{"title":"Progress in the Development of Imidazopyridine-Based Fluorescent Probes for Diverse Applications.","authors":"Preeti AshokKumar Chaudhran, Abha Sharma","doi":"10.1080/10408347.2022.2158720","DOIUrl":"10.1080/10408347.2022.2158720","url":null,"abstract":"<p><p>Different classes of Imidazopyridine i.e., Imidazo[1,2-<i>a</i>]pyridine, Imidazo[1,5-<i>a</i>] pyridine, Imidazo[4,5-<i>b</i>]pyridine, have shown versatile applications in various fields. In this review, we have concisely presented the usefulness of the fluorescent property of imidazopyridine in different fields such as imaging tools, optoelectronics, metal ion detection, etc. Fluorescence mechanisms such as excited state intramolecular proton transfer, photoinduced electron transfer, fluorescence resonance energy transfer, intramolecular charge transfer, etc. are incorporated in the designed fluorophore to make it for fluorescent applications. It has been widely employed for metal ion detection, where selective metal ion detection is possible with triazole-attached imidazopyridine, β-carboline imidazopyridine hybrid, quinoline conjugated imidazopyridine, and many more. Also, other popular applications involve organic light emitting diodes and cell imaging. This review shed a light on recent development in this area especially focusing on the optical properties of the molecules with their usage which would be helpful in designing application-based new imidazopyridine derivatives.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":" ","pages":"2148-2165"},"PeriodicalIF":4.2,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10500765","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Vibrational Spectroscopy Combined with Chemometrics in Authentication of Functional Foods.","authors":"Fengjiao Li, Jinyu Zhang, Yuanzhong Wang","doi":"10.1080/10408347.2022.2073433","DOIUrl":"10.1080/10408347.2022.2073433","url":null,"abstract":"<p><p>Many foods have both edible and medical importance and are appreciated as functional foods, preventing diseases. However, due to unscrupulous vendors and imperfect market supervision mechanisms, curative foods are prone to adulteration or some other events that harm the interests of consumers. However, traditional analytical methods are unsuitable and expensive for a broad and complex application. Therefore, people urgently need a fast, efficient, and accurate detection method to protect self-interests. Recently, the study of target samples by vibration spectrum shows strong qualitative and quantitative ability. The model established by platform technology combined with the stoichiometric analysis method can obtain better parameters, which it has good robustness and can detect functional food efficiently, quickly and nondestructive. The review compared and prospect five different vibrational spectroscopic techniques (near-infrared, Fourier transform infrared, Raman, hyperspectral imaging spectroscopy and Terahertz spectroscopy). In order to better solve some of the actual situations faced by certification, we explore and through relevant research and investigation to appropriately highlight the applicability and importance of technology combined with chemometrics in functional food authentication. There are four categories of authentication discussed: functional food authenticated in source, processing method, fraud and ingredient ratio. This paper provides an innovative process for the authentication of functional food, which has a meaningful reference value for future review or scientific research of relevant departments.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":"1 1","pages":"333-354"},"PeriodicalIF":5.0,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"47166350","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Carbon Dots in the Detection of Pathogenic Bacteria and Viruses.","authors":"Erhan Zor, Fariba Mollarasouli, Leyla Karadurmus, Goksu Ozcelikay, Sibel A Ozkan","doi":"10.1080/10408347.2022.2072168","DOIUrl":"10.1080/10408347.2022.2072168","url":null,"abstract":"<p><p>Bacterial and viruses pathogens are a significant hazard to human safety and health. In the imaging and detection of pathogenic microorganisms, the application of fluorescent nanoparticles is very useful. Carbon dots and quantum dots are preferred in this regard as labels, amplifiers, and/or electrode modifiers because of their outstanding features. However, precise diagnostics to identify numerous harmful bacteria simultaneously still face considerable hurdles, yet it is an inevitable issue. With the growing development of biosensors, nanoproduct-based bio-sensing has recently become one of the most promising methods for accurately identifying and quantifying various pathogens at low cost, high sensitivity, and selectivity, with time savings. The most recent applications of carbon dots in optical and electrochemical-based sensors are discussed in this review, along with some examples of pathogen sensors.HighlightsSimultaneous and early detection of pathogens is a critical issue in the management of readily spread to prevent epidemics.Carbon dots-based biosensors are more preferred in detection of pathogens due to high selectivity and sensitivity, as well as quick and cheap point-of-care platform.Summary of recent advances in the design of optical and electrochemical biosensors for the detection of pathogens.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":"1 1","pages":"219-246"},"PeriodicalIF":5.0,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"46482592","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Mohsen A M Alhamami, Jari S Algethami, Sikandar Khan
{"title":"A Review on Thiazole Based Colorimetric and Fluorimetric Chemosensors for the Detection of Heavy Metal Ions.","authors":"Mohsen A M Alhamami, Jari S Algethami, Sikandar Khan","doi":"10.1080/10408347.2023.2197073","DOIUrl":"10.1080/10408347.2023.2197073","url":null,"abstract":"<p><p>Thiazole and its derivatives play an important role in biological and non-biological fields due to several structural and electronic behaviors associated with it. Thiazole derivatives act as chemosensors because they formed metal complexes upon interacting with various heavy metal ions like Cd<sup>2+</sup>, Co<sup>2+</sup>, Cr<sup>3+</sup>, Fe<sup>3+</sup>, Ag<sup>+</sup>, Al<sup>3+</sup>, Cu<sup>2+</sup>, Pd<sup>2+</sup>, Hg<sup>2+</sup>, Ni<sup>2+</sup>, Ga<sup>3+</sup>, In<sup>3+</sup>, Sn<sup>4+</sup>, Pb<sup>2+</sup>, Zn<sup>2+</sup> as well as other cations. These metal ions are of prime importance from the environmental point of view with high. This review article focuses on the thiazole-based colorimetric as well as fluorometric sensor for the recognition of different heavy metal cations in various specimens like agricultural, biological, and environmental. It also summarizes the binding stoichiometry, detection limit, pH, structure, and practical application of the reported thiazole-based chemosensors. Further, the sensing performances, have been discussed and compared with some reported organic sensors.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":" ","pages":"2689-2713"},"PeriodicalIF":4.2,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"9629067","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Bogusław Buszewski, Dominika Błońska, Ewa Kłodzińska, Marek Konop, Anna Kubesová, Jiří Šalplachta
{"title":"Determination of Pathogens by Electrophoretic and Spectrometric Techniques.","authors":"Bogusław Buszewski, Dominika Błońska, Ewa Kłodzińska, Marek Konop, Anna Kubesová, Jiří Šalplachta","doi":"10.1080/10408347.2023.2219748","DOIUrl":"10.1080/10408347.2023.2219748","url":null,"abstract":"<p><p>In modern medical diagnostics, where analytical chemistry plays a key role, fast and accurate identification of pathogens is becoming increasingly important. Infectious diseases pose a growing threat to public health due to population growth, international air travel, bacterial resistance to antibiotics, and other factors. For instance, the detection of SARS-CoV-2 in patient samples is a key tool to monitor the spread of the disease. While there are several techniques for identifying pathogens by their genetic code, most of these methods are too expensive or slow to effectively analyze clinical and environmental samples that may contain hundreds or even thousands of different microbes. Standard approaches (e.g., culture media and biochemical assays) are known to be very time- and labor-intensive. The purpose of this review paper is to highlight the problems associated with the analysis and identification of pathogens that cause many serious infections. Special attention was paid to the description of mechanisms and the explanation of the phenomena and processes occurring on the surface of pathogens as biocolloids (charge distribution). This review also highlights the importance of electromigration techniques and demonstrates their potential for pathogen pre-separation and fractionation and demonstrates the use of spectrometric methods, such as MALDI-TOF MS, for their detection and identification.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":" ","pages":"2960-2983"},"PeriodicalIF":4.2,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"9631302","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Ebaa Adnan Azooz, Mustafa Tuzen, Wael I Mortada, Naeem Ullah
{"title":"A critical review of selected preconcentration techniques used for selenium determination in analytical samples.","authors":"Ebaa Adnan Azooz, Mustafa Tuzen, Wael I Mortada, Naeem Ullah","doi":"10.1080/10408347.2022.2153579","DOIUrl":"10.1080/10408347.2022.2153579","url":null,"abstract":"<p><p>Selenium (Se) is considered to be an essential trace element needed for all living organisms. The importance, deficiency, and toxic effects of Se mainly depend on its quantity and chemical nature. It has been observed that the inorganic versions of Se are more hazardous than the organic versions. This review is mainly focused on the application of different extraction methods used for Se extraction and determination such as microextraction, solid-phase extraction (SPE), and their modified modes in the last 12 years. The use of different dispersive medium (magnetic field, ultrasonic radiation, and vortex agitator) to enhance Se separation is also part of this review. The usage of environmentally friendly solvents such as supramolecular solvents, hydrophobic deep eutectic solvents (DESs), and ionic liquids (ILs) are also the focus of attention in this review. This review is also emphasized the application of advanced microextraction methods, particularly liquid-phase microextraction (LPME). The most recent advances in LPME extraction techniques for Se in various environmental samples, as well as their prospects, are reviewed. Additionally, a summary of cheap, simple, and accurate techniques that have not yet been used to determine small amounts of Se has been provided.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":" ","pages":"2072-2086"},"PeriodicalIF":4.2,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10369264","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Khrissy Aracélly Reis Medeiros, Livio Garcia da Costa, Gabriela Knippelberg Bifano Manea, Roberta de Moraes Maciel, Ednéia Caliman, Mônica Teixeira da Silva, Rodrigo Caciano de Sena, Elcio Cruz de Oliveira
{"title":"Determination of Total Sulfur Content in Fuels: A Comprehensive and Metrological Review Focusing on Compliance Assessment.","authors":"Khrissy Aracélly Reis Medeiros, Livio Garcia da Costa, Gabriela Knippelberg Bifano Manea, Roberta de Moraes Maciel, Ednéia Caliman, Mônica Teixeira da Silva, Rodrigo Caciano de Sena, Elcio Cruz de Oliveira","doi":"10.1080/10408347.2023.2249564","DOIUrl":"10.1080/10408347.2023.2249564","url":null,"abstract":"<p><p>Sulfur-containing compounds are naturally found in crude oil, and they can be partially removed during the refining process. The wide use of fossil fuels has a significant contribution to sulfur emissions into the atmosphere, and Governments are striving to reduce the amount of the fuels by environmental regulations. The reduction of sulfur levels in diesel and other transportation fuels is beneficial from economic and environmental points, but meeting this standard represents a major operational and economic challenge for the oil and gas industry. Quantitative measurement of the sulfur amount must be taken along the oil refining chains guided by standards of measurement and recommended analytical methods such as various American Society for Testing and Materials methods (ASTM D2622, ASTM D5453, ASTM D7039, and ASTM D7220). Advancement in the refining processes and environmental regulations also require reliable measurements and well-defined criteria for compliance assessment. This work presented a brief review of the ASTM Standards used in the laboratories of the Brazilian oil and gas industry to determine the total sulfur content in fuels. We also presented an approach based on the reproducibility of the measurement methods and the guard band concept to evaluate the conformity statement.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":" ","pages":"3398-3408"},"PeriodicalIF":5.4,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10108616","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Al-Montaser Bellah H Ali, Fatma A M Abdel-Aal, Azza H Rageh, Abdel-Maaboud I Mohamed
{"title":"A Comprehensive Review on Analytical Techniques for Determination of Sex Stimulants, PDE5 Inhibitors in Different Matrices with Special Focus on the Electroanalytical Methods.","authors":"Al-Montaser Bellah H Ali, Fatma A M Abdel-Aal, Azza H Rageh, Abdel-Maaboud I Mohamed","doi":"10.1080/10408347.2022.2152274","DOIUrl":"10.1080/10408347.2022.2152274","url":null,"abstract":"<p><p>Erectile dysfunction (ED) is one of the most common chronic diseases affecting men and its incidence increases with aging. Due to its substantial influence on the quality of life, phosphodiesterase type-5 (PDE5) inhibitors have been implemented to treat ED by increasing the penile blood flow that results in improving erection. PDE5 inhibitors is a class of drugs that affects many pharmacological sectors, and it is essential to review the different analytical methods described for their determination. Few reviews were published concerning this group of drugs. For this reason, this review article gathers the different analytical methods used to determine PDE5 inhibitors in pharmaceutical and biological samples over the past 20 years. Different analytical techniques were used to analyze these compounds in different matrices such as separation methods (capillary electrophoresis, LC-MS, UPLC-MS/MS, and GC-MS), spectroscopic methods (UV-visible methods, FT-IR spectroscopy and spectrofluorometry) and electrochemical methods (polarography, voltammetry and potentiometry). This review focuses on the different electrochemical methods and their use in analytical determination of PDE5 inhibitors in pharmaceutical dosage forms and biological samples. Moreover, it discusses the different modified electrodes used for their electroanalytical determination and the behavior of the studied drugs at different modified electrodes. Additionally, this review discusses the pharmacokinetics of the studied compounds and their interactions with other co-administered drugs especially the metabolic interactions between the studied compounds and other co-administered drugs in different matrices. This literature survey would provide a beneficial guide for future analytical investigation of PDE5 inhibitors.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":" ","pages":"2023-2052"},"PeriodicalIF":4.2,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10319670","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Ali Pourali, Aysa Abbasalizadeh, Mohammad Reza Afshar Mogaddam, Mir Ali Farajzadeh, Mustafa Tuzen, Mahboob Nemati
{"title":"Liquid Phase Microextraction of Hazardous Compounds in Dairy Products; Principal and Practical Aspects.","authors":"Ali Pourali, Aysa Abbasalizadeh, Mohammad Reza Afshar Mogaddam, Mir Ali Farajzadeh, Mustafa Tuzen, Mahboob Nemati","doi":"10.1080/10408347.2023.2204966","DOIUrl":"10.1080/10408347.2023.2204966","url":null,"abstract":"<p><p>Liquid phase microextraction techniques are considered as the miniaturized version of traditional liquid-liquid extraction, which use only several microliters of a proper solvent to extract the analytes from sample. In these methods, the target analytes are migrated into a water-immiscible organic solvent (acceptor phase) from an aqueous sample (donor phase). They are mainly classified into three main groups including (a) single-drop microextraction, (b) dispersive liquid-liquid microextraction, and (c) hollow fiber-liquid phase microextraction. These techniques have been successfully applied to the assessment of different analytes in food samples, pharmaceuticals, beverages, and so on. This review mainly focuses on up-to-date information on the application of liquid phase microextraction techniques in dairy products. The advantages and disadvantages of the developed liquid phase microextraction methods were discussed.</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":" ","pages":"2810-2826"},"PeriodicalIF":5.4,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"9436904","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Said Kinani, Adrien Roumiguières, Stéphane Bouchonnet
{"title":"A Critical Review on Chemical Speciation of Chlorine-Produced Oxidants (CPOs) in Seawater. Part 2: Sampling, Sample Preparation and Non-Chromatographic and Mass Spectrometric-Based Methods.","authors":"Said Kinani, Adrien Roumiguières, Stéphane Bouchonnet","doi":"10.1080/10408347.2022.2135984","DOIUrl":"10.1080/10408347.2022.2135984","url":null,"abstract":"<p><p>Chlorination of seawater forms a range of secondary oxidative species, collectively termed \"chlorine-produced oxidants\" (CPOs). These compounds do not have the same biocidal efficacy, the same fate and behavior in the marine environment, the same potential formation of chlorination by-products (CBPs), nor the same effects on marine organisms. Their chemical speciation is an important step toward an accurate assessment of the effectiveness of chlorination and the potential impacts of its releases, among others. The aim of this paper - which is the second of a trilogy dedicated to the chemical speciation of CPOs in seawater - is to cover all aspects related to CPOs analysis in seawater, from sampling to instrumental determination. First, it discusses the procedures involved in synthesis, storage, and standardization of analytical standards. Second, it deals with sampling and sample preparation, addressing all relevant issues related to these two key steps. Third, it provides a comprehensive and up-to-date overview of the colorimetric, titrimetric, and electrochemical methods used for CPOs determination and thoroughly discusses their advantages and limitations. Finally, this review ends with some recommendations for progress in the field of CPO analysis with the three aforementioned approaches. Chromatographic and mass spectrometric-based methods will be covered in the third and final article (Part III).</p>","PeriodicalId":10744,"journal":{"name":"Critical reviews in analytical chemistry","volume":"1 1","pages":"1851-1870"},"PeriodicalIF":4.2,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41334017","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}