Food Hygiene and Safety Science最新文献_第10页

[Proteome Analysis for Identification of the Origin of Biological Foreign Substances]. 生物外来物质来源鉴定的蛋白质组学分析

IF 0.3 4区农林科学

Food Hygiene and Safety Science Pub Date : 2022-01-01 DOI: 10.3358/shokueishi.63.218

Yukako Sato, Tomoko Dewa, Koji Suzuki, Yasushi Nagatomi, Tetsuro Magarifuchi, Yasuhisa Miyamoto

引用次数: 0

[Determination of Quinclorac in Livestock Products by LC-MS/MS]. [LC-MS/MS法测定畜产品中喹诺灭]。

IF 0.3 4区农林科学

Food Hygiene and Safety Science Pub Date : 2022-01-01 DOI: 10.3358/shokueishi.63.177

Yutaro Takewaki, Ryo Okabe, Satoru Nemoto, Mitsutoshi Aoyagi

引用次数: 0

[Single-laboratory Validation of an Analytical Method for Detarmination of Fusarium toxins in Buckwheat and Job's Tears]. [荞麦和薏米中镰刀菌毒素脱毒分析方法的单一实验室验证]。

IF 0.2 4区农林科学

Food Hygiene and Safety Science Pub Date : 2022-01-01 DOI: 10.3358/shokueishi.63.117

Miho Kawanishi, Kazuya Suenaga, Tomohiro Hirano

引用次数: 0

[Detection of Tetrodotoxin in Vomit and Urine from a Patient Suffering from Pufferfish Poisoning]. [一例河豚中毒患者呕吐物和尿液中河豚毒素的检测]。

IF 0.3 4区农林科学

Food Hygiene and Safety Science Pub Date : 2022-01-01 DOI: 10.3358/shokueishi.63.225

Junko Namba, Toyohiro Urayama, Hidefumi Kaneko, Atsushi Sato, Kae Fujimoto, Noriko Shigeta

引用次数: 0

[Quantitative Analysis of Bisacurone in Turmeric by HPLC Using Relative Molar Sensitivity]. 姜黄中比沙酮的相对摩尔灵敏度高效液相色谱定量分析

IF 0.3 4区农林科学

Food Hygiene and Safety Science Pub Date : 2022-01-01 DOI: 10.3358/shokueishi.63.202

Kazuo Koyama, Hiroshi Sasako, Yohei Higashi, Hirono Ichikawa, Ayako Nagoya, Takashi Hirao

{"title":"[Quantitative Analysis of Bisacurone in Turmeric by HPLC Using Relative Molar Sensitivity].","authors":"Kazuo Koyama, Hiroshi Sasako, Yohei Higashi, Hirono Ichikawa, Ayako Nagoya, Takashi Hirao","doi":"10.3358/shokueishi.63.202","DOIUrl":"https://doi.org/10.3358/shokueishi.63.202","url":null,"abstract":"A novel method was developed for quantification of bisacuron (BC) and dehydrozingerone (DZ), the functional component of turmeric (Curcuma longa.L)-containing foods, using a relative molar sensitivity (RMS) method based on the combination of HPLC-UV and 1H-NMR. The RMSs of BC and DZ using 4-hydroxybenzoic acid ethyl ester (HBE) as the internal standard were calculated to 1.66 and 2.55, respectively. Analysis of fourteen beverage products showed the high correlations between the concentrations of BC and DZ quantified by the RMS method and those quantified by absolute calibration curve method. A collaborative study was conducted by four laboratories on one beverage and one tablet products. The repeatable relative standard deviation (RSDr) of intra-laboratories ranged from 0.7 to 1.7%, and the reproducible relative standard deviation (RSDR) of inter-laboratories ranged from 2.0 to 7.3%. The RMS method enabled the quantification of analytes for which difficultly obtain standard materials such as BC and DZ, using an internal standard for which obtain routinely readily available. This RMS method is expected to be applied to quality control for food products containing turmeric.","PeriodicalId":54373,"journal":{"name":"Food Hygiene and Safety Science","volume":"63 6","pages":"202-209"},"PeriodicalIF":0.3,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10816272","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

[Prevalence of Foodborne Pathogens in Retail Meat in Saitama, Japan]. [日本埼玉市零售肉类中食源性病原体的流行情况]。

IF 0.3 4区农林科学

Food Hygiene and Safety Science Pub Date : 2022-01-01 DOI: 10.3358/shokueishi.63.151

Nozomi Sakakida, Mika Sato, Satomi Kando, Kaori Kashima, Shinichi Shimada, Rie Ishii

{"title":"[Prevalence of Foodborne Pathogens in Retail Meat in Saitama, Japan].","authors":"Nozomi Sakakida, Mika Sato, Satomi Kando, Kaori Kashima, Shinichi Shimada, Rie Ishii","doi":"10.3358/shokueishi.63.151","DOIUrl":"https://doi.org/10.3358/shokueishi.63.151","url":null,"abstract":"We investigated the prevalence of Campylobacter jejuni, Campylobacter coli, Salmonella, enterohemorrhagic Escherichia coli, enterotoxigenic Escherichia coli, Yersinia enterocolitica, and Escherichia albertii in domestic chicken and pork sold at retail stores in Saitama Prefecture, Japan. Campylobacter was detected in 35.7% (60/168) of chicken samples and 7.3% (14/190) of pork samples. C. jejuni and C. coli were predominant in chicken and pork, respectively. Salmonella was found in 58.1% (100/172) of chicken samples and 19.9% (41/206) of pork samples. Moreover, Salmonella Schwarzengrund was the major serovar observed in chicken isolates, whereas S. Typhimurium monophasic variant was in pork isolates. Furthermore, ETEC was found in 0.6% (1/160) of chicken samples and 2.4% (5/206) of pork samples. Y. enterocolitica was absent from all (83/83) chicken samples but was present in 9.3% (18/193) of pork samples, with a prevalence in pork tongues as high as 21.0% (13/62 samples). However, EHEC and E. albertii were not detected in our study. Therefore, the results of this study indicate that chicken was highly contaminated with Campylobacter sp. and Salmonella, and pork was with Y. enterocolitica serotype O3, Campylobacter sp., Salmonella, and ETEC.","PeriodicalId":54373,"journal":{"name":"Food Hygiene and Safety Science","volume":"63 4","pages":"151-157"},"PeriodicalIF":0.3,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"40335167","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

[Survey of Arsenic/Heavy Metals and Pesticide Residues in Edible Insects for Human Consumption or Supplied in Japan]. [日本供人食用或供应的食用昆虫中砷/重金属及农药残留调查]。

IF 0.3 4区农林科学

Food Hygiene and Safety Science Pub Date : 2022-01-01 DOI: 10.3358/shokueishi.63.136

Yugo Kitahara, Hiroshi Nomura, Nanami Nishihara, Takuya Ueda, Satoru Watanabe, Isao Saito, Jun Ueyama

引用次数: 1

[Separate Analysis of Loquat Fruit Pulp, Peel, and Pits to Calculate Pesticide Residue Levels in the Whole Commodity]. [分别分析枇杷果肉、果皮和果核以计算整个商品中的农药残留量]。

IF 0.2 4区农林科学

Food Hygiene and Safety Science Pub Date : 2022-01-01 DOI: 10.3358/shokueishi.63.62

Shinobu Hikino, Tomonari Yajima, Michiko Sakasai, Naruto Tomiyama, Kazuaki Iijima, Kazutoshi Ohyama

{"title":"[Separate Analysis of Loquat Fruit Pulp, Peel, and Pits to Calculate Pesticide Residue Levels in the Whole Commodity].","authors":"Shinobu Hikino, Tomonari Yajima, Michiko Sakasai, Naruto Tomiyama, Kazuaki Iijima, Kazutoshi Ohyama","doi":"10.3358/shokueishi.63.62","DOIUrl":"10.3358/shokueishi.63.62","url":null,"abstract":"To evaluate the effects of handling \"not detectable\" residues (ND: <0.01 mg/kg) in the pulp and detectable residues in the pits on the calculation of pesticide residue in the whole fruit, residue levels in the pulp, peel, and pits of loquat fruits were separately analyzed. Following conventional Japanese agricultural practices, 16 pesticides were sprayed at the maximum application rates in three test fields. All target pesticides were detected at quantifiable levels in the peel (n=144). In contrast, the percentages of detected pesticides in the pulp and pits were 42% (n=61) and 36% (n=52), respectively. Most pesticide residues were present in the peel. For comparison, the pesticide residue levels in the whole fruits were determined based on three indices: the highest estimate (H), calculated using the measured residue levels in the pits and by replacing the ND residues in the pulp as the limit of quantification (LOQ) values; conventional estimate (C), calculated by neglecting all residues in the pits (0 mg/kg) and replacing the ND residues in the pulp as LOQ values; and the lowest estimate (L), calculated by neglecting all residues in the pits and the ND residues in the pulp (0 mg/kg). The L/C and H/C ratios ranged from 74% (L/C) to 106% (H/C). In seven of eighty-three cases with less than 90% difference, residue levels in the whole loquat fruits were low (≤0.06 mg/kg), with the actual range being equal to or below the minimum unit of 0.01. In comparison of three field datasets, the range of residue levels was estimated to be 2.77 mg/kg. Based on the results of separate analysis, handling of ND residues in the pulp and detectable residues in the pits did not significantly affect the calculated pesticide residue levels in the whole loquat fruits.","PeriodicalId":54373,"journal":{"name":"Food Hygiene and Safety Science","volume":"43 1","pages":"62-69"},"PeriodicalIF":0.2,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"91386882","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

[Simultaneous Analysis of 7 Antiviral Agents in Chicken Tissues and Processed Products by LC-MS/MS]. [利用 LC-MS/MS 同时分析鸡组织和加工产品中的 7 种抗病毒药物]。

IF 0.2 4区农林科学

Food Hygiene and Safety Science Pub Date : 2022-01-01 DOI: 10.3358/shokueishi.63.1

Takayuki Asakura, Mariko Kitamura, Miho Yasumoto, Yoshitaka Takeuchi, Mitsuo Nakazato, Kazuo Yasuda

{"title":"[Simultaneous Analysis of 7 Antiviral Agents in Chicken Tissues and Processed Products by LC-MS/MS].","authors":"Takayuki Asakura, Mariko Kitamura, Miho Yasumoto, Yoshitaka Takeuchi, Mitsuo Nakazato, Kazuo Yasuda","doi":"10.3358/shokueishi.63.1","DOIUrl":"10.3358/shokueishi.63.1","url":null,"abstract":"Since amantadine, rimantadine, arbidol, laninamvir, oseltamivir, peramivir, and zanamivir may be used as antiviral agents to treat avian influenza, we herein developed a simultaneous assay using LC-MS/MS. This method was applied to chicken products (including yakitori (grilled chicken), fried chicken, chicken steak, and boiled eggs) as well as chicken tissues (muscle, fat, the liver, gizzards, and heart) and eggs.Samples were extracted with methanol-water (9 : 1), purified by a tandem column with an InertSep® MAX cartridge (upper part) and InertSep® MCX cartridge (lower part), and then measured by LC-MS/MS. The sample matrix had no effect on the identification of compounds. Chromatographic separation was performed on a ZIC-HILIC column using a mobile phase of 1% acetic acid solution and 1% acetic acid solution in acetonitrile, resulting in complete separation and other obstructive peaks from the sample matrices. An external solvent calibration curve was used for quantification.The application of the method to 6 samples of chicken tissues and eggs achieved good results of between 77.9 and 97.5% for trueness and between 1.7 and 9.2% for concurrent accuracy. The method was also applied to 9 samples of processed products, including grilled chicken and fried chicken, and achieved good results with true percentages ranging between 72.6 and 99.2% and concurrent accuracies between 3.0 and 11.2%. Therefore, the developed method may also be applied to processed products.The limit of quantification (LOQ) of the developed method was 0.01 mg/kg.The method was then applied to 42 types of commercial processed products, including yakitori, fried chicken, steamed chicken, chicken steak, and boiled eggs, and no antiviral agents were detected.Collectively, the present results confirmed that the method developed herein is applicable to not only chicken tissues, but also their processed products.","PeriodicalId":54373,"journal":{"name":"Food Hygiene and Safety Science","volume":"1 1","pages":"1-11"},"PeriodicalIF":0.2,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"77084603","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

[Pharmaceutical Ingredients Detected in Dietary Supplements Purchased by Chiba Prefecture (Fiscal Years 2014-2021)]. 【千叶县购买的膳食补充剂中检出的药物成分(2014-2021财年)】。

IF 0.3 4区农林科学

Food Hygiene and Safety Science Pub Date : 2022-01-01 DOI: 10.3358/shokueishi.63.141

Tomohide Fukiwake, Keigo Enomoto, Hiroki Yoshino, Katsuya Uchimoto, Maki Nishimura, Hiroshi Akiyama

{"title":"[Pharmaceutical Ingredients Detected in Dietary Supplements Purchased by Chiba Prefecture (Fiscal Years 2014-2021)].","authors":"Tomohide Fukiwake, Keigo Enomoto, Hiroki Yoshino, Katsuya Uchimoto, Maki Nishimura, Hiroshi Akiyama","doi":"10.3358/shokueishi.63.141","DOIUrl":"https://doi.org/10.3358/shokueishi.63.141","url":null,"abstract":"In the pharmaceutical ingredients contamination testing of 702 commercial dietary supplement products, during fiscal years 2014-2021, 14 pharmaceutical ingredients, barrenwort, leaf axils of senna, and small leaf of senna were detected in 28 products. Screening and confirmation of the pharmaceutical ingredients in the products were performed by ultra-high performance liquid chromatography with photodiode array detector and ultra-high performance liquid chromatography-quadrupole-kingdon trap mass spectrometry, respectively. In particular, leaf axils and small leaf of senna were identified by stereomicroscopy and scanning electron microscopy. Furthermore, we found several pharmaceutical ingredients that exceeded the daily medicated dosage; therefore, it is important to prevent the distribution of such products to prevent the occurrence of health hazard. For that reason, it is necessary to continue the sample purchasing and testing systems to monitor the distribution of products containing pharmaceutical ingredients.","PeriodicalId":54373,"journal":{"name":"Food Hygiene and Safety Science","volume":"63 4","pages":"141-150"},"PeriodicalIF":0.3,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"40336840","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0