Food Hygiene and Safety Science最新文献_第6页

[Development of Analytical Method and Surveillance ofGibberellic Acid in Banana, Cherry, and Kiwi Fruit]. [香蕉、樱桃和猕猴桃中赤霉素的分析方法开发与监测]。

IF 0.2 4区农林科学

Food Hygiene and Safety Science Pub Date : 2023-01-01 DOI: 10.3358/shokueishi.64.123

Yuki Yamasaki, Yoshinari Suzuki, Ikuko Kitayama, Mari Nunome, Midori Kondo, Takatoshi Sakai, Satoru Nemoto, Hiroshi Akiyama, Tomoaki Tsutsumi

{"title":"[Development of Analytical Method and Surveillance ofGibberellic Acid in Banana, Cherry, and Kiwi Fruit].","authors":"Yuki Yamasaki, Yoshinari Suzuki, Ikuko Kitayama, Mari Nunome, Midori Kondo, Takatoshi Sakai, Satoru Nemoto, Hiroshi Akiyama, Tomoaki Tsutsumi","doi":"10.3358/shokueishi.64.123","DOIUrl":"10.3358/shokueishi.64.123","url":null,"abstract":"Gibberellic acid (GA3) is commonly used as a plant growth regulator in many food crops owing to its essential signaling functions during plant growth and development. In Japan, a threshold for administrative action for GA3 content of 0.3 mg/kg applies in produce in which maximum residue limits have not been established. Although the threshold is based on previous studies, the GA3 concentrations in individual foods are still unknown. Thus, we surveyed the concentrations of GA3 in banana, cherry, and kiwi fruit on the Japanese market. We developed and validated a method for the analysis of GA3 using solid-phase extraction and LC-MS/MS in accordance with accepted criteria of trueness, repeatability, and selectivity. The limits of detection and of quantification were determined as 0.005 and 0.05 mg/kg, respectively, in all fruits. Concentrations of GA3 did not exceed 0.3 mg/kg regardless of ripeness, suggesting the reasonability of the current regulation of GA3 in banana, cherry, and kiwi fruit. These findings can support prompt administrative action on these fruits, contributing to the regulation of GA3 in Japan.","PeriodicalId":54373,"journal":{"name":"Food Hygiene and Safety Science","volume":"64 4","pages":"123-129"},"PeriodicalIF":0.2,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10180849","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

[Improvement of Nitrite Analysis Method in Food Products]. 食品中亚硝酸盐分析方法的改进

IF 0.3 4区农林科学

Food Hygiene and Safety Science Pub Date : 2023-01-01 DOI: 10.3358/shokueishi.64.21

Takahiro Sasaki, Shoichi Tahara, Mari Morikawa, Tomoki Igarashi, Yuki Sadamasu, Keiko Ushiyama, Yukiko Yamajima, Chigusa Kobayashi

{"title":"[Improvement of Nitrite Analysis Method in Food Products].","authors":"Takahiro Sasaki, Shoichi Tahara, Mari Morikawa, Tomoki Igarashi, Yuki Sadamasu, Keiko Ushiyama, Yukiko Yamajima, Chigusa Kobayashi","doi":"10.3358/shokueishi.64.21","DOIUrl":"https://doi.org/10.3358/shokueishi.64.21","url":null,"abstract":"The conventional analysis method has problems with extraction efficiency, operability, and reproducibility. In this study, we attempted to solve these problems and improve the analytical method to obtain sufficient extraction efficiency and good operability and accuracy. The conventional method was able to get sufficient extraction in dried meat products, where the extraction efficiency of the conventional method was low, by increasing the concentration of sodium hydroxide solution at the time of homogenization. Suction filtration after adding the defoaming agent was added allowed for accurate volume adjustment. The turbidity of the extract caused by insufficient addition of zinc acetate solution was removed by increasing the amount of zinc acetate solution that was added. Turbidity caused by starch was removed by adding pancreatin. The RSD of the quantitative values was improved by adding sodium hydroxide solution and 80-90℃ water and immediately homogenizing. Furthermore, by changing the dilution factor of the extract solution in the colorimetric method, the inhibition of coloration by reducing substances was suppressed, and more accurate quantitative values could be obtained than with the conventional method. The recovery rate was 78.5-105% (RSD 0.7-5.8%), which was a good result. This method was considered to be a useful analytical method that can contribute to improving the inspection accuracy of nitrite ion analysis.","PeriodicalId":54373,"journal":{"name":"Food Hygiene and Safety Science","volume":"64 1","pages":"21-28"},"PeriodicalIF":0.3,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10823515","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

[Development of a Simple Identification Method for Omphalotus guepiniformis by Color Reaction]. 一种简便的颜色反应鉴别方法的建立

IF 0.3 4区农林科学

Food Hygiene and Safety Science Pub Date : 2023-01-01 DOI: 10.3358/shokueishi.64.108

Hideyuki Shinohara, Ryuma Okawara, Yuka Nagaoka

引用次数: 0

[An LC-MS/MS Analytical Method for Moenomycin A in Livestock Products]. 畜产品中莫诺霉素A的LC-MS/MS分析方法[j]。

IF 0.3 4区农林科学

Food Hygiene and Safety Science Pub Date : 2023-01-01 DOI: 10.3358/shokueishi.64.61

Hiroyuki Kikuchi, Takatoshi Sakai, Tomoko Okura, Satoru Nemoto, Hiroshi Akiyama, Takaaki Taguchi, Tomoaki Tsutsumi

{"title":"[An LC-MS/MS Analytical Method for Moenomycin A in Livestock Products].","authors":"Hiroyuki Kikuchi, Takatoshi Sakai, Tomoko Okura, Satoru Nemoto, Hiroshi Akiyama, Takaaki Taguchi, Tomoaki Tsutsumi","doi":"10.3358/shokueishi.64.61","DOIUrl":"https://doi.org/10.3358/shokueishi.64.61","url":null,"abstract":"A simple and sensitive method for the determination of moenomycin A residues in livestock products using LC-MS/MS was developed. Moenomycin A, a residual definition of flavophospholipol, was extracted from samples with a mixture of ammonium hydroxide and methanol (1 : 9, v/v) preheated at 50℃. The crude extracted solutions were evaporated and purified by liquid-liquid partitioning between a mixture of ammonium hydroxide, methanol and water (1 : 60 : 40, v/v/v) and ethyl acetate. The alkaline layer was taken, and cleaned up using a strong anion exchange (InertSep SAX) solid phase extraction cartridge. The LC separation was performed on an Inertsil C8 column with liner gradient elution using 0.3 vol% formic acid and acetonitrile containing 0.3 vol% formic acid. Moenomycin A was detected using tandem mass spectrometry with negative ion electrospray ionization. Recovery tests were conducted using three porcine samples (muscle, fat and liver) and chicken eggs. Samples were spiked with moenomycin A at 0.01 mg/kg and at the Japanese Maximum Residue Limits (MRLs) established for each sample. The trueness ranged from 79 to 93% and precision ranged from 0.5 to 2.8%. The limit of quantification (S/N≥10) of the developed method is 0.01 mg/kg. The developed method would thus be very useful for regulatory monitoring of flavophospholipol in livestock products.","PeriodicalId":54373,"journal":{"name":"Food Hygiene and Safety Science","volume":"64 2","pages":"61-68"},"PeriodicalIF":0.3,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"9503178","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

[Prevalence and Antimicrobial Resistance of Campylobacter jejuni/coli and Analysis of Macrolide Resistance Isolates from Retail Meat in Tokyo, Japan (2010-2019)]. [日本东京市（2010-2019年）空肠弯曲杆菌/大肠杆菌的流行率和耐药性以及零售肉类中大环内酯类耐药性分离株的分析]。

IF 0.3 4区农林科学

Food Hygiene and Safety Science Pub Date : 2023-01-01 DOI: 10.3358/shokueishi.64.185

Yukari Nishino, Yukako Shimojima, Rie Fukui, Sumiyo Kuroda, Kaeko Yamazaki, Kaoru Hatakeyama, Keiko Yokoyama, Kenji Sadamasu

{"title":"[Prevalence and Antimicrobial Resistance of Campylobacter jejuni/coli and Analysis of Macrolide Resistance Isolates from Retail Meat in Tokyo, Japan (2010-2019)].","authors":"Yukari Nishino, Yukako Shimojima, Rie Fukui, Sumiyo Kuroda, Kaeko Yamazaki, Kaoru Hatakeyama, Keiko Yokoyama, Kenji Sadamasu","doi":"10.3358/shokueishi.64.185","DOIUrl":"10.3358/shokueishi.64.185","url":null,"abstract":"This study aimed to investigate the prevalence and antimicrobial sensitivity of Campylobacter jejuni and Campylobacter coli in retail meat (chicken, beef, pork, venison, wild boar, horse, lamb and mutton) in Tokyo (Japan) from 2010 to 2019. Furthermore, the resistance mechanism of erythromycin (EM)-resistant strains was analysed. C. jejuni had a highly positive rate in domestic chicken meat (53.4%, 334/626 samples), domestic chicken offal (49.3%, 34/69 samples), and domestic beef offal (28.3%, 47/166 samples), while C. coli had a high positivity rate in domestic pork offal (31.7%, 44/139 samples). The positive rate of C. jejuni was significantly higher in offal than that in meat in domestic beef, while the positive rate of C. coli was significantly higher in offal than that in meat in domestic beef and domestic pork (p<0.05). In the isolates, 1.0% (6/631 strains) of C. jejuni and 36.2% (55/152 strains) of C. coli were EM resistant, with 41.5% (262/631 strains) of C. jejuni and 65.1% (99/152 strains) of C. coli being ciprofloxacin resistant. A2075G mutation of the 23S rRNA gene was confirmed in all EM-resistant strains.","PeriodicalId":54373,"journal":{"name":"Food Hygiene and Safety Science","volume":"64 5","pages":"185-190"},"PeriodicalIF":0.3,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"50163710","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

[Analysis of Maximum Growth Rate and Construction of Predictive Growth Model for Bacillus cereusin Mashed Potato by Calorimetric Method]. [热量测定法分析蜡样芽孢杆菌马铃薯泥的最大生长率并构建预测生长模型]。

IF 0.3 4区农林科学

Food Hygiene and Safety Science Pub Date : 2023-01-01 DOI: 10.3358/shokueishi.64.200

Rie Togawa, Satomi Kanagawa, Saya Fukumoto, Fia Noviyanti, Yukie Hosotani, Daisuke Koizumi, Keishi Iohara, Jun Shimodaira, Susumu Kawasaki

{"title":"[Analysis of Maximum Growth Rate and Construction of Predictive Growth Model for Bacillus cereusin Mashed Potato by Calorimetric Method].","authors":"Rie Togawa, Satomi Kanagawa, Saya Fukumoto, Fia Noviyanti, Yukie Hosotani, Daisuke Koizumi, Keishi Iohara, Jun Shimodaira, Susumu Kawasaki","doi":"10.3358/shokueishi.64.200","DOIUrl":"10.3358/shokueishi.64.200","url":null,"abstract":"The maximum growth rate (μmax) of Bacillus cereus was estimated using a non-destructive isothermal calorimetric method, and a growth prediction model was constructed based on the measurement results. SCD medium and mashed potato were inoculated with serial-diluted inoculum of B. cereus. Heat generation curves were determined using an isothermal calorimeter at 35, 25, and 15℃. The μmax was determined from the relationship between the increase in B. cereus cell number and incubation time, which was detected through the heat generation of the B. cereus biological process. Moreover, the growth prediction model was constructed using Ratkowsky's square-root model. The results of the growth prediction model based on the data of the calorimetric and conventional culture methods for SCD were expressed as √μCalmax=0.0354 (T-4.9)[R2=0.99] and √μCCMmax=0.0335 (T-5.0)[R2=0.99]; a similar equation was provided by both methods. Conversely, the results of the growth prediction model based on the calorimetric method data for mashed potato were given as √μCalmax=0.0390 (T-8.5)[R2=0.99]; the maximum growth rates at 30 and 20℃ were predicted as 0.70 and 0.20 (1/hr), respectively. The maximum growth rates obtained using the conventional culture method were 0.63 and 0.29 (1/hr), respectively, similar to the calorimetric method results. The predictive microbiological analysis using the calorimetric method enabled the rapid provision of a growth prediction equation, and the number of samples could be substantially reduced compared with that for the conventional culture method.","PeriodicalId":54373,"journal":{"name":"Food Hygiene and Safety Science","volume":"64 6","pages":"200-205"},"PeriodicalIF":0.3,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139089372","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

[Development for the Simultaneous Analytical Method of Furan and Alkyl Furans in Processed Foods]. 加工食品中呋喃和烷基呋喃同时分析方法的研究进展

IF 0.3 4区农林科学

Food Hygiene and Safety Science Pub Date : 2023-01-01 DOI: 10.3358/shokueishi.64.29

Motoki Ogiso, Chihiro Hashimoto, Eisuke Toriumi, Kanako Nishimura, Seiichiro Iizuka, Kazuhiro Sakamoto, Yushi Yamamoto, Yukiko Yamada

引用次数: 0

[Proposal for Guidelines on the Notation and Investigation of Scientific Names for the Source of Natural Food Additives in Japanese Standards]. [关于日本标准中天然食品添加剂来源的科学名称标注和调查指南的建议]。

IF 0.3 4区农林科学

Food Hygiene and Safety Science Pub Date : 2023-01-01 DOI: 10.3358/shokueishi.64.78

Naoko Masumoto, Naoki Sugimoto, Kyoko Sato

{"title":"[Proposal for Guidelines on the Notation and Investigation of Scientific Names for the Source of Natural Food Additives in Japanese Standards].","authors":"Naoko Masumoto, Naoki Sugimoto, Kyoko Sato","doi":"10.3358/shokueishi.64.78","DOIUrl":"https://doi.org/10.3358/shokueishi.64.78","url":null,"abstract":"The official specifications for food additives from natural sources list the species according to their scientific and Japanese names, thereby providing a unique identifier for the species. This helps to prevent the use of nonprescribed species, which might cause unexpected or unintended health hazards. However, there are cases in which the names of the source species listed in the official specifications differ from the accepted scientific names based on the latest taxonomic research. In this paper, we argue that it is more important to define scientific and Japanese names with an emphasis on traceability in order to control the range of food additive ingredients in a rational and sustainable manner. Therefore, we proposed a method for ensuring traceability as well as a specific notation procedure for scientific and Japanese names. Using this method, we examined the source species for three food additives. In some cases, the range of sources species expanded with the change in scientific names. Ensuring traceability is extremely important, but it is also necessary to confirm whether unexpected species are included when names are changed.","PeriodicalId":54373,"journal":{"name":"Food Hygiene and Safety Science","volume":"64 2","pages":"78-88"},"PeriodicalIF":0.3,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"9503176","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

[Study on Migrants Found in Migration Solutions from Commercially Available Polyethylene Products]. [对市售聚乙烯产品迁移溶液中发现的迁移物的研究]。

IF 0.3 4区农林科学

Food Hygiene and Safety Science Pub Date : 2023-01-01 DOI: 10.3358/shokueishi.64.101

Keiko Iwakoshi, Katsushi Iwakoshi, Megumi Hasebe, Asa Osuga, Hiroyuki Miyakawa, Motoh Mutsuga, Chigusa Kobayashi

引用次数: 0

[Investigation of Genetically Modified Maize Imported into Japan in 2021/2022 and the Applicability of Japanese Official Methods]. [2021/2022 年日本进口转基因玉米的调查和日本官方方法的适用性]。

IF 0.2 4区农林科学

Food Hygiene and Safety Science Pub Date : 2023-01-01 DOI: 10.3358/shokueishi.64.218

Keisuke Soga, Chie Taguchi, Miyu Sugino, Tomohiro Egi, Jumpei Narushima, Satoko Yoshiba, Reona Takabatake, Kazunari Kondo, Norihito Shibata

{"title":"[Investigation of Genetically Modified Maize Imported into Japan in 2021/2022 and the Applicability of Japanese Official Methods].","authors":"Keisuke Soga, Chie Taguchi, Miyu Sugino, Tomohiro Egi, Jumpei Narushima, Satoko Yoshiba, Reona Takabatake, Kazunari Kondo, Norihito Shibata","doi":"10.3358/shokueishi.64.218","DOIUrl":"10.3358/shokueishi.64.218","url":null,"abstract":"Given that the number of genetically modified (GM) maize events that have been announced as having undergone safety assessment procedures in Japan is increasing yearly, more information is needed about their actual recent domestic distribution in Japan. In this study, we investigated whether current Japanese official qualitative and quantitative methods (the current official methods) for GM maize can comprehensively target events in domestically distributed maize. For samples with the identity-preserved (IP) handling system and non-IP samples from the United States (US) and non-IP samples from Brazil, we performed event-specific real-time PCR targeting 25 authorized single GM maize events in addition to the current official methods. According to our results, 15 events targeted by the current official methods were detected, but insect-resistance (IR) Event5307 and herbicide-tolerant (HT) DAS40278, not targeted by the current official methods, were detected in the US (one out of 5 lots) and Brazilian (four out of 5 lots) non-IP samples, respectively. Nevertheless, a survey of recent GM maize acreage in recent years has revealed that more than 95% of the acreage in US maize is occupied by HT or IR/HT stacked events, and that more than 95% of the acreage in Brazilian maize is occupied by IR or IR/HT stacked events. Because the current official methods can target all stacked events related to Event5307 and DAS40278, the only undetectable events are the single Event5307 and DAS40278, whose production is estimated to be less than 5% of the total production in the producing country. Therefore, we conclude that the current official methods for the labelling of GM maize should be maintained in view of practicability.","PeriodicalId":54373,"journal":{"name":"Food Hygiene and Safety Science","volume":"64 6","pages":"218-225"},"PeriodicalIF":0.2,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139089375","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0