Mariam A. Al-Dhaheri, Wesley J. Cantwell, Imad Barsoum, Rehan Umer
{"title":"Characterization of relaxation behaviour of CF/PEKK aerospace composites using the time-temperature-crystallinity superposition principle","authors":"Mariam A. Al-Dhaheri, Wesley J. Cantwell, Imad Barsoum, Rehan Umer","doi":"10.1177/00219983241260555","DOIUrl":"https://doi.org/10.1177/00219983241260555","url":null,"abstract":"In this study, the Time-Temperature-Crystallinity Superposition Principle (TTCSP) was applied to determine the viscoelastic behavior of Thermo-rheological Complex Materials (TCM), specifically Carbon fibre/Poly-Ether-Ketone-Ketone (CF/PEKK) composites. The study investigated the effects of various parameters on the viscoelastic behavior of the composites, such as the degree of crystallinity after different melting temperatures, relaxation, and crystallization times. The TTCSP was utilized on the relaxation data to generate great-grand master curves for the degree of crystallinity for different laminate lay-ups. Hot press forming was employed to manufacture samples under different processing conditions, including various melting and cold crystallization temperatures. Differential Scanning Calorimetry (DSC) was employed to calculate the degree of crystallinity of CF/PEKK composites, while the Dynamic Mechanical Analyzer (DMA) was used to obtain the relaxation data. The generated great-grand master curves proved effective in predicting the relaxation behavior of the composites consolidated using single and double hold cycles at different melting temperatures and crystallization times, respectively. The great-grand master curves presented in this study can serve as valuable tool to calibrate key viscoelastic and/or thermo-viscoelastic material models for aerospace-grade CF/PEKK composites. These models are crucial for simulations aimed at predicting residual stresses and process-induced deformations during the thermoforming process.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"37 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141196640","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Tomás Barros Vasconcelos, José Leandro Correia Alves, Evans Paiva da Costa Ferreira, Raimundo Carlos Silverio Freire Júnior, José Daniel Diniz Melo
{"title":"Static and fatigue behavior of double-double glass/epoxy laminates","authors":"Tomás Barros Vasconcelos, José Leandro Correia Alves, Evans Paiva da Costa Ferreira, Raimundo Carlos Silverio Freire Júnior, José Daniel Diniz Melo","doi":"10.1177/00219983241261065","DOIUrl":"https://doi.org/10.1177/00219983241261065","url":null,"abstract":"Double-double (DD) configuration has been proposed as a new concept in which a double set of double helix [±ϕ/± ψ]<jats:sub>n</jats:sub> angles are stacked up to form a composite laminate. This concept promises significant advantages over conventional layups for composite design optimization and manufacturing. This experimental study evaluated the performance of two elastically in-plane equivalent glass/epoxy laminates suited for wind turbine blade applications: a quadriaxial (Quad) [±45/(0/90)<jats:sub>3</jats:sub>]<jats:sub>s</jats:sub> and a double-double (DD) [±15/±75]<jats:sub>4T</jats:sub>. Mechanical tests were performed under cyclic uniaxial tensile-tensile load using unnotched and open hole specimens. Delamination initiating from the free edges resulted in premature failure of the unnotched DD specimens. For open hole specimens, fatigue tests results obtained from both stacking sequences showed similar performance. Ultimately, the study presented constitutes a valuable contribution to the understanding of fatigue behavior of double-double glass/epoxy laminates subjected to tensile cyclic loading.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"47 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141196637","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Muhammad Ali Bablu, Nicholas E Nowak, James M Manimala
{"title":"Role of particle material and geometry in the ballistic performance of nanoparticle-impregnated Kevlar fabric","authors":"Muhammad Ali Bablu, Nicholas E Nowak, James M Manimala","doi":"10.1177/00219983241259130","DOIUrl":"https://doi.org/10.1177/00219983241259130","url":null,"abstract":"The possibility of enhancing the ballistic performance of aramid fabrics such as Kevlar through the impregnation of nanoparticles is well established. In this study, the influence of the nanoparticle’s specifications such as size, shape, and material on the underlying mechanisms is investigated. A colloid-based treatment process is used to impregnate dry nanoparticles into Kevlar fabric. Using a customized gas gun rig, neat and treated samples are tested to determine the kinetic energy absorbed. Silica, alumina, and zinc oxide nanoparticles ranging from 10 to 125 nm, with spherical or cylindrical shape are considered. Silica treated samples perform significantly better (83% increase in energy absorbed vs neat fabric) than alumina or zinc oxide treated samples, likely due to greater agglomeration between yarn interfaces leading to enhanced frictional mechanisms. The exit-face damaged zone area acts as a surrogate for energy absorbed as it correlates well across all samples. Compared to samples with three layers treated individually, samples with three layers treated together display a 21% enhancement in the energy absorbed. Specific energy absorbed for three layers treated together with 80-nm silica is nearly 3 times higher than that for the neat fabric. Samples with three layers treated together with 80-nm silica provide the same performance as the neat fabric for a projectile that is nearly 70 m/s faster. Hybrid structural materials such as nanoparticle-fabric composites offer a promising route to enhance ballistic performance without weight penalty, while being amenable to multifunctional applications.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"121 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141196580","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Simulation and on-line monitoring using optical fiber Bragg grating sensors of temperature history during laser-assisted automated fiber placement","authors":"Dacheng Zhao, Weiping Liu, Jiping Chen, Songhao Zhu, Yang Yang, Guangquan Yue","doi":"10.1177/00219983241259849","DOIUrl":"https://doi.org/10.1177/00219983241259849","url":null,"abstract":"Automated fiber placement (AFP) in situ consolidation (ISC) of thermoplastic composite possess the potential to reduce manufacturing costs and improve manufacturing efficiency. The properties of composite manufactured by the ISC are affected by several mechanisms including polymer degradation, crystallization, intimate contact, polymer healing and void dynamics. All these mechanisms are directly affected by the temperature history. Consequently, the control and accurate measurement of temperature history during ISC are particularly important for improving the properties of composite. In this study, a simplified three-dimensional transient heat transfer model was established. The effect of tool temperature and placement speed on the temperature history and peak temperature were predicted. Simultaneously, an online temperature monitoring system was built and the optical Fiber Bragg Grating sensors (FBGS) was used to measure the temperature history. The results indicated that the predicted results of the model were consistent with the measured results, the error was below 8%. In addition, the temperature history of layers was significantly affected by the tool temperature and placement speed. The temperature of the layers decreased to near the tool temperature after cooling, and a higher tool temperature increasing its peak temperature because of the reduce of the cooling rate. On the contrary, an increase in placement speed will reduce the peak temperature of the layers.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"42 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-05-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141196582","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"The investigation of deflection behavior in carbon/epoxy and glass/epoxy composite laminates under low-velocity impact with small projectiles","authors":"Mohammad Javad Ramezani","doi":"10.1177/00219983241256334","DOIUrl":"https://doi.org/10.1177/00219983241256334","url":null,"abstract":"This study examined the impact behavior of carbon/epoxy and glass/epoxy composite laminates with 2, 4, and 6 mm thicknesses under low-velocity tests. The investigation involved subjecting the composite laminates under small-impact loads using spherical, cylindrical, and conical steel projectiles, each weighing 3 g. The impacts conducted at 29.5, 36.5, and 51 m/s velocities. This investigation modeled using finite element (FE) methods and analytical approaches. In the analytical method, the mass and spring model used for the impact of small projectiles. The research findings revealed that, in 2 mm thick carbon/epoxy composite laminates, the maximum deflection at the mid-point induced by a spherical projectile was 1.37 mm. This value exhibited a 48.91% and 19.13% increase compared to impacts with cylindrical and conical projectiles, respectively. Additionally, a comprehensive examination of delamination across all samples indicated the maximum delamination occurrence in glass/epoxy samples, showcasing lower impact resistance than carbon/epoxy laminates. Notably, with an increase in thickness, the delamination phenomenon in the samples exhibited a decreasing trend. In addition, the maximum value of delamination in the composite laminates were with spherical, conical, and cylindrical projectiles respectively, and also, there was an excellent convergence between FE and analytical results.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"51 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-05-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141196564","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Mechanical behavior of glass fiber-reinforced hollow glass particles filled epoxy composites under thermal loading","authors":"Anandakumar Paramasivam, Krishnan Kanny, Mohan Turup Pandurangan, Velmurugan Ramachandran","doi":"10.1177/00219983241259113","DOIUrl":"https://doi.org/10.1177/00219983241259113","url":null,"abstract":"The use of hollow glass particle-filled fiber-reinforced composites for aircraft applications requires proper understanding of their behavior under in-service temperature conditions in order to exploit their usage in the exterior parts of aircraft and other space vehicles. In this study, the glass fiber reinforced composites containing 0–30 vol% of glass microspheres were subjected to testing for monotonic tensile and flexural loading from room temperature to the test temperature (40°C – 120°C). The evolution of microscopic damage under different temperatures was elucidated by digital image correlation (DIC) strain fields. The strain fields revealed a transition from homogeneous to non-homogeneous pattern as the temperature increases due to softening of the matrix. As the glass microsphere contents in the matrix increased, the tensile and flexural properties of the composites decreased, and their reduction was highest for the specimen containing a 30 vol% microsphere by volume. The tensile properties are slightly decreased by increasing the temperature. The tensile specimens tested at room temperature exhibited limited delamination and fiber pullout, while extensive delamination and fiber splitting occurred in the specimens tested at 120°C. The flexural results of the glass fiber reinforced composite specimens exposed at 120°C demonstrated a considerable decrease in flexural strength compared with room temperature for 0 vol%, 10 vol%, 20 vol% and 30 vol% glass microsphere volume fraction. Finally, the Weibull parametric investigation was performed to model the degradation of modulus for various GMS contents with temperature variations.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"51 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-05-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141196639","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Lasse Malaske, Lucian-Attila Blaga, Luciano Bermann, Bilal Ahmad, Xiang Zhang, Benjamin Klusemann
{"title":"Feasibility study of friction stir joining of aluminium with carbon fibre reinforced thermoplastic composite","authors":"Lasse Malaske, Lucian-Attila Blaga, Luciano Bermann, Bilal Ahmad, Xiang Zhang, Benjamin Klusemann","doi":"10.1177/00219983241254889","DOIUrl":"https://doi.org/10.1177/00219983241254889","url":null,"abstract":"During the last decades, environmental concerns and limited resources have set focus of research on lightweight, mechanically high-performing structures for the transportation industry, in order to reduce fuel consumptions and CO<jats:sub>2</jats:sub> emissions. Friction Stir Joining (FSJ), as a variant of the Friction Stir Welding (FSW), is an innovative friction-based joining technique for metal-composite hybrid structures. Joining in the plasticized state below the melting temperature of the metal leads to a comparatively small heat-affected zone, so that only minor metallurgical changes occur. Additionally, only a short processing time and no additional weight in form of fasteners is needed. The main objective of this study is to evaluate the feasibility of metal-composite structures via FSJ, intending to enable a macro-mechanical interlocking bonding mechanism. Main focus was given to the integration of an aluminium nub inserted in a carbon fiber-reinforced polyphenylene sulfide (CF-PPS) sheet, to ensure sufficient plasticization of the aluminium part and no degradation in the polymer part. Residual stress arising from the friction stir joining process was also characterised using the Contour method. In this study, aluminium alloy 6082-T6 and CF-PPS composite sheets were used to produce long lap joints. Results have shown that the joints were created at almost constant peak temperature slightly above the melting temperature of the PPS but no physical-chemical changes were detected in the PPS. In addition, the influence of a PPS film as interlayer between the sheets was investigated in order to explore a method for preventing galvanic corrosion. Preliminary results indicate that it is not possible to integrate a metal nub to the CF-PPS without interrupting the PPS film. However, it is possible to create a nub within the PPS film.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"70 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-05-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141171081","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Reciprocating dry sliding wear behaviour of BN@MXene@AA7075 composites","authors":"Muhammet Mevlüt Karaca, Safa Polat, İsmail Esen","doi":"10.1177/00219983241257665","DOIUrl":"https://doi.org/10.1177/00219983241257665","url":null,"abstract":"Aluminium alloys are preferred in various fields, especially in the aviation and automotive sectors, due to their lightweight and durable nature. However, their usage is limited due to weak tribological properties such as low hardness and high adhesion tendency against steel. In order to overcome this deficiency, this study aimed to develop AA7075 matrix composites reinforced with BN and MXene. The productions were conducted by powder metallurgy method with these reinforcements in different ratios, both together and separately. The produced composites were characterized primarily by XRD and SEM analyses, followed by measurement of density and porosity values. Wear tests were conducted using the reciprocating ball-on-flat method, at a frequency of 3 Hz, a sliding distance of 100 m, and a stroke distance of 5 mm, with Inox steel ball. The highest improvement in wear rate was realized under 5 N load at 5 wt.% reinforcement ratios of 48% and 42% for BN and MXene, respectively. When 2 wt% BN and MXene reinforcements were applied together, the improvement rate remained around 34%. It can be said that BN and MXene show promising results by providing significant improvements compared to their counterparts in the literature, with MXene especially warranting further investigation.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"97 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-05-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141171072","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Investigation of the hybridization effect on mechanical properties of natural fiber reinforced biosourced composites","authors":"Nihel Ketata, Mohsen Ejday, Yves Grohens, Bastien Seantier, Noamen Guermazi","doi":"10.1177/00219983241255751","DOIUrl":"https://doi.org/10.1177/00219983241255751","url":null,"abstract":"Hybridizing the natural fibers with stronger synthetic fibers could significantly improve the properties of the natural fiber-reinforced composites. The improved mechanical capabilities of fiber reinforced polymers result from the fiber’s capacity for withstanding a more substantial portion of the mechanical load compared to the matrix it replaces. In order to guarantee the efficient transfer of the mechanical load from the matrix to the reinforcement, it is necessary to incorporate a fibrous filler. Transference takes place when the length of the fiber is longer than a specific critical length. Fibers which are shorter than the critical length will pull out from the matrix when tested to a tensile load. In some cases, complete transfer of the load is not performed. The goal of this study is to learn more about flax (FF), glass (GF), and mixtures of flax and glass (FF + GF) short fiber-reinforced PLA-PBS composites. This is performed to find out how the flax/glass combination affects the mechanical properties of PLA-PBS-reinforced short fiber composites. In order to extend their use for industrial applications, these composites were manufactured via extrusion and, afterward, injection molding. Fiber aspect ratios were followed after compounding and injection processing. The analysis of fiber lengths reveals a noteworthy observation: the proportion of fibers exceeding their critical length of 531 µm and 772 µm for FF and GF, respectively, is more significant when flax fibers (FF) and glass fibers (GF) are combined compared to when they reinforce the composite individually. Specifically, the composite containing both FF and GF exhibits a higher percentage of fibers surpassing their critical length, compared to their individual reinforcement in the composite. The results reveal that 27% of individually extracted single FF exceed their critical length, whereas a higher proportion, at 34%, is observed when FF is part of the composite mixture. In contrast, the critical length is surpassed by only 4% of individually extracted single GF, whereas the combined presence of GF in the composite results in a notably higher percentage, at 19%. The tensile properties of these composites were investigated considering the effect of the hybridization by flax/glass short fibers. It was noted that the tensile properties of the hybrid composites increase comparing to the flax composites from 42.4 MPa to 53 MPa for the tensile strength and from 4.9 GPa to 5.4 GPa for the tensile modulus. In contrast, the elongation at break of the hybrid composites decreases from 1.7% to 1.5% with the incorporation of glass fibers. The experimental results were compared with the predictions of the mixture law and the Cox-Krenchel model. The findings indicate that mixing synthetic fibers with natural fibers is an excellent approach to enhancing mechanical properties.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"66 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-05-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141152730","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Anisotropic auxetic composite laminates: A polar approach","authors":"Paolo Vannucci","doi":"10.1177/00219983241256335","DOIUrl":"https://doi.org/10.1177/00219983241256335","url":null,"abstract":"The problem of obtaining anisotropic auxetic composite laminates, i.e. having a negative Poisson’s ratio for at least some directions, is examined in this paper. In particular, the possibility of obtaining auxeticity stacking uni-directional identical plies is considered. It is shown that if the ply is composed by isotropic matrix and fibers, then it is impossible to obtain totally auxetic orthotropic laminates, i.e. auxeticity for each direction, unless at least one among matrix and fibers is auxetic itself. Moreover, it is shown what are the conditions, in terms of the mechanical properties of the constituents and of the volume fraction of the fibers, to fabricate uni-directional plies with which to realize laminates having a negative Poisson’s ratio for some directions. Several existing materials are also examined. All the analysis is done using the polar formalism, very effective for the study of plane anisotropic problems.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"3 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-05-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141152735","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}