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Advances in Electrocatalyzed Water Oxidation by Molecular Complexes of First Row Transition Metals 第一行过渡金属分子配合物电催化水氧化研究进展。
IF 7 2区 化学
Chemical record Pub Date : 2025-04-24 DOI: 10.1002/tcr.202400266
Chiara Lenzi, Andrea Masetti, Isacco Gualandi, Erika Scavetta, Luca Rigamonti, Rita Mazzoni
{"title":"Advances in Electrocatalyzed Water Oxidation by Molecular Complexes of First Row Transition Metals","authors":"Chiara Lenzi,&nbsp;Andrea Masetti,&nbsp;Isacco Gualandi,&nbsp;Erika Scavetta,&nbsp;Luca Rigamonti,&nbsp;Rita Mazzoni","doi":"10.1002/tcr.202400266","DOIUrl":"10.1002/tcr.202400266","url":null,"abstract":"<p>Energy transition toward sustainable, alternative, and affordable solutions is likely to be one of the major challenges of the anthropocene era. The oxygen evolution reaction (OER) is a pivotal electrocatalytic process essential for advancing renewable energy conversion and storage technologies, including water splitting, artificial photosynthesis, metal-air batteries, and fuel cells. Electrocatalytic pathways can significantly reduce the overall energy requirements of these devices, particularly focusing on the energy demands associated with water splitting for hydrogen production. This review, after introducing the state of the art in heterogeneous catalysis, will be devoted to the description of molecular water oxidation electrocatalysts (MWOCs), focusing on the recent advancements on catalysts composed of various metals, including Mn, Co, Cu, Ni, and Fe, in combination with a range of mono- and multidentate ligands. Critical insights are presented and discussed to provide readers with suggestions for ligand design in assisted catalysis. These observations aim to identify synergistic solutions that could enhance technological maturity by reducing energy absorption while improving stability and efficiency.</p>","PeriodicalId":10046,"journal":{"name":"Chemical record","volume":"25 6","pages":""},"PeriodicalIF":7.0,"publicationDate":"2025-04-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://onlinelibrary.wiley.com/doi/epdf/10.1002/tcr.202400266","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143986503","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
MOF-Based Electrocatalysts for Water Electrolysis, Energy Storage, and Sensing: Progress and Insights 基于mof的电催化剂用于水电解、储能和传感：进展和见解
IF 7 2区 化学
Chemical record Pub Date : 2025-04-24 DOI: 10.1002/tcr.202400253
Tao Pan, Yingying Wang, Sicong Zhang, Dianhui Wang, Qing Li, Huan Pang
{"title":"MOF-Based Electrocatalysts for Water Electrolysis, Energy Storage, and Sensing: Progress and Insights","authors":"Tao Pan,&nbsp;Yingying Wang,&nbsp;Sicong Zhang,&nbsp;Dianhui Wang,&nbsp;Qing Li,&nbsp;Huan Pang","doi":"10.1002/tcr.202400253","DOIUrl":"https://doi.org/10.1002/tcr.202400253","url":null,"abstract":"<p>Metal-organic frameworks (MOFs) and their derivatives have shown broad application prospects in fields such as water electrolysis, electrochemical energy storage, and sensing due to their high specific surface area, tunable structures, and abundant active sites. This article provides a comprehensive overview of our research group′s recent advancements in developing MOF-based electrocatalysts for Oxygen Evolution Reaction (OER) and Urea Oxidation Reaction (UOR) at anodes, as well as Hydrogen Evolution Reaction (HER) at cathodes during water electrolysis. Furthermore, we have integrated these catalysts into practical applications, including metal-air batteries, lithium-sulfur batteries, and non-enzymatic glucose sensors. To further demonstrate the innovative contributions of our work, we systematically compare it with the advanced work by other groups. Based on these findings and performance benchmarking analyses, we identify critical challenges that must be addressed to advance MOFs-based electrocatalysts toward next-generation energy conversion and sensing.</p>","PeriodicalId":10046,"journal":{"name":"Chemical record","volume":"25 5","pages":""},"PeriodicalIF":7.0,"publicationDate":"2025-04-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143939319","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Recent Advances in Fluorination Reactions via De-Carboxylative and De-Oxygenative Strategies: A Perspective. 脱羧和脱氧氟化反应的研究进展。
IF 7 2区 化学
Chemical record Pub Date : 2025-04-24 DOI: 10.1002/tcr.202500068
Nikita Goel, Poonam Kumari, Gunjan, Arushi Phillips, Sunita Bhagat
{"title":"Recent Advances in Fluorination Reactions via De-Carboxylative and De-Oxygenative Strategies: A Perspective.","authors":"Nikita Goel, Poonam Kumari, Gunjan, Arushi Phillips, Sunita Bhagat","doi":"10.1002/tcr.202500068","DOIUrl":"https://doi.org/10.1002/tcr.202500068","url":null,"abstract":"<p><p>Organic fluorine compounds encompass a vast and diverse variety of species that possess unique biological activity due to the presence of fluorine atoms. Fluorine is highly electronegative, increases the lipophilicity (fat-solubility) and hydrophobicity (water-repellent nature) of molecules, often exhibit remarkable chemical and thermal stability. This is especially useful in drug design, as it can improve the bioavailability of pharmaceutical compounds and help them interact more effectively with biological membranes. The growing demand for fluorinated compounds in materials science, agrochemicals, and medicine has made selective fluorine incorporation into organic molecules a challenging but necessary component of modern organic synthesis. Development of C-F building blocks are invaluable in organic synthesis due to their ability to impart chemical stability, selectivity, and reactivity to organic molecules. This article provides a detailed analysis of two popular fluorination processes: deoxyfluorination and decarboxyfluorination. Deoxyfluorination is the process of enhancing the physicochemical properties of molecules by replacing hydroxyl groups with fluorine atoms. Decarboxyfluorination is a type of chemical reaction where transformation of carboxylic acid derivatives into fluorinated compounds. The various fluorinating reagents, mechanistic processes, synthetic uses and substrate scope are covered in this section. When combined, these novel transformation strategies provide effective and focused approaches to the production of C-F bonds, offering useful resources for obtaining fluorinated compounds. This review mainly focuses on the construction of fluorinated compounds via deoxygenative and decarboxylative fluorination since 2011. We hope this review offers a useful conceptual overview and inspires further advancements in the efficient construction of C-F bond.</p>","PeriodicalId":10046,"journal":{"name":"Chemical record","volume":" ","pages":"e202500068"},"PeriodicalIF":7.0,"publicationDate":"2025-04-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143974718","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Woodward and Hoffmann. Hoffmann and Woodward. A Close Collaboration Had Yet to Begin** 伍德沃德和霍夫曼。霍夫曼和伍德沃德。密切合作尚未开始**
IF 7 2区 化学
Chemical record Pub Date : 2025-04-22 DOI: 10.1002/tcr.202400204
Jeffrey I. Seeman
{"title":"Woodward and Hoffmann. Hoffmann and Woodward. A Close Collaboration Had Yet to Begin**","authors":"Jeffrey I. Seeman","doi":"10.1002/tcr.202400204","DOIUrl":"https://doi.org/10.1002/tcr.202400204","url":null,"abstract":"<p>In 1965, R. B. Woodward and Roald Hoffmann published five communications in the <i>Journal of the American Chemical Society</i> in which they outlined the mechanisms of electrocyclizations, cycloadditions, and sigmatropic reactions – today known as the Woodward-Hoffmann rules. Over the next several years, the organic chemistry community rushed to test the validity of the W−H rules and expand the range of reactions covered by them. Meanwhile, Woodward and Hoffmann were besieged with invitations to lecture and write expositions on these concepts. In this publication, I present an analysis of Woodward and Hoffmann's next publications in 1966 and 1967 on the W−H rules. Two of these publications were based on lectures Woodward or Hoffmann presented in late 1965 and 1966. I also discuss their own continuing research on the topic in this time period (all by Hoffmann; none by Woodward). I conclude that the assumed intimate collaboration of Woodward and Hoffmann had actually not yet begun.</p>","PeriodicalId":10046,"journal":{"name":"Chemical record","volume":"25 5","pages":""},"PeriodicalIF":7.0,"publicationDate":"2025-04-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://onlinelibrary.wiley.com/doi/epdf/10.1002/tcr.202400204","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143939575","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Recent Advances in the Catalytic Synthesis of α-Ketoamides α-酮酰胺催化合成研究进展。
IF 7 2区 化学
Chemical record Pub Date : 2025-04-21 DOI: 10.1002/tcr.202500008
Mathew B. Aaron, P. S. Devi, Prof. Dr. Gopinathan Anilkumar
{"title":"Recent Advances in the Catalytic Synthesis of α-Ketoamides","authors":"Mathew B. Aaron,&nbsp;P. S. Devi,&nbsp;Prof. Dr. Gopinathan Anilkumar","doi":"10.1002/tcr.202500008","DOIUrl":"10.1002/tcr.202500008","url":null,"abstract":"<p><i>α</i>-Ketoamides are privileged chemical entities featuring a carbonyl group bonded to an amide. Bearing two pronucleophilic and two proelectrophilic sites, this structural scaffold exhibits distinct chemical properties and unparalleled biological activity. Owing to its wide application in medicinal, agricultural, and synthetic chemistry, methods for assembling this distinct moiety are ever-growing in demand. With the increasing focus on green synthesis, traditional routes to <i>α</i>-ketoamides have faded in recent years giving rise to the development of photocatalytic, electrosynthetic, and microwave-assisted catalytic protocols. We hereby provide a comprehensive and critical summary of all the catalytic advancements witnessed in this field from 2016 to the present.</p>","PeriodicalId":10046,"journal":{"name":"Chemical record","volume":"25 7","pages":""},"PeriodicalIF":7.0,"publicationDate":"2025-04-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143974829","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Research Projects How They Sprout, Bloom, and Wither Away 研究项目它们如何发芽、开花和枯萎
IF 7 2区 化学
Chemical record Pub Date : 2025-04-16 DOI: 10.1002/tcr.202400153
Reinhard W. Hoffmann
{"title":"Research Projects How They Sprout, Bloom, and Wither Away","authors":"Reinhard W. Hoffmann","doi":"10.1002/tcr.202400153","DOIUrl":"https://doi.org/10.1002/tcr.202400153","url":null,"abstract":"<p>The conception, initiation, major achievements, and termination of twelve different research projects in our research group are described. Covering a period of four decades, they mirror the changing trends and focusses of organic chemistry in the second half of the last century.</p>","PeriodicalId":10046,"journal":{"name":"Chemical record","volume":"25 5","pages":""},"PeriodicalIF":7.0,"publicationDate":"2025-04-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://onlinelibrary.wiley.com/doi/epdf/10.1002/tcr.202400153","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143938885","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Advancing CO2 Conversion with Cu-LDHs: A Review of Computational and Experimental Studies 利用Cu-LDHs推进CO2转化：计算和实验研究综述
IF 7 2区 化学
Chemical record Pub Date : 2025-04-14 DOI: 10.1002/tcr.202500014
Fabio Loprete, Eleonora Tosi Brandi, Francesco Calcagno, Jacopo De Maron, Andrea Fasolini, Riccardo Tarroni, Francesco Basile, Ivan Rivalta
{"title":"Advancing CO2 Conversion with Cu-LDHs: A Review of Computational and Experimental Studies","authors":"Fabio Loprete,&nbsp;Eleonora Tosi Brandi,&nbsp;Francesco Calcagno,&nbsp;Jacopo De Maron,&nbsp;Andrea Fasolini,&nbsp;Riccardo Tarroni,&nbsp;Francesco Basile,&nbsp;Ivan Rivalta","doi":"10.1002/tcr.202500014","DOIUrl":"10.1002/tcr.202500014","url":null,"abstract":"<p>Layered Double Hydroxides (LDHs) are versatile materials with tuneable properties. They show promising electro- and photo-catalytic activity in the activation and conversion of CO<sub>2</sub>. Their unique properties make LDHs pivotal materials in emerging sustainable strategies for mitigating the effect of CO<sub>2</sub> emissions. However, the intricate structure-property relationship inherent to LDHs challenges their rational design. In this review, we provide a comprehensive overview of both experimental and computational studies about LDHs for photo- and electro-catalytic conversion of CO<sub>2</sub>, mainly focusing on Cu-based systems due to their superior performance in producing C<sub>2</sub> products. We present a background framework, describing the essentials computational and experimental tools, designed to support both experimentalists and theoreticians in the development of tailored LDH materials for efficient and sustainable CO<sub>2</sub> valorisation. Finally, we discuss future potential advancements, emphasizing the importance of new synergistic experimental-computational studies.</p>","PeriodicalId":10046,"journal":{"name":"Chemical record","volume":"25 7","pages":""},"PeriodicalIF":7.0,"publicationDate":"2025-04-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://onlinelibrary.wiley.com/doi/epdf/10.1002/tcr.202500014","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143968003","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Cover Picture: A Comprehensive Survey of Stink Bug Pheromones - Extraction, Identification, Synthesis, Biosynthesis, and Phylogenetic Insights (Chem. Rec. 4/2025) 封面图片：臭虫信息素的综合调查-提取，鉴定，合成，生物合成和系统发育的见解（化学）。Rec。4/2025)
IF 7 2区 化学
Chemical record Pub Date : 2025-04-11 DOI: 10.1002/tcr.202580401
João P. A. Souza, Isaac R. Jorge, Aluska T. dos Santos, Leonardo Figueiredo, Brunno B. Rosa, Prof. Dr. Andressa Paladini, Prof. Dr. Paulo H. G. Zarbin
{"title":"Cover Picture: A Comprehensive Survey of Stink Bug Pheromones - Extraction, Identification, Synthesis, Biosynthesis, and Phylogenetic Insights (Chem. Rec. 4/2025)","authors":"João P. A. Souza,&nbsp;Isaac R. Jorge,&nbsp;Aluska T. dos Santos,&nbsp;Leonardo Figueiredo,&nbsp;Brunno B. Rosa,&nbsp;Prof. Dr. Andressa Paladini,&nbsp;Prof. Dr. Paulo H. G. Zarbin","doi":"10.1002/tcr.202580401","DOIUrl":"https://doi.org/10.1002/tcr.202580401","url":null,"abstract":"<p>This cover illustrates the evolutionary relationships of stink bugs (Pentatomidae) through a phylogenetic tree, with species positioned along its branches to reflect their diversity and ecological roles. In the background, key chemical structures of their pheromones are subtly displayed, representing distinct metabolic pathways that guided their phylogenetic placement. This visual narrative bridges chemistry and evolution, showcasing how chemical diversity has shaped the evolutionary history of these remarkable insects. More details can be found in article number e202400140 by Paulo H. G. Zarbin and co-workers. (DOl: 10.1002/tcr.202400140.\u0000 <figure>\u0000 <div><picture>\u0000 <source></source></picture><p></p>\u0000 </div>\u0000 </figure>\u0000 </p>","PeriodicalId":10046,"journal":{"name":"Chemical record","volume":"25 4","pages":""},"PeriodicalIF":7.0,"publicationDate":"2025-04-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://onlinelibrary.wiley.com/doi/epdf/10.1002/tcr.202580401","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143821995","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Self-assembly of Tyrosine Scaffolds in Aqueous Media: Complex Molecular Architectures from Simple Building Blocks 酪氨酸支架在水介质中的自组装：简单构建块的复杂分子结构。
IF 7 2区 化学
Chemical record Pub Date : 2025-04-10 DOI: 10.1002/tcr.202500005
Dineshkumar Bharathidasan, Dr. Chandan Maity
{"title":"Self-assembly of Tyrosine Scaffolds in Aqueous Media: Complex Molecular Architectures from Simple Building Blocks","authors":"Dineshkumar Bharathidasan,&nbsp;Dr. Chandan Maity","doi":"10.1002/tcr.202500005","DOIUrl":"10.1002/tcr.202500005","url":null,"abstract":"<p>Mimicking natural systems, self-assembly has been employed for constructing highly stable and well-ordered supramolecular structures. Amino acids are frequently used as building blocks in the self-assembly process due to their advantageous characteristics including easy availability, easy functionalization, tunable mechanical property, and biodegradability. <i>In situ</i> generation of active building blocks to obtain complex materials via self-assembly has enhanced their application in biomedical fields including bio-imaging, therapeutics. Single amino acid as the small building-block can provide artificial supramolecular materials with unique properties. In this review, we summarize the self-assembly of tyrosine-derivatives as single amino acid-based building blocks providing supramolecular assemblies and provide perspectives on their potential impact. Finally, we discuss the ongoing challenges for future research.</p>","PeriodicalId":10046,"journal":{"name":"Chemical record","volume":"25 6","pages":""},"PeriodicalIF":7.0,"publicationDate":"2025-04-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143985006","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Discover the Evolution: A Comprehensive Review of Transition and Rare Earth Metals for Oxygen Reduction Reaction, from Mono to High-Entropy Catalysts 发现演变：从单熵催化剂到高熵催化剂的氧还原反应过渡和稀土金属的综合评述。
IF 7 2区 化学
Chemical record Pub Date : 2025-04-10 DOI: 10.1002/tcr.202500032
Jala Bib Khan, Yuan-Chang Liang
{"title":"Discover the Evolution: A Comprehensive Review of Transition and Rare Earth Metals for Oxygen Reduction Reaction, from Mono to High-Entropy Catalysts","authors":"Jala Bib Khan,&nbsp;Yuan-Chang Liang","doi":"10.1002/tcr.202500032","DOIUrl":"10.1002/tcr.202500032","url":null,"abstract":"<p>Green energy, including metal-air batteries and fuel cells, is the key solution to climate change. The efficiency of these energy technologies depends on the oxygen reduction reaction (ORR) at the cathode, which is a slow process requiring expensive noble metal catalysts, like platinum, for improvement. The high cost of this catalyst restricts its widespread use in producing metal-air batteries and fuel cells. An alternative approach is to utilize non-noble metals, such as transition and rare earth metal catalysts, which are more cost-effective and demonstrate comparable durability and effectiveness to noble metals. With their affordability and distinct electronic structure, these non-noble metals have the potential to revolutionize the industry. Transition and rare earth metals can enhance the effectiveness of ORR catalysts by manipulating the electronic and surface molecular makeup through ′doping′ and ′synergistic effects′. This article discusses the roles of various non-noble metals in the ORR process, covering fundamental to advanced levels, as well as the progression from mono to high-entropy systems (systems with increasing complexity and potential for improved performance), including bi-, tri-, and tetra-metallic catalysts in a comprehensive manner, and emphasizes opportunities for researchers to propose innovative strategies for optimizing the ORR process.</p>","PeriodicalId":10046,"journal":{"name":"Chemical record","volume":"25 7","pages":""},"PeriodicalIF":7.0,"publicationDate":"2025-04-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143955897","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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