process with different heating/cooling rates (100 and 200 °C/h) and holding times (1, 2, and 3 h) was proposed to optimize the microstructure and fatigue performance of thin-walled bulges. The experimental results indicate that the added annealing at 520 °C at a heating/cooling rate of 100 °C/h and holding 3 h can decrease residual stress from 480 to 74.5 MPa and improve fatigue cycle number from 984 to 2727 without affecting the ultimate tensile strength of about 550 MPa. Stress-relief annealing only delays the fracture process of the regions I and III, but it hardly suppresses the fracture of region II as microcracks. In addition, the existence of initial microcracks is the main factor leading to a shortened fatigue life. This study can provide theoretical support and technical reference for low-cost optimization of the fatigue performance of high-strength thin-walled steel tubes in the aerospace and automotive manufacturing industries.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"34 18","pages":"19980 - 19991"},"PeriodicalIF":2.0,"publicationDate":"2025-02-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145090483","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Min Zheng, Jie Chen, Zongxiao Zhu, Jiao Chen, Jun Cheng, Shengyu Zhu, Jun Yang
{"title":"Temperature-Adaptive Self-Lubricating Alloys with Soft Silver and Tribo-Chemical Silver Vanadate","authors":"Min Zheng, Jie Chen, Zongxiao Zhu, Jiao Chen, Jun Cheng, Shengyu Zhu, Jun Yang","doi":"10.1007/s11665-025-10770-0","DOIUrl":"10.1007/s11665-025-10770-0","url":null,"abstract":"<div><p>Self-adaptive conception provides a reference for design of high-temperature self-lubricating material. Herein, temperature-adaptive Ni<sub>3</sub>Al-based self-lubricating alloys were designed and fabricated based on soft lubricating silver and tribo-chemical silver vanadate, and their performance was investigated over a broad range of temperatures. Ni<sub>3</sub>Al-Ag-V alloys exhibit excellent self-lubricating properties and wear resistance over a wide temperature range, especially for the Ni<sub>3</sub>Al-20 wt.%Ag-5 wt.%V alloy with friction coefficients as low as 0.26 and 0.23 at room temperature and 900 °C, respectively, and wear rates as low as 5 × 10<sup>−6</sup> mm<sup>3</sup>/Nm and 4 × 10<sup>−5</sup> mm<sup>3</sup>/Nm in turn. It is proposed for a temperature-adaptive lubrication mechanism, such as tribo-chemistry of silver vanadate, tribo-transfer film, and the synergistic lubrication effect of soft metal Ag at low temperatures and silver vanadate at high temperatures.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"34 18","pages":"20197 - 20211"},"PeriodicalIF":2.0,"publicationDate":"2025-02-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145090484","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
G. X. Zhou, T. Zhao, R. Wang, C. H. Zhang, C. L. Wu, S. Zhang, J. Chen
{"title":"Study on Microstructure and Cavitation Resistance of Fe-Based and Ni-Based Alloy Coatings by Plasma Transfer Arc Welding","authors":"G. X. Zhou, T. Zhao, R. Wang, C. H. Zhang, C. L. Wu, S. Zhang, J. Chen","doi":"10.1007/s11665-025-10705-9","DOIUrl":"10.1007/s11665-025-10705-9","url":null,"abstract":"<div><p>Fe-based alloy and Ni-based alloy modified layers were prepared on the surface of Z5CND16-05 martensitic stainless steel by plasma transfer arc process. The differences in microstructure, microhardness, friction, corrosion resistance, and cavitation resistance of coatings with different alloy compositions were studied. The results show that the Fe-based alloy coating is composed of cellular α-Fe solid solution matrix phase and gray eutectic structures (Fe, Cr)<sub>7</sub>C<sub>3</sub> and (Fe, Cr)<sub>23</sub>C<sub>6</sub> distributed between dendrites. The nickel-based alloy coating structure is mainly light gray dendrites, and the matrix is γ-Ni face-centered cubic solid solution. The nickel-based alloy coating structure shows directional growth at the interface. Due to the existence of equiaxed crystals in Ni-based alloy coating and the refinement of microstructure in Fe-based alloy coating, their wear resistance is better than that of substrate. In 3.5 wt% NaCl solution at room temperature, the electrochemical corrosion current density of nickel-based alloy coating is 1.7 × 10<sup>−7</sup> cm<sup>−2</sup>, and its passivation film shows good continuity and integrity. Compared with martensitic stainless steel substrate, the microhardness of the two materials is significantly improved. After cavitation erosion for 4 hours, the weight loss of Ni-based alloy coating is the lowest, and the average erosion rate is the lowest of 1.50 μm/h.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"34 18","pages":"19881 - 19894"},"PeriodicalIF":2.0,"publicationDate":"2025-02-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145090487","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}