Abdul Nazer K H, Namitha Venugopal, Hrithik Krishna Raj, Chinnu V K, Pankaj Sagar
{"title":"Assessment of thermal conductivity in activated carbon adsorbents for liquid nitrogen-based cryo-adsorption vacuum pump applications.","authors":"Abdul Nazer K H, Namitha Venugopal, Hrithik Krishna Raj, Chinnu V K, Pankaj Sagar","doi":"10.1063/5.0242242","DOIUrl":"https://doi.org/10.1063/5.0242242","url":null,"abstract":"<p><p>This paper presents a method for measuring the thermal conductivity of activated carbon adsorbents at liquid nitrogen (LN2) temperature for LN2-based cryo-adsorption vacuum pumps. This method is simple, versatile, and adaptable to various sample geometries of material under evaluation, including powders, spheres, granules, and pellets. This method can also be applied to assess similar materials with thermal conductivity in the range of 0.1-1.5 W/(m K). The thermal conductivity was evaluated by establishing a temperature gradient across the LN2-cooled sample using controlled heat inputs. The measurement accuracy was verified using glassy glycerol whose thermal conductivities at LN2 temperature had already been studied and reported in the literature. The thermal conductivities of activated carbon measured ranged from 0.14 to 0.25 W/(m K) across different sample types and conditions, including forms, packing density, and filler compositions. With an error margin established at 5%, the technique proves both effective and reliable for thermal conductivity measurements at LN2 temperature, offering promising applications in cryogenic engineering, insulation material development, and thermal management systems.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":"96 3","pages":""},"PeriodicalIF":1.3,"publicationDate":"2025-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143711141","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
R Yamato, S Kobayashi, T Fujita, K Nagaoka, K Nagasaki, S Inagaki, T Kawate, H Ohgaki, T Kii, H Zen, S Kado, T Minami, H Okada, S Ohshima, S Konoshima, T Mizuuchi, Y Mototake
{"title":"Measurement of x-ray bremsstrahlung radiation from high energy electrons by stochastic acceleration in Heliotron J.","authors":"R Yamato, S Kobayashi, T Fujita, K Nagaoka, K Nagasaki, S Inagaki, T Kawate, H Ohgaki, T Kii, H Zen, S Kado, T Minami, H Okada, S Ohshima, S Konoshima, T Mizuuchi, Y Mototake","doi":"10.1063/5.0231450","DOIUrl":"https://doi.org/10.1063/5.0231450","url":null,"abstract":"<p><p>A synthetic diagnostic of x-ray bremsstrahlung radiation and a Monte Carlo radiation transport simulation were carried out to obtain the electron energy distribution in stochastic acceleration experiments in Heliotron J, a mid-sized heliotron-type magnetic confinement device. Three sets of LaBr3(Ce) scintillator and photomultiplier tubes were installed in Heliotron J in three directions relative to the magnetic field line, co, counter, and perpendicular, to determine the velocity distribution of the high-energy electrons. These systems are positioned about 5 m away from the vacuum chamber and shielded by lead blocks and magnetic shields to reduce the influence of stray radiation and magnetic fields. The vacuum chamber of Heliotron J is made of stainless steel with a 3D helical shape. Since its x-ray shielding effect is not negligible when obtaining the x-ray energy distribution in the vacuum chamber, the Monte Carlo radiation transport code particle and heavy ion transport code system was applied to Heliotron J to clarify the shielding effect. Given the vacuum chamber and coil shape information and x-ray energy distribution expected in the vacuum chamber, this code can calculate x-ray energy distribution considering the shielding effect of Heliotron J. This simulation model was based on computer aided design data of Heliotron J devices. The x-ray energy distribution in the vacuum vessel was adapted until the simulated and measured x-ray spectra outside the vacuum vessel match with each other. The shapes of resultant distribution have two types of shape: power-law distribution at more than 450 keV and Maxwell distribution at less than 450 keV. At a higher energy range, x-ray bremsstrahlung energy distribution is consistent with the characteristic of stochastic acceleration.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":"96 3","pages":""},"PeriodicalIF":1.3,"publicationDate":"2025-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143711147","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"A highly optical, controlled trajectory rapid compression and expansion machine for gas phase chemical physics research.","authors":"A C Dhotre, S Biswas","doi":"10.1063/5.0212259","DOIUrl":"https://doi.org/10.1063/5.0212259","url":null,"abstract":"<p><p>A highly optical Controlled Trajectory Rapid Compression and Expansion Machine (CT-RCEM) has been developed at the University of Minnesota (UMN) for fundamental research in gas phase chemical reaction kinetics, combustion, and high-temperature gas dynamics. Unlike traditional rapid compression machines, UMN CT-RCEM features precise piston motion control using an electrohydraulic actuation system and an active feedback motion controller, allowing digital adjustment of compression ratio, stroke, compression time, and piston trajectory. This innovation eliminates mechanical interventions, enables a higher number of experimental tests in a given time, and offers superior control over the thermodynamic states of the gas mixture under investigation. Equipped with multiple optical windows, including an end-wall, four side-walls, and their variants to accommodate various experimental scenarios, CT-RCEM provides exceptional optical accessibility, enabling fundamental studies utilizing advanced optical and laser diagnostics. Custom-designed UV-grade sapphire windows with specialized seals withstand high combustion temperatures and pressures of up to 250 bar. The optical windows are interchangeable with metal windows, allowing easy integration of equipment such as igniters, injectors, glow plugs, pre-chambers, and sensors. The versatility, functionality, and performance of the CT-RCEM were demonstrated through autoignition experiments with dimethyl ether/air, spark ignition, and optical pre-chamber visualization studies with methane/air. UMN's highly optical CT-RCEM provides a unique platform for gas phase chemical physics research and holds the potential to advance renewable fuels, plasma, and low-emission propulsion alternatives, promoting sustainable energy solutions.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":"96 3","pages":""},"PeriodicalIF":1.3,"publicationDate":"2025-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143664322","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
C Yoo, G D Conway, W Burke, P A Molina Cabrera, B Vanovac, R Bielajew, D J Cruz-Zabala, A Silva, A E White
{"title":"Design of a correlation reflectometer radiometer diagnostic and measurements of the electron density-temperature cross-phase angle in the H-mode pedestal with small edge localized modes at ASDEX Upgrade.","authors":"C Yoo, G D Conway, W Burke, P A Molina Cabrera, B Vanovac, R Bielajew, D J Cruz-Zabala, A Silva, A E White","doi":"10.1063/5.0243894","DOIUrl":"https://doi.org/10.1063/5.0243894","url":null,"abstract":"<p><p>This work presents the hardware design and first results from a newly commissioned correlation reflectometer radiometer diagnostic that measures the cross-phase angle between electron density and temperature fluctuations in ASDEX Upgrade plasmas. This diagnostic employs cross correlations between signals measured by a tunable, continuous wave, perpendicular incidence, fluctuation reflectometer, and a 24-channel radiometer sharing the same line of sight. Novel measurements in the pedestal of a helium H-mode plasma with small edge localized modes show changes in the cross-phase angle between the electron density and temperature fluctuations from ∼90° to 120°, suggesting changes in the properties of the turbulence driving transport in the plasma edge.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":"96 3","pages":""},"PeriodicalIF":1.3,"publicationDate":"2025-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143543398","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Yue Zhang, Ming Kong, Saijie Mou, Shilin Gu, Lu Liu, Lei Zhu
{"title":"Development and evaluation of a bipedal stepping piezoelectric actuator based on stick-slip principle.","authors":"Yue Zhang, Ming Kong, Saijie Mou, Shilin Gu, Lu Liu, Lei Zhu","doi":"10.1063/5.0244587","DOIUrl":"https://doi.org/10.1063/5.0244587","url":null,"abstract":"<p><p>In this work, a novel bipedal stepping piezoelectric actuator based on stick-slip principle is proposed. An integrated stator with symmetrically positioned dual driving feet has been developed, characterized by its element analysis. Key structural parameters were optimized, and a prototype was fabricated for a series of experiments. The experimental results demonstrate that the actuator attains a maximum output speed of 4550 μm/s at a voltage of 150 V and a frequency of 350 Hz. The stepping efficiency is measured at 0.886, with a maximum horizontal load capacity of 170 g. Furthermore, the actuator exhibits a displacement resolution of 180 nm, making it highly suitable for precision actuation and applications in fields such as biomedical engineering.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":"96 3","pages":""},"PeriodicalIF":1.3,"publicationDate":"2025-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143543415","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"An apparatus for preparing frozen solution samples in ultrahigh vacuum experiments.","authors":"Xinmeng Liu, Jiadong Guo, Jiani Hong, Ying Jiang","doi":"10.1063/5.0253060","DOIUrl":"https://doi.org/10.1063/5.0253060","url":null,"abstract":"<p><p>Here, we develop an apparatus for preparing frozen solution samples, which can be characterized by surface science techniques under ultrahigh vacuum (UHV) conditions. When a temperature-controlled substrate makes contact with a frozen solution at 77 K, the surface of the frozen solution is locally melted and then refreezes together with the substrate. By detaching the substrate from the frozen solution in situ in a high vacuum, the frozen solution is cleaved and transferred onto the substrate. Applying this method, we demonstrate transferring NaCl and LiNO3 frozen solutions onto an Au substrate and directly imaging the crystallization of NaCl and LiNO3 with atomic resolution using atomic force microscopy (AFM) in UHV at 5 K. This apparatus provides a new approach to transfer solution samples in their glassy states into the UHV environment while maintaining the cleanliness of the samples, laying the foundation for further research related to the solution environment in real life, such as crystallization, hydration, chemical reaction, materials synthesis, and bioimaging.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":"96 3","pages":""},"PeriodicalIF":1.3,"publicationDate":"2025-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143731523","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Development of a helix-based beam position monitor calibration system for sub-relativistic charged-particle beams.","authors":"Minwen Wang, Xin Zhuo, Mingtong Zhao, Maocheng Wang, Yihua Yan, Wenbo Ye, Mengtong Qiu, Zhongming Wang, Rui Zhu","doi":"10.1063/5.0256290","DOIUrl":"https://doi.org/10.1063/5.0256290","url":null,"abstract":"<p><p>Accurate calibration of beam position monitor (BPM) responses is a prerequisite for precise beam position measurements. Traditional methods such as the stretched-wire or antenna method can accurately calibrate BPM responses for relativistic beams, but there has been a lack of effective calibration methods for non-relativistic beams, limiting the measurement accuracy of BPMs in low-energy proton or heavy ion linear accelerators. In this study, we developed a BPM calibration platform based on helical slow-wave structures, capable of effectively simulating the electromagnetic fields generated by non-relativistic beams and calibrating the BPM response to these beams. We introduced a period averaging method, which reduces calibration errors caused by impedance mismatches in the helix. We achieved offline calibration of button-type BPMs for non-relativistic beam response characteristics with β as low as 0.122 using this platform. BPM calibration data were compared with simulations and then on-line measurements in the medium beam transport line at the Xi'an Proton Application Facility. Within the central linear response region of the BPM (∼16% of the BPM aperture), the calibrated linear sensitivity of 0.0668 ± 0.0003 is in close agreement with the actual measurement result of 0.0669 ± 0.0009. In the nonlinear response region further from the center, extending to at least 60% of the BPM aperture, the relative measurement error of beam position can be controlled to within 1.2% after calibration. This advance significantly expands the measurement range and enhances the measurement accuracy of BPMs for non-relativistic beams.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":"96 3","pages":""},"PeriodicalIF":1.3,"publicationDate":"2025-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143701373","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Kaisheng Lin, Miaotian Wang, Yaohui Wang, Hongwei Li, Weimin Wang
{"title":"A multi-channel MRI console for ultra-high field up to 14 T.","authors":"Kaisheng Lin, Miaotian Wang, Yaohui Wang, Hongwei Li, Weimin Wang","doi":"10.1063/5.0239183","DOIUrl":"https://doi.org/10.1063/5.0239183","url":null,"abstract":"<p><p>Ultra-high field magnetic resonance imaging (MRI) offers significant advantages in terms of signal-to-noise ratio and spatial resolution. In this study, we detail the development of a multi-channel home-built MRI console operating at 14 T. We propose a hybrid analog-digital framework that shifts high-frequency radio frequency transmission and reception issues to lower frequencies, utilizing software-defined radio technology to process these low-frequency signals. Digital pre-emphasis is used in gradient calculations to counteract the effects of eddy currents during gradient switching. Our console can transmit and receive at center frequencies up to 600 MHz. The pulse programmer module achieves a timing resolution of 20 ns, while the transmitter can independently generate waveforms with varying amplitude, frequency, phase, and envelope. The receiver's dual-stage gain control provides 63 dB of adjustable range, optimizing the magnetic resonance (MR) signal's dynamic range. After frequency conversion, the MR signals are digitized with 16-bit resolution and 100 MHz sampling rate. High-resolution water phantom images are acquired on the 14 T Bruker Ascend 600 nuclear magnetic resonance magnet, demonstrating its potential for clinical research and application.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":"96 3","pages":""},"PeriodicalIF":1.3,"publicationDate":"2025-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143573798","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Marta Klepacka, Alexander Belushkin, Evgeny Goremychkin, Dorota Chudoba
{"title":"High luminosity inverse geometry inelastic neutron scattering spectrometer at pulsed fast reactor.","authors":"Marta Klepacka, Alexander Belushkin, Evgeny Goremychkin, Dorota Chudoba","doi":"10.1063/5.0244264","DOIUrl":"https://doi.org/10.1063/5.0244264","url":null,"abstract":"<p><p>The project of a new inelastic neutron scattering (INS) spectrometer in inverse geometry at the IBR-2 pulsed fast reactor (JINR, Dubna, Russia) has been proposed as a replacement for the old NERA instrument. The major feature of the proposed spectrometer is the substantially increased area of the energy analyzer, made of highly oriented pyrolytic graphite (HOPG). We developed a new method of constructing the large area reflecting surface of the energy analyzer for the time-of-flight INS spectrometer in inverse geometry at the pulsed neutron source. According to our calculations, the total area of the HOPG analyzer would be as large as 3.14 m2 with a solid angle coverage of 5.8 sr. In comparison with the existing NERA spectrometer, this gives a factor of thirty in enhancement of the spectrometer's luminosity.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":"96 3","pages":""},"PeriodicalIF":1.3,"publicationDate":"2025-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143649934","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Ahmed Gadelmawla, Yuta Yamamoto, Koji Kimura, Halubai Sekhar, Naohisa Happo, Kyle G Webber, Tomohiro Matsushita, Hiroo Tajiri, Koichi Hayashi
{"title":"Application of x-ray fluorescence holography to a single grain in polycrystalline ferroelectric ceramics.","authors":"Ahmed Gadelmawla, Yuta Yamamoto, Koji Kimura, Halubai Sekhar, Naohisa Happo, Kyle G Webber, Tomohiro Matsushita, Hiroo Tajiri, Koichi Hayashi","doi":"10.1063/5.0242691","DOIUrl":"https://doi.org/10.1063/5.0242691","url":null,"abstract":"<p><p>X-ray fluorescence holography (XFH) was, for the first time, applied to a polycrystalline system in order to visualize local structures within a single grain in the system using an x-ray microbeam. XFH was performed on (Ba,Ca)(Zr,Ti)O3 (BCZT) piezoelectric ceramic as the polycrystalline system in the normal mode with a two-dimensional detector. After data acquisition and processing, we obtained a Zr-Kα hologram from the BCZT ceramic. The Kossel lines were clearly observed, which were in good agreement with our simulated results, although there is a possibility that the hologram is contaminated by the signals from other surrounding grains. Furthermore, we confirmed that several atomic images reconstructed from the obtained Zr-Kα hologram can be related to the Ti atoms around Zr in the real space plane. These results clearly demonstrate the applicability of XFH to polycrystalline samples, which significantly expands the potential use of this technique for micro- or mesoscopic research in materials science.</p>","PeriodicalId":21111,"journal":{"name":"Review of Scientific Instruments","volume":"96 3","pages":""},"PeriodicalIF":1.3,"publicationDate":"2025-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143650080","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}