Critical reviews in analytical chemistry最新文献

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Recent Approaches for Analytical Characterization of Phospholipids in Food Matrices. Is the Phospholipid Fraction Exploited in the Authentication of Food Lipids? 食品基质中磷脂分析表征的最新方法。磷脂组分在食品油脂鉴定中有应用吗?
IF 4.2 2区 化学
Critical reviews in analytical chemistry Pub Date : 2025-01-01 Epub Date: 2023-10-08 DOI: 10.1080/10408347.2023.2264981
Rosalía López-Ruiz, Ana M Jimenez-Carvelo, Luis Cuadros-Rodríguez
{"title":"Recent Approaches for Analytical Characterization of Phospholipids in Food Matrices. Is the Phospholipid Fraction Exploited in the Authentication of Food Lipids?","authors":"Rosalía López-Ruiz, Ana M Jimenez-Carvelo, Luis Cuadros-Rodríguez","doi":"10.1080/10408347.2023.2264981","DOIUrl":"10.1080/10408347.2023.2264981","url":null,"abstract":"<p><p>Phospholipids (PhLs) are essential components of cell membranes, characterized by a hydrophobic tail and a hydrophilic headgroup. They play several roles in biological systems, including energy storage, protection, and antioxidant properties. PhLs are found naturally in foods such as egg yolks, milk, or vegetable oils. The composition and concentration of PhLs observed in these foods vary according to the analytical methodology applied, mainly in the extraction and sample treatment process. Analytical targeted approaches for characterized PhLs involve liquid chromatography and mass spectrometry techniques. These methods provide insights into the composition and content of PhLs in food matrices. However, there is limited research on using PhL profiles for food quality evaluation and authentication purposes. Untargeted approaches, such as fingerprinting, have the potential to assess the authenticity of food products by capturing analytical signals linked to the PhL fraction. This review focusses on recent analytical strategies used in characterizing PhLs in distinctive foodstuffs (eggs, milk, and vegetable oils). It discusses sample preparation, analytical separation, and detection techniques. The review also highlights the potential of multivariate approaches to incorporate information on PhL composition to assess the authenticity of food products, an area that has been largely overlooked in previous studies.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":" ","pages":"99-108"},"PeriodicalIF":4.2,"publicationDate":"2025-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41127224","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Mass Spectrometry Based on Chemical Derivatization Has Brought Novel Discoveries to Lipidomics: A Comprehensive Review. 基于化学衍生的质谱法给脂质组学带来了新的发现:综述。
IF 4.2 2区 化学
Critical reviews in analytical chemistry Pub Date : 2025-01-01 Epub Date: 2023-10-02 DOI: 10.1080/10408347.2023.2261130
Dan Wang, Huaming Xiao, Xin Lv, Hong Chen, Fang Wei
{"title":"Mass Spectrometry Based on Chemical Derivatization Has Brought Novel Discoveries to Lipidomics: A Comprehensive Review.","authors":"Dan Wang, Huaming Xiao, Xin Lv, Hong Chen, Fang Wei","doi":"10.1080/10408347.2023.2261130","DOIUrl":"10.1080/10408347.2023.2261130","url":null,"abstract":"<p><p>Lipids, as one of the most important organic compounds in organisms, are important components of cells and participate in energy storage and signal transduction of living organisms. As a rapidly rising field, lipidomics research involves the identification and quantification of multiple classes of lipid molecules, as well as the structure, function, dynamics, and interactions of lipids in living organisms. Due to its inherent high selectivity and high sensitivity, mass spectrometry (MS) is the \"gold standard\" analysis technique for small molecules in biological samples. The combination chemical derivatization with MS detection is a unique strategy that could improve MS ionization efficiency, facilitate structure identification and quantitative analysis. Herein, this review discusses derivatization-based MS strategies for lipidomic analysis over the past decade and focuses on all the reported lipid categories, including fatty acids and modified fatty acids, glycerolipids, glycerophospholipids, sterols and saccharolipids. The functional groups of lipids mainly involved in chemical derivatization include the C=C group, carboxyl group, hydroxyl group, amino group, carbonyl group. Furthermore, representative applications of these derivatization-based lipid profiling methods were summarized. Finally, challenges and countermeasures of lipid derivatization are mentioned and highlighted to guide future studies of derivatization-based MS strategy in lipidomics.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":" ","pages":"21-52"},"PeriodicalIF":4.2,"publicationDate":"2025-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41127223","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Recent Advances in Catecholamines Analytical Detection Methods and Their Pretreatment Technologies. 儿茶酚胺分析检测方法及其预处理技术的最新进展。
IF 4.2 2区 化学
Critical reviews in analytical chemistry Pub Date : 2025-01-01 Epub Date: 2023-09-21 DOI: 10.1080/10408347.2023.2258982
Jie Jiang, Meng Zhang, Zhilong Xu, Yali Yang, Yimeng Wang, Hong Zhang, Kai Yu, Guangfeng Kan, Yanxiao Jiang
{"title":"Recent Advances in Catecholamines Analytical Detection Methods and Their Pretreatment Technologies.","authors":"Jie Jiang, Meng Zhang, Zhilong Xu, Yali Yang, Yimeng Wang, Hong Zhang, Kai Yu, Guangfeng Kan, Yanxiao Jiang","doi":"10.1080/10408347.2023.2258982","DOIUrl":"10.1080/10408347.2023.2258982","url":null,"abstract":"<p><p>Catecholamines (CAs), including adrenaline, noradrenaline, and dopamine, are neurotransmitters and hormones that play a critical role in regulating the cardiovascular system, metabolism, and stress response in the human body. As promising methods for real-time monitoring of catecholamine neurotransmitters, LC-MS detectors have gained widespread acceptance and shown significant progress over the past few years. Other detection methods such as fluorescence detection, colorimetric assays, surface-enhanced Raman spectroscopy, and surface plasmon resonance spectroscopy have also been developed to varying degrees. In addition, efficient pretreatment technology for CAs is flourishing due to the increasing development of many highly selective and recoverable materials. There are a few articles that provide an overview of electrochemical detection and efficient enrichment, but a comprehensive summary focusing on analytical detection technology is lacking. Thus, this review provides a comprehensive summary of recent analytical detection technology research on CAs published between 2017 and 2022. The advantages and limitations of relevant methods including efficient pretreatment technologies for biological matrices and analytical methods used in combination with pretreatment technology have been discussed. Overall, this review article provides a better understanding of the importance of accurate CAs measurement and offers perspectives on the development of novel methods for disease diagnosis and research in this field.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":" ","pages":"1-20"},"PeriodicalIF":4.2,"publicationDate":"2025-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41110586","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Recent Advances in Organic Sensors for the Detection of Ag+ Ions: A Comprehensive Review (2019-2023). 检测Ag+离子的有机传感器的最新进展:综述(2019-2023)。
IF 4.2 2区 化学
Critical reviews in analytical chemistry Pub Date : 2025-01-01 Epub Date: 2023-10-04 DOI: 10.1080/10408347.2023.2263877
Mubark Alshareef
{"title":"Recent Advances in Organic Sensors for the Detection of Ag<sup>+</sup> Ions: A Comprehensive Review (2019-2023).","authors":"Mubark Alshareef","doi":"10.1080/10408347.2023.2263877","DOIUrl":"10.1080/10408347.2023.2263877","url":null,"abstract":"<p><p>Recently, organic sensors for the detection of Ag<sup>+</sup> and other metal ions have experienced significant advancements. This is because there is a growing demand for reliable and sensitive tools to monitor various environmental pollutants. Organic sensors have O-, S-, and N-donor atoms, which can act as a ligand and coordinate with different metal ions, hence stabilizing them in a variety of oxidation states. This interaction gives colorimetric and fluorescence changes, which are used to monitor Ag<sup>+</sup> and other metal ions. This comprehensive review highlights the latest developments in organic sensors for the recognition of Ag<sup>+</sup>. We present an in-depth analysis of the underlying principles and mechanisms governing Ag<sup>+</sup> ion recognition. Various organic sensing platforms, such as fluorescent and colorimetric sensors, are discussed, shedding light on their unique advantages and limitations. Special attention is given to the diverse range of organic ligands, receptors, and functional materials used to achieve high sensitivity, selectivity, and quantification accuracy. Additionally, we delve into real-world applications of organic sensors for Ag<sup>+</sup> ion detection, examining their performance in complex matrices such as biological, environmental, industrial and agricultural matrices.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":" ","pages":"83-98"},"PeriodicalIF":4.2,"publicationDate":"2025-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41111328","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
A Review of Electrochemical Techniques for Corrosion Monitoring - Fundamentals and Research Updates. 电化学腐蚀监测技术综述——基础和研究进展。
IF 4.2 2区 化学
Critical reviews in analytical chemistry Pub Date : 2025-01-01 Epub Date: 2023-10-25 DOI: 10.1080/10408347.2023.2267671
Sheetal, Sheetal Kundu, Sanjeeve Thakur, Ashish Kumar Singh, Manjeet Singh, Balaram Pani, Viswanathan S Saji
{"title":"A Review of Electrochemical Techniques for Corrosion Monitoring - Fundamentals and Research Updates.","authors":"Sheetal, Sheetal Kundu, Sanjeeve Thakur, Ashish Kumar Singh, Manjeet Singh, Balaram Pani, Viswanathan S Saji","doi":"10.1080/10408347.2023.2267671","DOIUrl":"10.1080/10408347.2023.2267671","url":null,"abstract":"<p><p>Interculturally, corrosion has been counted as one of the most expensive factors toward the retrogression of concrete and metallic structures resulting in huge monetary losses and unanticipated loss of life. To a large extent, corrosion-related catastrophes can be avoided by having the ability to monitor corrosion before structural integrity is jeopardized. This paper critically reviews the various accustomed electrochemical techniques utilized for corrosion monitoring in terms of their definition, timeline, experimental set-up, advantages, and shortcomings. Additionally, literature exploiting these techniques as their corrosion detection technique has been focused on here. Furthermore, a comparison between recently reported methods has been made to provide better insights into the research progress in this arena.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":" ","pages":"161-186"},"PeriodicalIF":4.2,"publicationDate":"2025-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"50161022","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Advances in Optical Probes for the Detection of Hydrazine in Environmental and Biological Systems. 用于检测环境和生物系统中肼的光学探针的进展。
IF 4.2 2区 化学
Critical reviews in analytical chemistry Pub Date : 2025-01-01 Epub Date: 2023-10-10 DOI: 10.1080/10408347.2023.2261546
Lun Zhang, Lijuan Cheng
{"title":"Advances in Optical Probes for the Detection of Hydrazine in Environmental and Biological Systems.","authors":"Lun Zhang, Lijuan Cheng","doi":"10.1080/10408347.2023.2261546","DOIUrl":"10.1080/10408347.2023.2261546","url":null,"abstract":"<p><p>Hydrazine, as a crucial raw material in the fine chemical industry, plays an indispensable role in fuel, catalyst, pesticide and drug synthesis. Due to its good water solubility and high toxicity, hydrazine can cause irreparable damage to water and soil in the environment, and it can also be released by taking certain drugs, which brings potential risks to human health. Therefore, it is vital to develop a method that can specifically detect hydrazine in the environment and <i>in vivo</i>. As an effective analysis and detection tool, fluorescence probe has attracted extensive attention in recent years. In this review, we summarized and classified hydrazine fluorescence probes based on various reaction mechanisms, and discussed their structures and applications in the past ten years. At least, we briefly outline the challenges and prospects in this field.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":" ","pages":"53-82"},"PeriodicalIF":4.2,"publicationDate":"2025-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41194055","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Factors Affecting the Extraction of (Poly)Phenols from Natural Resources Using Deep Eutectic Solvents Combined with Ultrasound-Assisted Extraction. 深层共晶溶剂与超声辅助萃取相结合从自然资源中提取(聚)酚的影响因素。
IF 4.2 2区 化学
Critical reviews in analytical chemistry Pub Date : 2025-01-01 Epub Date: 2023-10-18 DOI: 10.1080/10408347.2023.2266846
Shahida Anusha Siddiqui, Ali Ali Redha, Molla Salauddin, Iskandar Azmy Harahap, H P Vasantha Rupasinghe
{"title":"Factors Affecting the Extraction of (Poly)Phenols from Natural Resources Using Deep Eutectic Solvents Combined with Ultrasound-Assisted Extraction.","authors":"Shahida Anusha Siddiqui, Ali Ali Redha, Molla Salauddin, Iskandar Azmy Harahap, H P Vasantha Rupasinghe","doi":"10.1080/10408347.2023.2266846","DOIUrl":"10.1080/10408347.2023.2266846","url":null,"abstract":"<p><p>Replacing conventional solvents with deep eutectic solvents (DES) has shown promising effects on the extraction yield of (poly)phenols. DES can be combined with ultrasound-assisted extraction (UAE) to further increase the extraction efficiency of (poly)phenols from natural resources compared to conventional methods. This review discusses the factors associated with DES (composition, solvent-to-sample ratio, extraction duration, and temperature) and UAE (ultrasound frequency, power, intensity, and duty cycle) methods that influence the extraction of (poly)phenols and informs future improvements required in the optimization of the extraction process. For the optimum (poly)phenol extraction from natural resources, the following parameters shall be considered: ultrasound frequency should be in the range of 20-50 kHz, ultrasound intensity in the range of 60-120 W/cm<sup>2</sup>, ultrasound duty cycle in the range of 40-80%, ultrasound duration for 10-30 minutes, and ultrasound temperature for 25-50 °C. Among the reported DES systems, choline chloride with glycerol or lactic acid, with a solvent-to-sample mass ratio of 10-30:1 shown to be effective. The solvent composition and solvent-to-sample mass ratio should be selected according to the target compound and the source material. However, the high viscosity of DES is among the major limitations. Optimizing these factors can help to increase the yield of extracted (poly)phenols and their applications.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":" ","pages":"139-160"},"PeriodicalIF":4.2,"publicationDate":"2025-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41233058","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Mass Spectrometry Analysis for Clinical Applications: A Review. 质谱分析的临床应用:综述。
IF 4.2 2区 化学
Critical reviews in analytical chemistry Pub Date : 2025-01-01 Epub Date: 2023-11-01 DOI: 10.1080/10408347.2023.2274039
Hong Zhang, Yali Yang, Yanxiao Jiang, Meng Zhang, Zhilong Xu, Xiaofei Wang, Jie Jiang
{"title":"Mass Spectrometry Analysis for Clinical Applications: A Review.","authors":"Hong Zhang, Yali Yang, Yanxiao Jiang, Meng Zhang, Zhilong Xu, Xiaofei Wang, Jie Jiang","doi":"10.1080/10408347.2023.2274039","DOIUrl":"10.1080/10408347.2023.2274039","url":null,"abstract":"<p><p>Mass spectrometry (MS) has become an attractive analytical method in clinical analysis due to its comprehensive advantages of high sensitivity, high specificity and high throughput. Separation techniques coupled MS detection (e.g., LC-MS/MS) have shown unique advantages over immunoassay and have developed as golden criterion for many clinical applications. This review summarizes the characteristics and applications of MS, and emphasizes the high efficiency of MS in clinical research. In addition, this review also put forward further prospects for the future of mass spectrometry technology, including the introduction of miniature MS instruments, point-of-care detection and high-throughput analysis, to achieve better development of MS technology in various fields of clinical application. Moreover, as ambient ionization mass spectrometry (AIMS) requires little or no sample pretreatment and improves the flux of MS, this review also summarizes its potential applications in clinic.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":" ","pages":"213-232"},"PeriodicalIF":4.2,"publicationDate":"2025-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"71421377","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Unlocking the Hidden Depths: Multi-Modal Integration of Imaging Mass Spectrometry-Based and Molecular Imaging Techniques. 解开隐藏的深度:基于成像质谱和分子成像技术的多模集成。
IF 4.2 2区 化学
Critical reviews in analytical chemistry Pub Date : 2025-01-01 Epub Date: 2023-10-17 DOI: 10.1080/10408347.2023.2266838
Behnaz Akbari, Bertrand Russell Huber, Janet Hope Sherman
{"title":"Unlocking the Hidden Depths: Multi-Modal Integration of Imaging Mass Spectrometry-Based and Molecular Imaging Techniques.","authors":"Behnaz Akbari, Bertrand Russell Huber, Janet Hope Sherman","doi":"10.1080/10408347.2023.2266838","DOIUrl":"10.1080/10408347.2023.2266838","url":null,"abstract":"<p><p>Multimodal imaging (MMI) has emerged as a powerful tool in clinical research, combining different imaging modes to acquire comprehensive information and enabling scientists and surgeons to study tissue identification, localization, metabolic activity, and molecular discovery, thus aiding in disease progression analysis. While multimodal instruments are gaining popularity, challenges such as non-standardized characteristics, custom software, inadequate commercial support, and integration issues with other instruments need to be addressed. The field of multimodal imaging or multiplexed imaging allows for simultaneous signal reproduction from multiple imaging strategies. Intraoperatively, MMI can be integrated into frameless stereotactic surgery. Recent developments in medical imaging modalities such as magnetic resonance imaging (MRI), and Positron Emission Topography (PET) have brought new perspectives to multimodal imaging, enabling early cancer detection, molecular tracking, and real-time progression monitoring. Despite the evidence supporting the role of MMI in surgical decision-making, there is a need for comprehensive studies to validate and perform integration at the intersection of multiple imaging technologies. They were integrating mass spectrometry-based technologies (e.g., imaging mass spectrometry (IMS), imaging mass cytometry (IMC), and Ion mobility mass spectrometry ((IM-IM) with medical imaging modalities, offering promising avenues for molecular discovery and clinical applications. This review emphasizes the potential of multi-omics approaches in tissue mapping using MMI integrated into desorption electrospray ionization (DESI) and matrix-assisted laser desorption ionization (MALDI), allowing for sequential analyses of the same section. By addressing existing knowledge gaps, this review encourages future research endeavors toward multi-omics approaches, providing a roadmap for future research and enhancing the value of MMI in molecular pathology for diagnosis.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":" ","pages":"109-138"},"PeriodicalIF":4.2,"publicationDate":"2025-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41233059","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Analytical Methods for the Determination of Quercetin and Quercetin Glycosides in Pharmaceuticals and Biological Samples. 药物和生物样品中槲皮素和槲皮素糖苷的测定分析方法。
IF 4.2 2区 化学
Critical reviews in analytical chemistry Pub Date : 2025-01-01 Epub Date: 2023-10-29 DOI: 10.1080/10408347.2023.2269421
Fotouh R Mansour, Inas A Abdallah, Alaa Bedair, Mahmoud Hamed
{"title":"Analytical Methods for the Determination of Quercetin and Quercetin Glycosides in Pharmaceuticals and Biological Samples.","authors":"Fotouh R Mansour, Inas A Abdallah, Alaa Bedair, Mahmoud Hamed","doi":"10.1080/10408347.2023.2269421","DOIUrl":"10.1080/10408347.2023.2269421","url":null,"abstract":"<p><p>Flavonoids are plant-derived compounds that have several health benefits, including antioxidative, anti-inflammatory, anti-mutagenic, and anti-carcinogenic effects. Quercetin is a flavonoid that is widely present in various fruits, vegetables, and drinks. Accurate determination of quercetin in different samples is of great importance for its potential health benefits. This review, is an overview of sample preparation and determination methods for quercetin in diverse matrices. Previous research on sample preparation and determination methods for quercetin are summarized, highlighting the advantages and disadvantages of each method and providing insights into recent developments in quercetin sample treatment. Various analytical techniques are discussed including spectroscopic, chromatographic, electrophoretic, and electrochemical methods for the determination of quercetin and its derivatives in different samples. UV-Vis (Ultraviolet-visible) spectrophotometry is simple and inexpensive but lacks selectivity. Chromatographic techniques (HPLC, GC) offer selectivity and sensitivity, while electrophoretic and electrochemical methods provide high resolution and low detection limits, respectively. The aim of this review is to comprehensively explore the determination methods for quercetin and quercetin glycosides in diverse matrices, with emphasis on pharmaceutical and biological samples. The review also provides a theoretical basis for method development and application for the analysis of quercetin and quercetin glycosides in real samples.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":" ","pages":"187-212"},"PeriodicalIF":4.2,"publicationDate":"2025-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"71411025","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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