Anton Mostovoy, Amirbek Bekeshev, Andrey Shcherbakov, Ainagul Apendina, Raigul Orynbassar, Victoria Svitkina, Marina Lopukhova
{"title":"Investigating of epoxy nanocomposites structure and properties that contain both pristine and aminosilane-treated silicon carbide (SiC) particles","authors":"Anton Mostovoy, Amirbek Bekeshev, Andrey Shcherbakov, Ainagul Apendina, Raigul Orynbassar, Victoria Svitkina, Marina Lopukhova","doi":"10.1177/00219983241253818","DOIUrl":"https://doi.org/10.1177/00219983241253818","url":null,"abstract":"This article presents a methodology for functionalization of silicon carbide (SiC) through chemical modification using γ-aminopropyltriethoxysilane (APTES) and its subsequent dispersion in an epoxy composition. The research revealed that functionalizing SiC particles with γ-aminopropyltriethoxysilane (SiC<jats:sub>(APTES)</jats:sub>) enhanced their chemical compatibility with the epoxy composition, facilitating the dispersion of SiC particles. Furthermore, it was observed that the functionalization of the filler had a profound impact on the structure, curing kinetics, and physical and mechanical properties of epoxy nanocomposites. The addition of SiC<jats:sub>(APTES)</jats:sub> into the epoxy composition resulted in a significant reinforcement of the material. Specifically, the flexural stress and flexural modulus of elasticity increased by 179% and 74%, respectively, while the impact strength experienced a remarkable improvement of 462%. Additionally, the tensile strength and tensile modulus of elasticity increased by 83% and 70%, respectively, compared to the epoxy composite without SiC. The application of SiC<jats:sub>(APTES)</jats:sub> also played a crucial role in initiating the polymerization process through the involvement of reactive amino groups, leading to a reduction in the initial curing temperature and an amplification of the thermal effects of the polymerization reaction. Moreover, the presence of functionalized SiC significantly influenced the structure of the epoxy composite, thereby contributing to its enhanced strength. In summary, the inclusion of SiC in the epoxy composition not only bolstered the material but also improved its thermal stability.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"17 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-05-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140829121","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Experimental investigation on the effects of stainless-steel mesh reinforcing layers on low-velocity impact response of hybrid thermoplastic glass fiber composites","authors":"Sepanta Mandegarian, Mehdi Hojjati","doi":"10.1177/00219983241253028","DOIUrl":"https://doi.org/10.1177/00219983241253028","url":null,"abstract":"This study aims to assess the hybridization effect on the perforation threshold of Low-Velocity Impact (LVI) in thermoplastic glass composite laminates, incorporating layers of resin-impregnated stainless-steel mesh. Reinforcing methodologies such as hybridization are recently being adopted as a practical approach to increasing the energy-absorbing capacity of polymer composites. In the current paper, a multi-step hot press lamination method has been employed to fabricate the hybrid composite laminates strengthened with stainless-steel mesh layers. Several stacking sequences, metal mesh wire sizes, orientation and position relative to the impactor have been examined under various LVI energies. It was revealed that the LVI penetration energy was increased for the thermoplastic-based composite laminates reinforced with stainless-steel mesh layers. Furthermore, the LVI penetration energy threshold was significantly influenced by the metal mesh wire size, orientation and stacking sequence. Finally, the backlight method capability was assessed to detect the after-impact interlaminar damages.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"29 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-05-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140829197","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Menna A Saleh, Sinan Olcun, Mohamed Karam, Roger Kempers, Garrett W Melenka
{"title":"High stiffness 3D-printed continuous pitch carbon fiber reinforced polymer composites","authors":"Menna A Saleh, Sinan Olcun, Mohamed Karam, Roger Kempers, Garrett W Melenka","doi":"10.1177/00219983241249526","DOIUrl":"https://doi.org/10.1177/00219983241249526","url":null,"abstract":"This study presents a method for 3D printing very high stiffness pitch-based carbon fiber (CF) reinforced polylactic acid (PLA) composites using a modified open-source 3D printer. The fused filament fabrication (FFF) technique was used to fabricate the samples with alternating layers of PLA and PLA-coated pitch CF. The tensile Young’s modulus of the 3D-printed composite samples was measured to characterize the effect of different grades and volume fractions of pitch CF on the behaviour of the printed composites. Three grades of pitch CF which have different Young’s modulus were used with volume fractions ranging from 2.4 to 8.4%. Tensile tests showed that the K1392U CF reinforced composite with a 7.3% volume fraction demonstrated the highest improvement in Young’s modulus of 850% compared to neat 3D-printed PLA. This improvement is notably higher than any previous 3D-printed carbon-based composites at a relatively low volume fraction of CF. Statistical analysis showed increased Young’s modulus in all of 3D-printed composite samples tested. The experimental values were compared to the Halpin-Tsai model and suggest that some degree of fibre breakage occurred during the 3D printing process owing to the relative stiffness of the pitch-based fibers. Future directions and suggestions for process improvements are discussed.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"91 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-05-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140829209","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Lais Kohan, Carlos A Fioroni, Adriano GDS Azevedo, Barbara Leonardi, Julia Baruque-Ramos, Raul Fangueiro, Holmer Savastano Junior
{"title":"Jute textiles with enhanced interfacial bonding as reinforcement for cementitious composites","authors":"Lais Kohan, Carlos A Fioroni, Adriano GDS Azevedo, Barbara Leonardi, Julia Baruque-Ramos, Raul Fangueiro, Holmer Savastano Junior","doi":"10.1177/00219983241249237","DOIUrl":"https://doi.org/10.1177/00219983241249237","url":null,"abstract":"In fabric-cement composites, the limited impregnation of cementitious matrix products due to thick and twisted yarns leads to premature failure due to poor bonding strength. In addition, cellulosic textile reinforcements have many challenges about durability, appearance of voids at mortar-fiber interface, and rise of microcracks. Textile performances were evaluated in different conditions: coated with micro-silica powder, pretreated, and without any treatment. This study also assessed how textile weave structure and yarn geometry configuration affect the interactions of two different jute textiles (Close Weave Jute Fabric – CJF and Open Weave Jute Fabric - OJT) when used as reinforcement in mortar matrix. Textile characterization and composite analysis (by four-point bending tests, SEM/EDS, and physical tests) were conducted to assess the different textile reinforcements, the mechanical behavior of produced composites, and visual and chemical compounds analysis of the interfacial transition zone between textile and mortar matrix after silica coating. Micro silica powder coating was deemed necessary to address limited impregnation and to avoid telescope pull-off. Weave structure determined the difference between jute fabrics to reinforce mortar matrix, being only OJF (larger interstices in the weave structure) with micro silica coating allowed a better matrix interaction and stood out from the other textiles and achieved the best specific energy of all samples, (4.28 ± 0.91) kJ.m-2. Calcium and silicon inside the yarn interstices and textile-matrix interface indicate the formation of strong bonds by calcium-silicate-hydrate products. The silica coating treatment enhanced formation of strong bonds, which demonstrated future promise for natural fiber application.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"20 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-04-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140810215","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Study of 3D-printed onyx parts reinforced with continuous glass fibers: Focus on mechanical characterization, analytical prediction and numerical simulation","authors":"Daouda Nikiema, Pascale Balland, Alain Sergent","doi":"10.1177/00219983241247913","DOIUrl":"https://doi.org/10.1177/00219983241247913","url":null,"abstract":"The 3D printing of continuous-fiber composites is currently relevant to engineers and researchers. This study aims to characterize and predict the mechanical properties of Onyx/glass fiber specimens printed using 3D printing. The work assesses the impact of glass fiber printing parameters on the mechanical behavior of printed parts and proposes analytical and numerical methods to predict mechanical properties. A physicochemical analysis was conducted on 3D printed continuous glass fibers. The study also investigated the impact of fiber printing parameters on composite parts. The results indicate that the 3D-printed glass fibers consist of nylon, continuous glass fibers, and voids (porosity), which range from 58% to 63%, 31% to 38%, and 5% to 8%, respectively. Mechanical characterizations indicate that printing fiber layers in blocks results in superior mechanical properties compared to printing alternating layers of glass fibers and Onyx. Additionally, the concentric mode of fiber printing can be challenging if the ‘start rotation’ parameter is not adjusted correctly. Premature specimen breakage occurred when fiber printing began within their useful length, resulting in a deformation at break that was approximately 34% less, depending on the starting position. The proposed analytical and numerical prediction methods had prediction errors of approximately 7% to 12% and 5% to 7%, respectively. Engineers can use these prediction approaches during the dimensioning phase of 3D printed composite parts.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"28 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-04-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140630100","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"In situ compressive behavior of carbon fibers reinforced PolyEtherEther Ketone laminates exposed to one-sided heat flux","authors":"Benoit Vieille, Alexis Coppalle","doi":"10.1177/00219983241248754","DOIUrl":"https://doi.org/10.1177/00219983241248754","url":null,"abstract":"This study investigates the influence of a combined thermal heat flux (imposed by a cone calorimeter) and a compressive loading on the deformation and damage mechanisms within quasi-isotropic carbon fibers reinforced PolyEtherEther Ketone laminates. Thermogravimetric Analyses conducted at increasing heating rates under nitrogen (from 5 to 500°C/min) provide valuable information on the thermal decomposition of C/PEEK that ranges from 550°C to 627°C, with a corresponding mass loss ranging from 20 to 26%. From the thermo-mechanical coupling standpoint, the softening and the thermal decomposition of the PEEK matrix under a 50 kW/m<jats:sup>2</jats:sup> heat flux result in the micro-buckling of fibers bundles in matrix-rich areas at the ply scale. Ultimately, it leads to the formation and propagation in the transverse direction of plastic kink bands at the laminates scale. Post-failure observations show that this macroscopic kinking propagates specifically according to the PEEK matrix pyrolysis.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"2013 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-04-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140617704","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Till Hermann, Dariusz Niedziela, Diyora Salimova, Timo Schweiger
{"title":"Predicting the fiber orientation of injection molded components and the geometry influence with neural networks","authors":"Till Hermann, Dariusz Niedziela, Diyora Salimova, Timo Schweiger","doi":"10.1177/00219983241248216","DOIUrl":"https://doi.org/10.1177/00219983241248216","url":null,"abstract":"The injection molding simulation of short fiber reinforced plastics (SFRP) is time consuming. However, until now it is necessary for predicting the local fiber orientation, to optimize the molding process and to predict the mechanical behavior of the material. This research presents the capabilities of artificial neural networks (NN) in predicting fiber orientation tensor (FOT) during injection molding processes, with a focus on enhancing computational efficiency compared to traditional simulation methods. Three NN architectures are compared based on simulated injection molded plates, with the goal of predicting the effect of the plate geometry on the local fiber orientation. Results indicate that NN outperform the baseline assumption of aligned fibers and demonstrate significant potential for accurate FOT prediction. The computational efficiency of NN, especially during the prediction phase, showcases a reduction in processing time by a factor of 10<jats:sup>4</jats:sup> compared to traditional simulation methods. This research lays a foundation for further exploration into the feasibility of NN in partly replacing time-consuming simulations for practical applications in injection molding processes.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"39 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-04-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140570111","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Ines Mössinger, Lukas Raps, Daniel Fricke, Jonathan Freund, Miriam Löbbecke, Ashley R Chadwick
{"title":"Characteristics of in-situ automated fiber placement carbon-fiber-reinforced low-melt polyaryl ether ketone laminates part 1: Manufacturing influences","authors":"Ines Mössinger, Lukas Raps, Daniel Fricke, Jonathan Freund, Miriam Löbbecke, Ashley R Chadwick","doi":"10.1177/00219983241244882","DOIUrl":"https://doi.org/10.1177/00219983241244882","url":null,"abstract":"This study presents an investigation into mechanical and thermal properties, as well as the microstructure of Automated Fiber Placement-manufactured laminates using a novel carbon fiber-reinforced low-melt polyaryl ether ketone polymer material. The material’s lower melting temperature and lower melt viscosity as compared to established high-temperature thermoplastic materials as PEEK, promises favourable characteristics for the Automated Fiber Placement process. This work aims at in-situ consolidation and the influence of a heated tooling and a post process tempering step, which both turned out to be promising in previous investigations. Laminates were manufactured using a cold tooling, a heated tooling configuration, a cold tooling with a subsequent tempering process step and a hot-pressed reference laminate. Differential Scanning Calorimetry showed that crystallinity values more than doubled for the heated tooling and post process tempering configurations, compared to the cold tooling, reaching 24% and 30%, respectively. Mechanical strength values showed an increase in interlaminar shear strength and compression strength but did not increase to the same extent as was expected from the increase in crystallinity. With Scanning Electron Microscopy differences in the microscopic structure of the polymer matrix could be detected. While the post process tempering step leads to a mostly lamellar crystalline structure, the heated tooling configuration and the post process hot pressing induce a predominance of crystalline spherulites, which might positively affect the mechanical performance. Computed Tomography scans revealed a high amount of porosity in the in-situ-manufactured samples and unprocessed tape material, which likely mitigated the positive effect of increased crystallinity.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"6 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-04-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140570093","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Renaud Metz, Sofiane Terzi, Barbara Fayard, Jean-Louis Bantignies, Mehrdad Hassanzadeh
{"title":"Contribution to the percolation threshold study of Silicon carbide filled polydimethylsiloxane composites used for field grading application","authors":"Renaud Metz, Sofiane Terzi, Barbara Fayard, Jean-Louis Bantignies, Mehrdad Hassanzadeh","doi":"10.1177/00219983241246615","DOIUrl":"https://doi.org/10.1177/00219983241246615","url":null,"abstract":"The correlations between the electrical behavior and microstructural properties of samples consisting of particle composites fabricated from SiC particles embedded in a silicone matrix, were investigated using X-ray computed tomography. In the voltage field range 200-1000 V/mm, the measured conductivity as a function of SiC volume fraction exhibits two distinct gaps. Upon further investigations, we attribute these observations to percolation thresholds at the microscale. The first gap, corresponding to interconnections between SiC particles that were originally disconnected, is more significant at higher voltage; while the second one, resulting from shortening conductivity pathways between the external surfaces of the samples with the increase of SiC volume fraction, seems more sensitive to lower voltages and is correlated with a decrease of the tortuosity of the percolated SiC network.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"15 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-04-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140569999","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Dynamic responses and interactive failure mechanisms of carbon fiber composite face sheets/double-layer corrugated core sandwich structures under low-velocity impacts loading","authors":"Hangyan Wang, Jiayou Guo, Guangguang Zhang, Shuiting Zhou, Liange Ouyang","doi":"10.1177/00219983241246109","DOIUrl":"https://doi.org/10.1177/00219983241246109","url":null,"abstract":"A single-layer and double-layer corrugated core sandwich structure consisting of carbon fibre–reinforced polymer (CFRP) panels and aluminium alloy core layers was designed. Numerical simulations were carried out in HyperMesh/LsDyna, and the simulation results of single-layer and double-layer corrugated sandwich structure were compared with the experimental results to verify the reliability of the proposed numerical model. Compared with the results of single-layer and double-layer corrugated sandwich structure, the superiority of a double-layer corrugated sandwich structure in anti-collision performance is verified. Considering the effects of impact energy and impact position on impact force, energy absorption capacity, and failure mode, a series of low-velocity impact finite element simulations was carried out. It was found that the main failure mode of composite laminates included fibre damage, matrix damage and delamination, and core buckling. At the same impact position, the higher the impact energy, the greater the initial slopes of the contact force-time and absorbed energy-time curves, the higher the peak force, and the larger the energy absorption capacity. Under the same impact energy, when the impactor hit the wave crest of the sandwich structure, the damage to the structure was small; however, the maximum impact force on the structure was large (∼8 kN).","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"28 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-04-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140570264","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}