Critical reviews in analytical chemistry最新文献_第3页

Recent Trends and Advances in Porous Metal-Organic Framework Nanostructures for the Electrochemical and Optical Sensing of Heavy Metals in Water. 用于水中重金属电化学和光学传感的多孔金属有机框架纳米结构的最新趋势和进展。

IF 4.2 2区化学

Critical reviews in analytical chemistry Pub Date : 2024-08-01 Epub Date: 2022-08-13 DOI: 10.1080/10408347.2022.2106543

Naini Garg, Akash Deep, Amit L Sharma

{"title":"Recent Trends and Advances in Porous Metal-Organic Framework Nanostructures for the Electrochemical and Optical Sensing of Heavy Metals in Water.","authors":"Naini Garg, Akash Deep, Amit L Sharma","doi":"10.1080/10408347.2022.2106543","DOIUrl":"10.1080/10408347.2022.2106543","url":null,"abstract":"With the expansion and advancement in agricultural and chemical industries, various toxic heavy metals such as lead, cadmium, mercury, zinc, copper, arsenic etc. are continuously released into the environment. Intake of sources contaminated with such toxic metals leads to various health issues. Keeping the serious effects of these toxic metal ions in view, various organic-inorganic nanomaterials based sensors have been exploited for their detection via optical, electrochemical and colorimetric approaches. Since a chemical sensor works on the principle of interaction between the sensing layer and the analytes, a sensor material with large surface area is required to enable the largest possible interaction with the target molecules and hence the sensitivity of the chemical sensor. However, commonly employed materials such as metal oxides and conducting polymers tend to feature relatively low surface areas, and hence resulting in low sensitivity of the sensor. Metal-Organic Frameworks (MOFs) nanostructures are another category of organic-inorganic materials endowed with large surface area, ultra-high and tunable porosity, post-synthesis modification features, readily available active sites, catalytic activity, and chemical/thermal stability. These properties provide high sensitivity to the MOF based sensors due to the adsorption of large number of target analytes. The current review article focuses on MOFs based optical and electrochemical sensors for the detection of heavy metals.","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":null,"pages":null},"PeriodicalIF":4.2,"publicationDate":"2024-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"40613698","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Microextraction Techniques for Sample Preparation of Amphetamines in Urine: A Comprehensive Review. 用于尿液中苯丙胺类药物样品制备的微萃取技术：全面综述。

IF 4.2 2区化学

Critical reviews in analytical chemistry Pub Date : 2024-08-01 Epub Date: 2022-09-11 DOI: 10.1080/10408347.2022.2113028

Nasim Nourani, Arezou Taghvimi, Ahad Bavili-Tabrizi, Yousef Javadzadeh, Siavoush Dastmalchi

引用次数: 0

Deep Eutectic Solvents for Extraction and Preconcentration of Organic and Inorganic Species in Water and Food Samples: A Review. 用于萃取和预富集水和食品样品中有机和无机物的深共晶溶剂：综述。

IF 4.2 2区化学

Critical reviews in analytical chemistry Pub Date : 2024-08-01 Epub Date: 2022-08-18 DOI: 10.1080/10408347.2022.2111655

Muhammad Farooque Lanjwani, Mustafa Tuzen, Muhammad Yar Khuhawar, Mohammad Reza Afshar Mogaddam, Mir Ali Farajzadeh

{"title":"Deep Eutectic Solvents for Extraction and Preconcentration of Organic and Inorganic Species in Water and Food Samples: A Review.","authors":"Muhammad Farooque Lanjwani, Mustafa Tuzen, Muhammad Yar Khuhawar, Mohammad Reza Afshar Mogaddam, Mir Ali Farajzadeh","doi":"10.1080/10408347.2022.2111655","DOIUrl":"10.1080/10408347.2022.2111655","url":null,"abstract":"Deep eutectic solvents (DESs) have been developed as green solvents and these are capable as alternatives to conventional solvents used for the extraction of organic and inorganic species from food and water samples. The continuous generation of contaminated waste and increasing concern for the human health and environment have compelled the scientific community to investigate more ecological schemes. In this concern, the use of DESs have developed in one of the chief approach in the field of chemistry. These solvents have appeared as a capable substitute to conventional hazardous solvents and ionic liquids. The DESs has distinctive properties, easy preparation and components availability. It is not only used in scienctific fields but also used in quotidian life. There are many advantages of DESs in analytical chemistry, they are largely used for extraction and determination of inorganic and organic compounds from different samples. In previous a few years, several advanced researches have been focused on the separation and preconcentration of low level of pollutants using DESs as the extractants. This review summarizes the use of DESs in the separation and preconcentration of organic and inorganic species from water and food samples using various microextraction processes.","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":null,"pages":null},"PeriodicalIF":4.2,"publicationDate":"2024-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"40620757","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Electrochemical Sensing Systems for the Analysis of Catechol and Hydroquinone in the Aquatic Environments: A Critical Review. 用于分析水生环境中儿茶酚和对苯二酚的电化学传感系统：评论。

IF 4.2 2区化学

Critical reviews in analytical chemistry Pub Date : 2024-08-01 Epub Date: 2022-08-25 DOI: 10.1080/10408347.2022.2114784

Hicham Meskher, Fethi Achi

{"title":"Electrochemical Sensing Systems for the Analysis of Catechol and Hydroquinone in the Aquatic Environments: A Critical Review.","authors":"Hicham Meskher, Fethi Achi","doi":"10.1080/10408347.2022.2114784","DOIUrl":"10.1080/10408347.2022.2114784","url":null,"abstract":"Because of their unique physical, chemical, and biological characteristics, conductive nanomaterials have a lot of potential for applications in materials science, energy storage, environmental science, biomedicine, sensors/biosensors, and other fields. Recent breakthroughs in the manufacture of carbon materials, conductive polymers, metals, and metal oxide nanoparticles based electrochemical sensors and biosensors for applications in environmental monitoring by detection of catechol (CC) and hydroquinone (HQ) are presented in this review. To achieve this goal, we first introduced recent works that discuss the effects of phenolic compounds and the need for accurate, inexpensive, and quick monitoring, and then we focused on the use of the most important applications of nanomaterials, such as carbon-based materials, metals, and metal oxides nanoparticles, and conductive polymers, to develop sensors to monitor catechol and hydroquinone. Finally, we identified challenges and limits in the field of sensors and biosensors, as well as possibilities and recommendations for developing the field for better future applications. Meanwhile, electrochemical sensors and biosensors for catechol and hydroquinone measurement and monitoring were highlighted and discussed particularly. This review, we feel, will aid in the promotion of nanomaterials for the development of innovative electrical sensors and nanodevices for environmental monitoring.","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":null,"pages":null},"PeriodicalIF":4.2,"publicationDate":"2024-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"40639208","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Insights on the Extraction and Analysis of Phenolic Compounds from Citrus Fruits: Green Perspectives and Current Status. 从柑橘类水果中提取和分析酚类化合物的启示：绿色前景与现状。

IF 4.2 2区化学

Critical reviews in analytical chemistry Pub Date : 2024-08-01 Epub Date: 2022-08-22 DOI: 10.1080/10408347.2022.2107871

Vitor L Sanches, Leonardo M de Souza Mesquita, Juliane Viganó, Letícia S Contieri, Rodrigo Pizani, Jaísa Chaves, Laíse Capelasso da Silva, Mariana Corrêa de Souza, Marcia Cristina Breitkreitz, Maurício A Rostagno

{"title":"Insights on the Extraction and Analysis of Phenolic Compounds from Citrus Fruits: Green Perspectives and Current Status.","authors":"Vitor L Sanches, Leonardo M de Souza Mesquita, Juliane Viganó, Letícia S Contieri, Rodrigo Pizani, Jaísa Chaves, Laíse Capelasso da Silva, Mariana Corrêa de Souza, Marcia Cristina Breitkreitz, Maurício A Rostagno","doi":"10.1080/10408347.2022.2107871","DOIUrl":"10.1080/10408347.2022.2107871","url":null,"abstract":"Citrus fruits (CF) are highly consumed worldwide, fresh, processed, or prepared as juices and pies. To illustrate the high economic importance of CF, the global production of these commodities in 2021 was around 98 million tons. CF's composition is considered an excellent source of phenolic compounds (PC) as they have a large amount and variety. Since ancient times, PC has been highlighted to promote several benefits related to oxidative stress disorders, such as chronic diseases and cancer. Recent studies suggest that consuming citrus fruits can prevent some of these diseases. However, due to the complexity of citrus matrices, extracting compounds of interest from these types of samples, and identifying and quantifying them effectively, is not a simple task. In this context, several extractive and analytical proposals have been used. This review discusses current research involving CF, focusing mainly on PC extraction and analysis methods, regarding advantages and disadvantages from the perspective of Green Chemistry.","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":null,"pages":null},"PeriodicalIF":4.2,"publicationDate":"2024-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"40434261","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

A Journey from the Drops of Mercury to the Mysterious Shores of the Brain: The 100-Year Adventure of Voltammetry. 从水滴到大脑神秘海岸的旅程：伏安法的百年探险。

IF 4.2 2区化学

Critical reviews in analytical chemistry Pub Date : 2024-08-01 Epub Date: 2022-08-22 DOI: 10.1080/10408347.2022.2113760

Zühre Şentürk

{"title":"A Journey from the Drops of Mercury to the Mysterious Shores of the Brain: The 100-Year Adventure of Voltammetry.","authors":"Zühre Şentürk","doi":"10.1080/10408347.2022.2113760","DOIUrl":"10.1080/10408347.2022.2113760","url":null,"abstract":"Voltammetry, which is at the core of electroanalytical chemistry, is an analytical method that investigates and evaluates the current-potential relationship obtained at a given working electrode. If it is used dropping mercury as working electrode, the method is called as polarography. The current year 2022 marks the 100th anniversary of the discovery of polarography by Czech Jaroslav Heyrovský. He received the Nobel Prize in Chemistry in 1959 for this discovery and his contribution to the scientific world. A hundred years, within the endless existence of the universe is maybe nothing. A hundred years, in the history of mankind is a line, maybe a short paragraph. But, in science, a hundred years can lead to very significant advances in a field and often to the birth and establishment of an entirely new scientific discipline. Indeed, in the last hundred years, the design and use of new electrochemical devices, depending on the progress in microelectronics and computer technologies, has almost revolutionized voltammetry. Besides these developments, due to the fact that the redox (oxidation/reduction) process is very basic for living organisms; the voltammetry, especially with the beginning of the 21st century, has started to be used as a very powerful tool in neuroscience to solve the mystery of the brain (the basic problems of biomolecules with physiological and genetic importance in brain tissue). This review article is an overview of the 100-year history and fascinating development of voltammetry from Heyrovský to the present.","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":null,"pages":null},"PeriodicalIF":4.2,"publicationDate":"2024-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"40631622","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Impurities in Active Pharmaceutical Ingredients and Drug Products: A Critical Review. 活性药物成分和药物产品中的杂质：批判性评论》。

IF 4.2 2区化学

Critical reviews in analytical chemistry Pub Date : 2024-07-26 DOI: 10.1080/10408347.2024.2384046

Cleydson Finotti Cordeiro, Lucas Lopardi Franco, Diogo Teixeira Carvalho, Rudy Bonfilio

{"title":"Impurities in Active Pharmaceutical Ingredients and Drug Products: A Critical Review.","authors":"Cleydson Finotti Cordeiro, Lucas Lopardi Franco, Diogo Teixeira Carvalho, Rudy Bonfilio","doi":"10.1080/10408347.2024.2384046","DOIUrl":"https://doi.org/10.1080/10408347.2024.2384046","url":null,"abstract":"The presence of impurities in active pharmaceutical ingredients (APIs) and drug products represents a risk to patients' health. Such substances are related to diverse side effects and may have mutagenic potential. That's why it is necessary to establish acceptable limits for these by-products, to minimize the risk associated with medicinal therapy. This work focused on presenting a critical review of relevant points related to the presence of impurities in pharmaceuticals. The main legislation and guidelines from the FDA, EMA, ICH, and Pharmacopeias about the subject were evaluated, and recent articles related to the topic were searched in Scopus, ScienceDirect, PubMed, and Web of Science from 2013 to 2023. Additionally, the analytical techniques used for quantifying impurities were discussed, along with relevant tests for assessing the toxicological and mutagenic risks of these by-products. Recent legislation, including ICH Q3A (R2), ICH Q3B (R2), ICH M7 (R2), ICH Q3D (R2), ICH Q3C (R9), ICH Q3E, ICH Q6A, ICH M3 (R2), as well as FDA and EMA guidelines, highlights a comprehensive and effective framework for controlling impurities in pharmaceuticals. Despite this, there remains a lack of harmonization and standardized procedures across different regions. From the review of scientific literature, we observed that advancements in analytical techniques have significantly improved the sensitivity and selectivity in detecting impurities and degradation products. This underscores the ongoing commitment of health agencies and the pharmaceutical industry to ensure the safety and efficacy of medicinal products.","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":null,"pages":null},"PeriodicalIF":4.2,"publicationDate":"2024-07-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141765683","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

2D MXene-Based Nanoscale Materials for Electrochemical Sensing Toward the Detection of Hazardous Pollutants: A Perspective. 用于电化学传感以检测有害污染物的二维 MXene 纳米材料：透视。

IF 4.2 2区化学

Critical reviews in analytical chemistry Pub Date : 2024-07-24 DOI: 10.1080/10408347.2024.2379851

Tahir Ali Sheikh, Muhammad Ismail, Muhammad Fazle Rabbee, Hira Khan, Ayesha Rafique, Zeerak Rasheed, Amna Siddique, Muhammad Zeeshan Rafiq, Zafar A K Khattak, Shehzada Muhammad Sajid Jillani, Umer Shahzad, Muhammad Nadeem Akhtar, Mohsin Saeed, Khalid A Alzahrani, Jamal Uddin, Mohammed M Rahman, Francis Verpoort

{"title":"2D MXene-Based Nanoscale Materials for Electrochemical Sensing Toward the Detection of Hazardous Pollutants: A Perspective.","authors":"Tahir Ali Sheikh, Muhammad Ismail, Muhammad Fazle Rabbee, Hira Khan, Ayesha Rafique, Zeerak Rasheed, Amna Siddique, Muhammad Zeeshan Rafiq, Zafar A K Khattak, Shehzada Muhammad Sajid Jillani, Umer Shahzad, Muhammad Nadeem Akhtar, Mohsin Saeed, Khalid A Alzahrani, Jamal Uddin, Mohammed M Rahman, Francis Verpoort","doi":"10.1080/10408347.2024.2379851","DOIUrl":"https://doi.org/10.1080/10408347.2024.2379851","url":null,"abstract":"MXenes (Mn+1XnTx), a subgroup of 2-dimensional (2D) materials, specifically comprise transition metal carbides, nitrides, and carbonitrides. They exhibit exceptional electrocatalytic and photocatalytic properties, making them well-suited for the detection and removal of pollutants from aqueous environments. Because of their high surface area and remarkable properties, they are being utilized in various applications, including catalysis, sensing, and adsorption, to combat pollution and mitigate its adverse effects. Different characterization techniques like XRD, SEM, TEM, UV-Visible spectroscopy, and Raman spectroscopy have been used for the structural elucidation of 2D MXene. Current responses against applied potential were measured during the electrochemical sensing of the hazardous pollutants in an aqueous system using a variety of electroanalytical techniques, including differential pulse voltammetry, amperometry, square wave anodic stripping voltammetry, etc. In this review, a comprehensive discussion on structural patterns, synthesis, properties of MXene and their application for electrochemical detection of lethal pollutants like hydroquionone, phenol, catechol, mercury and lead, etc. are presented. This review will be helpful to critically understand the methods of synthesis and application of MXenes for the removal of environmental pollutants.","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":null,"pages":null},"PeriodicalIF":4.2,"publicationDate":"2024-07-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141757651","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Latest Developments in Direct and Non-Direct LC-MS Methods Based on Liquid Electron Ionization (LEI). 基于液体电子电离 (LEI) 的直接和非直接 LC-MS 方法的最新发展。

IF 4.2 2区化学

Critical reviews in analytical chemistry Pub Date : 2024-07-24 DOI: 10.1080/10408347.2024.2381543

Genny Grasselli, Adriana Arigò, Pierangela Palma, Giorgio Famiglini, Achille Cappiello

{"title":"Latest Developments in Direct and Non-Direct LC-MS Methods Based on Liquid Electron Ionization (LEI).","authors":"Genny Grasselli, Adriana Arigò, Pierangela Palma, Giorgio Famiglini, Achille Cappiello","doi":"10.1080/10408347.2024.2381543","DOIUrl":"https://doi.org/10.1080/10408347.2024.2381543","url":null,"abstract":"Mass spectrometry (MS) enables precise identification and quantification of molecules, particularly when combined with chromatography. The advent of atmospheric pressure ionization (API) techniques allowed the efficient coupling of liquid chromatography with MS (LC-MS), extending analyses to nonvolatile and thermolabile compounds. API techniques present limitations such as low informative capacity and reproducibility of mass spectra, increasing instrument complexity and costs. Other challenges include analyzing poorly polar molecules and matrix effects (ME), which negatively impact quantitative analyses, necessitating extensive sample purification or using expensive labeled standards. These limitations prompted the exploration of alternative solutions, leading to the development of the Liquid Electron Ionization (LEI) interface. The system has demonstrated excellent robustness and reproducibility. LEI has been employed to analyze various compounds, including pesticides, drugs of abuse, phenols, polycyclic aromatic hydrocarbons (PAHs), phthalates, and many others. Its versatility has been validated with single quadrupole, triple quadrupole, and QToF detectors, operating in electron ionization (EI) or chemical ionization (CI) modes and with both reverse phase liquid chromatography (RPLC) and normal phase liquid chromatography (NPLC). LEI has also been successfully integrated with the Microfluidic Open Interface (MOI), Membrane Introduction Mass Spectrometry (MIMS), and Microfluidic Water-Assisted Trap Focusing (M-WATF), broadening its application scope and consistently demonstrating promising results in terms of sensitivity and identification power. The most recent advancement is the development of Extractive-Liquid Sampling Electron Ionization-Mass Spectrometry (E-LEI-MS), a surface sampling and real-time analysis technique based on the LEI concept. This review article offers a comprehensive and up-to-date picture of the potential of LEI.","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":null,"pages":null},"PeriodicalIF":4.2,"publicationDate":"2024-07-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141751287","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Food Additives and Evolved Methods of Detection: A Review. 食品添加剂和检测方法的演变：综述。

IF 4.2 2区化学

Critical reviews in analytical chemistry Pub Date : 2024-07-17 DOI: 10.1080/10408347.2024.2372501

Aiswarya P S, Ditto Abraham Thadathil, Louis George, Anitha Varghese

引用次数: 0