Biomaterial investigations in dentistry最新文献

{"title":"Monowave and polywave light-curing of bulk-fill resin composites: degree of conversion and marginal adaptation following thermomechanical aging.","authors":"Sheila Celia Mondragón Contreras,&nbsp;Ana Luiza Barbosa Jurema,&nbsp;Evaniele Santos Claudino,&nbsp;Eduardo Bresciani,&nbsp;Taciana Marco Ferraz Caneppele","doi":"10.1080/26415275.2021.1937181","DOIUrl":"https://doi.org/10.1080/26415275.2021.1937181","url":null,"abstract":"<p><p><i>Aim:</i> This study aimed to evaluate the effect of polymerization with either a monowave (MW) or a polywave (PW) light-curing unit (LCU) on the degree of conversion (DC) and marginal adaptation following thermomechanical aging of an ormocer bulk-fill resin composite (RC) (Admira fusion X-tra Bulk Fill - AB), a methacrylate-based bulk-fill RC (Tetric N-Ceram Bulk Fill - TB) and a conventional RC (Tetric N-Ceram - TC). <i>Methods:</i> DC was assessed in five samples of each RC using Fourier transform infrared spectroscopy. For determination of marginal adaptation, standard preparations were made in 60 bovine incisors, divided into three groups, according to the RC. The bulk-fill RC was inserted in a single increment of 4 mm. In contrast, the conventional RC was inserted in three increments. Marginal gap was evaluated after thermomechanical aging. Data were analyzed using a two-way analysis of variance (ANOVA) and Tukey's tests for multiple comparisons (<i>α</i> = 0.05). <i>Results:</i> The two-way ANOVA showed a significant effect (<i>p</i><.05) of the RC factor but not of the LCU factor. The Tukey test showed that TB had the significantly lowest DC followed by TC, and with AB having the significantly highest DC. For the marginal adaptation, a significant effect was found for the LCU factor and the for the interaction RC × LCU (<i>p</i><.05). Groups light-cured with PW showed significantly wider marginal gaps than MW. TC presented wider marginal gaps (17.36 µm) when cured with PW than when cured with MW (13.05 µm). The two bulk-fill RC resulted in similar marginal gap formation to each other. <i>Conclusion:</i> The ormocer-based bulk-fill RC showed a higher DC than the methacrylate-based bulk-fill RC but similar marginal adaptation. The LCU, MW or PW, had no significant influence on the DC, and no relevance on the marginal adaptation.</p>","PeriodicalId":72378,"journal":{"name":"Biomaterial investigations in dentistry","volume":" ","pages":"72-78"},"PeriodicalIF":0.0,"publicationDate":"2021-07-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/26415275.2021.1937181","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39291814","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Fracture resistance of resin based and lithium disilicate endocrowns. Which is better? - A systematic review of <i>in-vitro</i> studies.","authors":"Joshna Beji Vijayakumar,&nbsp;Preethi Varadan,&nbsp;Lakshmi Balaji,&nbsp;Mathan Rajan,&nbsp;Rajeswari Kalaiselvam,&nbsp;Sindhu Saeralaathan,&nbsp;Arathi Ganesh","doi":"10.1080/26415275.2021.1932510","DOIUrl":"https://doi.org/10.1080/26415275.2021.1932510","url":null,"abstract":"<p><p><b>Objectives:</b> The primary objective of this systematic review is to compare the fracture resistance of lithium disilicate (LDS)-based endocrowns and resin-based (RB) endocrowns of in-vitro studies, and the secondary objective is to compare their catastrophic failures. <b>Materials and Methods:</b> The review protocol was registered in the P ROSP ERO database (CRD42020166201). A comprehensive literature search was done in PubMed, Cochrane, EBSCOhost and Google Scholar using key terms. Only in-vitro studies that compared fracture resistance of LDS-based endocrowns and indirect RB endocrowns in molars were included. Data extraction, risk of bias assessment and qualitative analysis of the included studies were performed. <b>Results:</b> Five studies were included in this systematic review. The overall risk of bias for the included studies was moderate. Under axial loading, RB endocrowns showed similar fracture resistance when compared with LDS endocrowns. However, they showed better fracture resistance when compared with zirconia reinforced lithium silicate (ZLS) endocrowns. Furthermore, RB endocrowns showed fewer catastrophic failures than LDS-based endocrowns. <b>Conclusions:</b> RB endocrowns have similar or better fracture resistance and fewer catastrophic failures when compared to LDS-based endocrowns.</p>","PeriodicalId":72378,"journal":{"name":"Biomaterial investigations in dentistry","volume":" ","pages":"104-111"},"PeriodicalIF":0.0,"publicationDate":"2021-07-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/26415275.2021.1932510","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39291815","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Influence of different tooth preparation and bonding techniques on the fracture resistance of tooth fragment reattachment.","authors":"Shaymaa M Nagi,&nbsp;Sherif M Khadr","doi":"10.1080/26415275.2021.1952873","DOIUrl":"https://doi.org/10.1080/26415275.2021.1952873","url":null,"abstract":"<p><strong>Purpose: </strong>comparing the influence of different tooth preparation and bonding techniques on the fracture resistance of tooth fragment reattachment.</p><p><strong>Materials and method: </strong>Ninety bovine central incisors were selected. Fifteen teeth act as a control (Group A). Experimental specimens were sectioned at the mesial-incisal proximal edge 3 mm from the incisal edge in a labio-lingual direction at 25degree inclination apically. Experimental specimens were then divided into five groups according to the tooth reattachment techniques utilized; Group B: no tooth preparation + Cured bond + Flowable composite; Group C: no tooth preparation + Uncured bond + Flowable composite; Group D: Bevel + bond + Flowable composite; Group E: Over-contouring + bond + Nanohybrid composite; Group F: Over-contouring + bond + Flowable composite. Specimens were subjected to thermocycling between 5 °C and 55 °C for 500 cycles with 30 sec. dwell time. Fracture strength was evaluated using universal testing machine. Data was analyzed using One-way ANOVA.</p><p><strong>Results: </strong>There was a statistically significant difference between Group A and all the experimental groups, <i>p</i> < .001. Group E showed the highest statistically significant fracture resistance mean value compared to other experimental groups, while the lowest mean value was found in Group B.</p><p><strong>Conclusion: </strong>Though, none of the tested techniques resulted in fracture resistance similar to that of intact teeth, over-contouring technique with nanohybrid composite application showed better performances compared to the other techniques tested in the current study. Bonding plus flowable resin composite application with no additional tooth preparation and placement of a bevel are not suggested due to the low fracture strength achieved.</p>","PeriodicalId":72378,"journal":{"name":"Biomaterial investigations in dentistry","volume":" ","pages":"112-118"},"PeriodicalIF":0.0,"publicationDate":"2021-07-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/26415275.2021.1952873","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39276530","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Marginal and internal fit of crowns based on additive or subtractive manufacturing.","authors":"Yasser Haddadi,&nbsp;Bahram Ranjkesh,&nbsp;Flemming Isidor,&nbsp;Golnosh Bahrami","doi":"10.1080/26415275.2021.1938576","DOIUrl":"10.1080/26415275.2021.1938576","url":null,"abstract":"<p><strong>Objective: </strong>To assess the marginal and internal fit of crowns manufactured by additive and subtractive manufacturing technique.</p><p><strong>Materials and methods: </strong>Twenty extracted teeth prepared for complete coverage crowns were scanned with an intra-oral scanner (Omnicam, DentsplySirona). For the subtractive manufacturing (SM) group, ten crowns were manufactured in a hybrid resin block (Vita Enamic, Vita Zahnfabrik). For the additive manufacturing (AM) group, the crowns were manufactured in a hybrid resin material (NextDent C&B, 3D systems). The design parameters were identical for the two groups. The marginal and internal fit (determined at the axial wall, the cusp tip and occlusally) was assessed before cementation with the replica technique and after cementation under stereomicroscope after sectioning of the crowned teeth.</p><p><strong>Results: </strong>For the SM group, the marginal fit was 91 µm (±28 µm) before cementation and 85 µm (±18 µm) after cementation. In the AM group, the marginal fit was 75 µm (±29 µm) before cementation and 71 µm (±18 µm) after cementation. The differences were not statistically significant. As regards the internal fit, the fit at the axial wall was statistically significantly better in the SM group than in the AM group (<i>p</i>=.009 before cementation and .03 after cementation). Occlusally the fit in the AM group was significantly better than in the SM group after cementation (<i>p</i><.001).</p><p><strong>Conclusion: </strong>Within the limitations of the current study, the marginal fit of additively manufactured crowns is comparable to crowns manufactured with chair-side subtractive technique and within the clinically acceptable range. As regards the internal fit no one technique was consistently superior.</p>","PeriodicalId":72378,"journal":{"name":"Biomaterial investigations in dentistry","volume":" ","pages":"87-91"},"PeriodicalIF":0.0,"publicationDate":"2021-06-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/26415275.2021.1938576","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39166630","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"A three-year randomized clinical trial evaluating direct posterior composite restorations placed with three self-etch adhesives.","authors":"Joseph Sabbagh,&nbsp;Layal El Masri,&nbsp;Jean Claude Fahd,&nbsp;Paul Nahas","doi":"10.1080/26415275.2021.1939034","DOIUrl":"https://doi.org/10.1080/26415275.2021.1939034","url":null,"abstract":"<p><strong>Aim: </strong>To compare the clinical performance of composite restorations placed with a universal adhesive, one-step and two-step self-etch adhesives in class I and II posterior cavities.</p><p><strong>Materials and methods: </strong>In this <i>in vivo</i> study, 46 volunteers presenting with at least three carious lesions were included. Each participant received the three restorative systems: universal adhesive/nanofilled composite (Scotchbond Universal/Filtek Z350 XT: SBU/FZXT), one-step self-etch adhesive/microhybrid composite (G-aenial bond/G-aenial Posterior: GB/GP) and the two-step self-etch adhesive/nanohybrid composite (OptiBond XTR/Herculite Ultra: OBX/HU). The adhesives were all placed in self-etch mode. In total, 138 restorations were evaluated at baseline and at 6,12 and 36 months using the modified United States Public Health Service criteria. Data were analysed using Kruskal-Wallis, Mann-Whitney U, Friedman and Wilcoxon non-parametric tests (<i>p</i> < .05). Ninety-one restorations were evaluated at 36 months.</p><p><strong>Results: </strong>Seven restorations, three SBU/FZXT, three GB/GP and one OBX/HU failed during this study. The reasons for failure were marginal fracture and secondary caries. SBU/FZXT restorations showed significant marginal deterioration in all parameters. Overall success rates were: 93.5% (SBU/FZXT), 96.6% (GB/GP) and 96.8% (OBX/HU).</p><p><strong>Conclusions: </strong>After three years, the three restorative systems have comparable clinical effectiveness and success rates, except for the marginal integrity, that was suboptimal for both the SBU/FZXT and GB/GP restorations in comparison to the OBX/HU restorations.</p>","PeriodicalId":72378,"journal":{"name":"Biomaterial investigations in dentistry","volume":" ","pages":"92-103"},"PeriodicalIF":0.0,"publicationDate":"2021-06-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/26415275.2021.1939034","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39166631","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Bond strength between titanium and polymer-based materials adhesively cemented.","authors":"Camilla Johansson,&nbsp;Aleksandra Håkansson,&nbsp;Evaggelia Papia","doi":"10.1080/26415275.2021.1937182","DOIUrl":"https://doi.org/10.1080/26415275.2021.1937182","url":null,"abstract":"<p><p>The aim was to evaluate the bond strength between titanium and polymer-based materials for prosthetic restorations, cemented with different adhesive cement systems. Eight groups with 13 specimens in each group were included. Each specimen consisted of two parts: a cylinder of titanium resembling a titanium base, and a cylinder of one of two polymer-based materials Micro Filled Hybrid (MFH) or Telio CAD and cemented with one of four adhesive cement systems, namely Multilink Hybrid Abutment, Panavia V5, RelyX Ultimate and G-Cem LinkAce. The titanium was sandblasted with 50 µm Al₂O₃ and treated according to each cement manufacturer's recommendations. The polymer-based materials were pre-treated according to the manufacturer's instructions including sandblasting for MFH. After cementation, the groups were water stored for one day before thermocycling: 5000 cycles in 5-55 °C. A shear bond strength test was performed (crosshead speed 0.5 mm/min) and data was analysed with one-way ANOVA, Tukey's test. Telio CAD cemented with Panavia V5 and G-Cem LinkAce showed significantly lower bond strength compared to all other groups, due to spontaneous debonding. The highest numerical bond strength was found in the group of MFH cemented with RelyX Ultimate or with G-Cem LinkAce. Generally, the Telio CAD groups showed lower bond strength values than the MFH groups. The conclusions are that pre-treatment methods and choice of cement system are of importance for polymer-based materials for prosthetic restorations. The bond strength is adequate for provisional cementation irrespective of cement system when pre-treating by sandblasting, but cement dependent without sandblasting.</p>","PeriodicalId":72378,"journal":{"name":"Biomaterial investigations in dentistry","volume":" ","pages":"79-86"},"PeriodicalIF":0.0,"publicationDate":"2021-06-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/26415275.2021.1937182","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39156764","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"A comparative evaluation of penetration depth and surface microhardness of Resin Infiltrant, CPP-ACPF and Novamin on enamel demineralization after banding: an <i>in vitro</i> study.","authors":"Nishita Rana,&nbsp;Namita Singh,&nbsp;Shaila,&nbsp;Abi M Thomas,&nbsp;Rajan Jairath","doi":"10.1080/26415275.2021.1919119","DOIUrl":"https://doi.org/10.1080/26415275.2021.1919119","url":null,"abstract":"<p><strong>Background: </strong>The field of dentistry has been revolutionized by various concepts. Minimal invasive dentistry is the preferred treatment approach in the present era; therefore, various techniques have been advocated to arrest caries lesions at an early stage on the grounds of better understanding of the dynamic nature of dental caries. Thus, study was conducted to compare and evaluate the penetration depth and enamel microhardness of Resin Infiltrant, CPP-ACPF and Novamin on artificial demineralized enamel surface after orthodontic banding.</p><p><strong>Material and methods: </strong>Eighty extracted sound premolars were banded. The bands were cemented with type 1 GIC and further divided into - Group I: Resin Infiltrant, Group II: CCP-ACPF, Group III: Novamin and Group IV: Control. The samples were incubated for 30 days and then thermocycled. A window of 4 mm × 4 mm was prepared on the buccal surface of samples and artificially demineralized for 4 weeks. A single application was made for Resin Infiltrant, while Novamin and CCP-ACPF were applied twice daily. These samples were otherwise immersed in artificial saliva, and this was protocol was observed for 14 days. For the evaluation of penetration depth, 10 samples from each group were bucco-lingually sectioned and immersed in methylene blue dye solution for 24 h and then evaluated under stereomicroscope. For the enamel surface microhardness, remaining 10 samples from each group were embedded in acrylic resin with outer buccal surface exposed and were tested by a using digital Micro-Vickers hardness tester.</p><p><strong>Results: </strong>All groups showed a significant difference in the depth of dye penetration and surface microhardness compared to the control group. As compared to the other tested groups, Resin Infiltrant exhibited the highest significant reduction in demineralization and increased microhardness. Novamin had a deeper penetration and increase in microhardness as compared to CCP-ACPF.</p><p><strong>Conclusion: </strong>Resin Infiltrant exhibited the highest potential to impede caries and constitutes a competent aerosol free micro-invasive strategy for combating non cavitated lesions approaching the outer layer dentine which are too advanced for remineralizing agents but do not necessarily require any drilling of tooth.</p>","PeriodicalId":72378,"journal":{"name":"Biomaterial investigations in dentistry","volume":" ","pages":"64-71"},"PeriodicalIF":0.0,"publicationDate":"2021-06-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/26415275.2021.1919119","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39114797","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Barrier membranes for tissue regeneration in dentistry.","authors":"Jun-Ichi Sasaki, Gabriela L Abe, Aonan Li, Pasiree Thongthai, Ririko Tsuboi, Tomoki Kohno, Satoshi Imazato","doi":"10.1080/26415275.2021.1925556","DOIUrl":"10.1080/26415275.2021.1925556","url":null,"abstract":"<p><p><b>Background:</b> In dentistry, barrier membranes are used for guided tissue regeneration (GTR) and guided bone regeneration (GBR). Various membranes are commercially available and extensive research and development of novel membranes have been conducted. In general, membranes are required to provide barrier function, biosafety, biocompatibility and appropriate mechanical properties. In addition, membranes are expected to be bioactive to promote tissue regeneration. <b>Objectives:</b> This review aims to organize the fundamental characteristics of the barrier membranes that are available and studied for dentistry, based on their components. <b>Results:</b> The principal components of barrier membranes are divided into nonbiodegradable and biodegradable materials. Nonbiodegradable membranes are manufactured from synthetic polymers, metals or composites of these materials. The first reported barrier membrane was made from expanded polytetrafluoroethylene (e-PTFE). Titanium has also been applied for dental regenerative therapy and shows favorable barrier function. Biodegradable membranes are mainly made from natural and synthetic polymers. Collagens are popular materials that are processed for clinical use by cross-linking. Aliphatic polyesters and their copolymers have been relatively recently introduced into GTR and GBR treatments. In addition, to improve the tissue regenerative function and mechanical strength of biodegradable membranes, inorganic materials such as calcium phosphate and bioactive glass have been incorporated at the research stage. <b>Conclusions:</b> Currently, there are still insufficient guidelines for barrier membrane choice in GTR and GBR, therefore dentists are required to understand the characteristics of barrier membranes.</p>","PeriodicalId":72378,"journal":{"name":"Biomaterial investigations in dentistry","volume":" ","pages":"54-63"},"PeriodicalIF":0.0,"publicationDate":"2021-05-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8158285/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"39008148","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"The effect of refractive index of fillers and polymer matrix on translucency and color matching of dental resin composite.","authors":"Maija Oivanen,&nbsp;Filip Keulemans,&nbsp;Sufyan Garoushi,&nbsp;Pekka K Vallittu,&nbsp;Lippo Lassila","doi":"10.1080/26415275.2021.1906879","DOIUrl":"https://doi.org/10.1080/26415275.2021.1906879","url":null,"abstract":"<p><strong>Objective: </strong>When restorative resin composites absorb light from the surrounding tooth structures, it creates a color-match, which is known as 'a chameleon effect'. In this study, series of co-monomer mixtures were prepared with an increasing refraction index (RI) and mixed with glass fillers. The aim of this study was to optimize the mismatch of RI of resin/fillers to create the chameleon effect.</p><p><strong>Materials and methods: </strong>BisGMA/TEGDMA resins were prepared with seven different mix fractions from 20 to 80%. Two different series (A&B) of submicron (Ø 0.7 μm) silanized fillers (70 wt%) (A: Schott RI = 1.53, B: Esschem RI = 1.54) were mixed with resins (30 wt%). Disc-shaped specimens (1 mm thickness, Ø10 mm) for each composite combination (<i>n</i> = 3) were prepared and light cured for 20 s. Commercial resin composite (OmniChroma, Tokuyama Dental) was used as control. The translucency parameter (TP) was measured using a spectrophotometer. The color matching abilities of the experimental composites were visually analyzed. Data were statistically analyzed using ANOVA.</p><p><strong>Results: </strong>The composition of resin and type of fillers had a statistically significant effect on TP values (<i>p</i> < .05). The highest TP values were achieved around 50%-50% fractions of Bis-GMA and TEGDMA for series A and around 60%-40% fraction of Bis-GMA and TEGDMA for series B. Data showed that a high or low fraction of BisGMA resulted in a low translucent composite. Experimental resin composite (80% Bis-GMA) from series A was behaving similarly to Omnichroma in reference to TP values and color matching.</p><p><strong>Conclusions: </strong>Including fillers with RI of 1.53 into BisGMA/TEGDMA resin with RI of 1.524 resulted in composite resin providing a good color match with surrounding structure 'chameleon effect'.</p>","PeriodicalId":72378,"journal":{"name":"Biomaterial investigations in dentistry","volume":" ","pages":"48-53"},"PeriodicalIF":0.0,"publicationDate":"2021-04-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/26415275.2021.1906879","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"38875147","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Studies of the early stages of the dynamic setting process of chemically activated restorative glass-ionomer cements.","authors":"Fernanda M Tsuzuki,&nbsp;Renata C Pascotto,&nbsp;Luis C Malacarne,&nbsp;Antonio C Bento,&nbsp;Antonio Medina Neto,&nbsp;Lidiane Vizioli de Castro-Hoshino,&nbsp;Monique Souza,&nbsp;John W Nicholson,&nbsp;Mauro L Baesso","doi":"10.1080/26415275.2021.1898964","DOIUrl":"https://doi.org/10.1080/26415275.2021.1898964","url":null,"abstract":"<p><strong>Objective: </strong>To evaluate the early stages of the setting process of chemically activated restorative glass-ionomer cements (GICs).</p><p><strong>Material and methods: </strong>Five GICs were evaluated (<i>n</i> = 5): Equia Forte (GC), Equia Forte HT (GC), Ketac Universal (3M ESPE), Maxxion R (FGM) and Riva Self Cure (SDI) by Thermography, Fourier Transform Infrared Attenuated Total Reflectance Spectroscopy (FTIR-ATR) and Gillmore needle indentation mechanical testing. The FTIR-ATR spectra showed the formation of metal carboxylates within the cements and enabled the stabilization time (ST) to be determined and the thermographic camera measured the temperature field images in the sample. Data were statistically analyzed by ANOVA and Tukey-Kramer (<i>α</i> = 5%).</p><p><strong>Results: </strong>The Gillmore needle test showed that the order of hardening was opposite to the order of ST values determined by FTIR. The results with the thermographic camera showed two stages of temperature variation, which coincided with the evolution of specific infrared bands. The exception was Maxxion R, which showed only a single step change in temperature.</p><p><strong>Conclusion: </strong>The early stages of the GIC setting reaction show temperature changes, both endothermic and exothermic, at specific times, confirming the occurrence of individual chemical reactions. The early setting involves reactions other than carboxylate formation.<b>Significance</b>: This study gives further detail of the early stages of the setting of GICs, and past research regarding the setting reaction of GIC.</p>","PeriodicalId":72378,"journal":{"name":"Biomaterial investigations in dentistry","volume":" ","pages":"39-47"},"PeriodicalIF":0.0,"publicationDate":"2021-04-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/26415275.2021.1898964","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"38875146","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}