{"title":"Effect of Electropulsing Cyclic Baking Process on Microstructure and Mechanical Properties during Hot Compression for 7050 Aluminum Alloy","authors":"Yang Tian, Zhenshuai Li, Yifu Jiang, Tiegang Li","doi":"10.1007/s11665-025-11003-0","DOIUrl":null,"url":null,"abstract":"<div><p>In the present study, transmission electron microscopy (TEM), differential scanning calorimeter (DSC), and electron back-scattered diffraction (EBSD) were performed to investigate the effect of electropulsing cyclic baking process on microstructure and mechanical properties during hot compression for 7050 aluminum alloy in detail. The novel ECB process was compared with traditional furnace heating (FH). The results show that the quantity and size of precipitation under the FH condition were smaller than those in ECB condition, with temperature positively correlating to precipitation. The ECB process could efficiently promote the nucleation and growth of <i>η</i>’ and <i>η</i> phases. In the ECB/160 °C sample, a high density of <i>η</i>’ and a few <i>η</i> phases were observed, while the ECB/180 °C sample exhibited a large number of <i>η</i> phases, with nearly no <i>η</i>’ precipitates in the Al matrix. Additionally, the fraction of low-angle grain boundaries (LAGBs) and medium-angle grain boundaries (MAGBs) increased with the aging temperature, with higher values in the ECB samples compared to the FH samples at the same temperature. Both continuous dynamic recrystallization (CDRX) and discontinuous dynamic recrystallization (DDRX) occurred during both ECB and FH processes, and high fraction recrystallization was obtained through reducing the nucleation energy required for recrystallization through electropulsing cyclic baking process. The ECB samples exhibited superior strength and plasticity compared to the FH samples. Specifically, the ultimate tensile strength, yield strength, and elongation of the ECB/160 °C sample were 436 MPa, 538 MPa, and 12.56%, respectively, demonstrating excellent overall mechanical properties.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"34 20","pages":"23353 - 23361"},"PeriodicalIF":2.0000,"publicationDate":"2025-03-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Materials Engineering and Performance","FirstCategoryId":"88","ListUrlMain":"https://link.springer.com/article/10.1007/s11665-025-11003-0","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0
Abstract
In the present study, transmission electron microscopy (TEM), differential scanning calorimeter (DSC), and electron back-scattered diffraction (EBSD) were performed to investigate the effect of electropulsing cyclic baking process on microstructure and mechanical properties during hot compression for 7050 aluminum alloy in detail. The novel ECB process was compared with traditional furnace heating (FH). The results show that the quantity and size of precipitation under the FH condition were smaller than those in ECB condition, with temperature positively correlating to precipitation. The ECB process could efficiently promote the nucleation and growth of η’ and η phases. In the ECB/160 °C sample, a high density of η’ and a few η phases were observed, while the ECB/180 °C sample exhibited a large number of η phases, with nearly no η’ precipitates in the Al matrix. Additionally, the fraction of low-angle grain boundaries (LAGBs) and medium-angle grain boundaries (MAGBs) increased with the aging temperature, with higher values in the ECB samples compared to the FH samples at the same temperature. Both continuous dynamic recrystallization (CDRX) and discontinuous dynamic recrystallization (DDRX) occurred during both ECB and FH processes, and high fraction recrystallization was obtained through reducing the nucleation energy required for recrystallization through electropulsing cyclic baking process. The ECB samples exhibited superior strength and plasticity compared to the FH samples. Specifically, the ultimate tensile strength, yield strength, and elongation of the ECB/160 °C sample were 436 MPa, 538 MPa, and 12.56%, respectively, demonstrating excellent overall mechanical properties.
期刊介绍:
ASM International''s Journal of Materials Engineering and Performance focuses on solving day-to-day engineering challenges, particularly those involving components for larger systems. The journal presents a clear understanding of relationships between materials selection, processing, applications and performance.
The Journal of Materials Engineering covers all aspects of materials selection, design, processing, characterization and evaluation, including how to improve materials properties through processes and process control of casting, forming, heat treating, surface modification and coating, and fabrication.
Testing and characterization (including mechanical and physical tests, NDE, metallography, failure analysis, corrosion resistance, chemical analysis, surface characterization, and microanalysis of surfaces, features and fractures), and industrial performance measurement are also covered