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Crystal structure of tin(II) perchlorate trihydrate. 三水合高氯酸锡的晶体结构。
IF 0.9
Acta crystallographica. Section E, Structure reports online Pub Date : 2014-11-12 eCollection Date: 2014-12-01 DOI: 10.1107/S1600536814024283
Erik Hennings, Horst Schmidt, Martin Köhler, Wolfgang Voigt
{"title":"Crystal structure of tin(II) perchlorate trihydrate.","authors":"Erik Hennings,&nbsp;Horst Schmidt,&nbsp;Martin Köhler,&nbsp;Wolfgang Voigt","doi":"10.1107/S1600536814024283","DOIUrl":"https://doi.org/10.1107/S1600536814024283","url":null,"abstract":"<p><p>The title compound, [Sn(H2O)3](ClO4)2, was synthesized by the redox reaction of copper(II) perchlorate hexa-hydrate and metallic tin in perchloric acid. Both the trigonal-pyramidal [Sn(H2O)3](2+) cations and tetra-hedral perchlorate anions lie on crystallographic threefold axes. In the crystal, the cations are linked to the anions by O-H⋯O hydrogen bonds, generating (001) sheets. </p>","PeriodicalId":7117,"journal":{"name":"Acta crystallographica. Section E, Structure reports online","volume":null,"pages":null},"PeriodicalIF":0.9,"publicationDate":"2014-11-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1107/S1600536814024283","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"32946123","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 5
Crystal structure of tin(IV) chloride octa-hydrate. 八水合物氯化锡(IV)的晶体结构。
IF 0.9
Acta crystallographica. Section E, Structure reports online Pub Date : 2014-11-12 eCollection Date: 2014-12-01 DOI: 10.1107/S1600536814024271
Erik Hennings, Horst Schmidt, Wolfgang Voigt
{"title":"Crystal structure of tin(IV) chloride octa-hydrate.","authors":"Erik Hennings,&nbsp;Horst Schmidt,&nbsp;Wolfgang Voigt","doi":"10.1107/S1600536814024271","DOIUrl":"https://doi.org/10.1107/S1600536814024271","url":null,"abstract":"<p><p>The title compound, [SnCl4(H2O)2]·6H2O, was crystallized according to the solid-liquid phase diagram at lower temperatures. It is built-up of SnCl4(H2O)2 octa-hedral units (point group symmetry 2) and lattice water mol-ecules. An intricate three-dimensional network of O-H⋯O and O-H⋯Cl hydrogen bonds between the complex molecules and the lattice water molecules is formed in the crystal structure. </p>","PeriodicalId":7117,"journal":{"name":"Acta crystallographica. Section E, Structure reports online","volume":null,"pages":null},"PeriodicalIF":0.9,"publicationDate":"2014-11-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1107/S1600536814024271","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"32946125","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Crystal structure of 2-(2,4-di-chloro-phen-yl)-4-hydroxy-9-phenyl-sulfonyl-9H-carbazole-3-carbaldehyde. 2-(2,4-二氯苯基)-4-羟基-9-苯基磺基- 9h -咔唑-3-乙醛的晶体结构。
IF 0.9
Acta crystallographica. Section E, Structure reports online Pub Date : 2014-11-08 eCollection Date: 2014-12-01 DOI: 10.1107/S1600536814024064
M Umadevi, B M Ramalingam, R Yamuna, A K Mohanakrishnan, G Chakkaravarthi
{"title":"Crystal structure of 2-(2,4-di-chloro-phen-yl)-4-hydroxy-9-phenyl-sulfonyl-9H-carbazole-3-carbaldehyde.","authors":"M Umadevi,&nbsp;B M Ramalingam,&nbsp;R Yamuna,&nbsp;A K Mohanakrishnan,&nbsp;G Chakkaravarthi","doi":"10.1107/S1600536814024064","DOIUrl":"https://doi.org/10.1107/S1600536814024064","url":null,"abstract":"<p><p>In the title compound, C25H15Cl2NO4S, the di-chloro-phenyl ring is twisted by 68.69 (11)° from the mean plane of the carbazole ring system [r.m.s. deviation = 0.084 (2)°]. The hy-droxy group is involved in an intra-molecular O-H⋯O hydrogen bond, which generates an S(6) graph-set motif. In the crystal, pairs of C-H⋯Cl hydrogen bonds link mol-ecules into inversion dimers with an R (2) 2(26) motif. Weak C-H⋯O inter-actions further link these dimers into ribbons propagating in [100]. </p>","PeriodicalId":7117,"journal":{"name":"Acta crystallographica. Section E, Structure reports online","volume":null,"pages":null},"PeriodicalIF":0.9,"publicationDate":"2014-11-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257421/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"32944618","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Crystal structure of 2-[12-methyl-14-phenyl-10,13,14,16-tetra-aza-tetra-cyclo[7.7.0.0(2,7).0(11,15)]hexa-deca-1(16),2,4,6,9,11(15),12-heptaen-8-yl-idene]propandi-nitrile. 2-[12-甲基-14-苯基-10,13,14,16-四氮杂-四环[7.7.0.0(2,7).0(11,15)]六-十-1(16)，2,4,6,9,11(15)，12-庚-8-基烯]丙腈的晶体结构。
IF 0.9
Acta crystallographica. Section E, Structure reports online Pub Date : 2014-11-08 eCollection Date: 2014-12-01 DOI: 10.1107/S1600536814024167
Joel T Mague, Shaaban K Mohamed, Mehmet Akkurt, Hussein M S El-Kashef, Mustafa R Albayati
{"title":"Crystal structure of 2-[12-methyl-14-phenyl-10,13,14,16-tetra-aza-tetra-cyclo[7.7.0.0(2,7).0(11,15)]hexa-deca-1(16),2,4,6,9,11(15),12-heptaen-8-yl-idene]propandi-nitrile.","authors":"Joel T Mague, Shaaban K Mohamed, Mehmet Akkurt, Hussein M S El-Kashef, Mustafa R Albayati","doi":"10.1107/S1600536814024167","DOIUrl":"10.1107/S1600536814024167","url":null,"abstract":"<p><p>In the title mol-ecule, C22H12N6, the fused tetracyclic core shows a small lengthwise twist as indicated by the dihedral of 2.7 (2)° between the outer rings. In the crystal, mol-ecules stack along the b-axis direction via offset π-stacking [centroid-centroid distances = 3.5282 (13) and 3.5597 (14) Å] with the stacks weakly associated through C-H⋯N hydrogen bonds. The phenyl ring is rotationally disordered over two orientations with an occupancy ratio of 0.516 (4):0.484 (4). </p>","PeriodicalId":7117,"journal":{"name":"Acta crystallographica. Section E, Structure reports online","volume":null,"pages":null},"PeriodicalIF":0.9,"publicationDate":"2014-11-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1107/S1600536814024167","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"32945289","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Crystal structure of the ternary silicide Gd2Re3Si5. 三元硅化物Gd2Re3Si5的晶体结构。
IF 0.9
Acta crystallographica. Section E, Structure reports online Pub Date : 2014-11-08 eCollection Date: 2014-12-01 DOI: 10.1107/S1600536814024234
Vitaliia Fedyna, Roksolana Kozak, Roman Gladyshevskii
{"title":"Crystal structure of the ternary silicide Gd2Re3Si5.","authors":"Vitaliia Fedyna,&nbsp;Roksolana Kozak,&nbsp;Roman Gladyshevskii","doi":"10.1107/S1600536814024234","DOIUrl":"https://doi.org/10.1107/S1600536814024234","url":null,"abstract":"<p><p>A single crystal of the title compound, the ternary silicide digadolinium trirhenium penta-silicide, Gd2Re3Si5, was isolated from an alloy of nominal composition Gd20Re30Si50 synthesized by arc melting and investigated by X-ray single-crystal diffraction. Its crystal structure belongs to the U2Mn3Si5 structure type. All atoms in the asymmetric lie on special positions. The Gd site has site symmetry m..; the two Mn atoms have site symmetries m.. and 2.22; the three Si atoms have site symmetries m.., ..2 and 4.. . The coordination polyhedra of the Gd atoms have 21 vertices, while those of the Re atoms are cubo-octa-hedra and 13-vertex polyhedra. The Si atoms are arranged as tricapped trigonal prisms, bicapped square anti-prisms, or 11-vertex polyhedra. The crystal structure of the title compound is also related to the structure types CaBe2Ge2 and W5Si3. It can be represented as a stacking of Gd-centred polyhedra of composition [GdSi9]. The Re atoms form infinite chains with an Re-Re distance of 2.78163 (5) Å and isolated squares with an Re-Re distance of 2.9683 (6) Å. </p>","PeriodicalId":7117,"journal":{"name":"Acta crystallographica. Section E, Structure reports online","volume":null,"pages":null},"PeriodicalIF":0.9,"publicationDate":"2014-11-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1107/S1600536814024234","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"32946121","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal structure of betulinic acid methanol monosolvate. 白桦酸甲醇单溶剂化物的晶体结构。
IF 0.9
Acta crystallographica. Section E, Structure reports online Pub Date : 2014-11-08 eCollection Date: 2014-12-01 DOI: 10.1107/S1600536814023848
Wei Tang, Neng-Hua Chen, Guo-Qiang Li, Guo-Cai Wang, Yao-Lan Li
{"title":"Crystal structure of betulinic acid methanol monosolvate.","authors":"Wei Tang,&nbsp;Neng-Hua Chen,&nbsp;Guo-Qiang Li,&nbsp;Guo-Cai Wang,&nbsp;Yao-Lan Li","doi":"10.1107/S1600536814023848","DOIUrl":"https://doi.org/10.1107/S1600536814023848","url":null,"abstract":"<p><p>The title compound [systematic name: 3β-hy-droxy-lup-20(29)-en-28-oic acid methanol monosolvate], C30H48O3·CH3OH, is a solvent pseudopolymorph of a naturally occurring plant-derived lupane-type penta-cyclic triterpenoid, which was isolated from the traditional Chinese medicinal plant Syzygium jambos (L.) Alston. The dihedral angle between the planes of the carb-oxy-lic acid group and the olefinic group is 12.17 (18)°. The A/B, B/C, C/D and D/E ring junctions are all trans-fused. In the crystal, O-H⋯O hydrogen bonds involving the hy-droxy and carb-oxy-lic acid groups and the methanol solvent mol-ecule give rise to a two-dimensional network structure lying parallel to (001). </p>","PeriodicalId":7117,"journal":{"name":"Acta crystallographica. Section E, Structure reports online","volume":null,"pages":null},"PeriodicalIF":0.9,"publicationDate":"2014-11-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1107/S1600536814023848","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"32945371","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 6
Crystal structure of bis-(propane-1,3-diaminium) hexa-fluorido-aluminate di-aqua-tetra-fluorido-aluminate tetra-hydrate. 二(丙烷-1,3-二胺)六氟铝酸酯二水四氟铝酸酯四水合物的晶体结构。
IF 0.9
Acta crystallographica. Section E, Structure reports online Pub Date : 2014-11-08 eCollection Date: 2014-12-01 DOI: 10.1107/S1600536814024155
Insaf Abdi, Khulood Al-Sadhan, Amor Ben Ali
{"title":"Crystal structure of bis-(propane-1,3-diaminium) hexa-fluorido-aluminate di-aqua-tetra-fluorido-aluminate tetra-hydrate.","authors":"Insaf Abdi,&nbsp;Khulood Al-Sadhan,&nbsp;Amor Ben Ali","doi":"10.1107/S1600536814024155","DOIUrl":"https://doi.org/10.1107/S1600536814024155","url":null,"abstract":"<p><p>The title compound, (C3H12N2)2[AlF6][AlF4(H2O)2]·4H2O, was obtained by a solvothermal method in ethanol as solvent and with aluminium hydroxide, HF and 1,3-di-amino-propane as educts. The asymmetric unit contains a quarter each of two crystallographically independent propane-1,3-di-ammonium dicat-ions, [AlF6](3-) and [AlF4(H2O)2](-) anions and four water mol-ecules. The cations, anions and three of the independent water mol-ecules are situated on special positions mm, while the fourth water mol-ecule is disordered about a mirror plane. In the crystal, inter-molecular N-H⋯F and O-H⋯F hydrogen bonds link the cations and anions into a three-dimensional framework with the voids filled by water mol-ecules, which generate O-H⋯O hydrogen bonds and further consolidate the packing. </p>","PeriodicalId":7117,"journal":{"name":"Acta crystallographica. Section E, Structure reports online","volume":null,"pages":null},"PeriodicalIF":0.9,"publicationDate":"2014-11-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1107/S1600536814024155","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"32946122","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal structure of (E)-4-{[2-(2,4-di-nitro-phen-yl)hydrazin-1-yl-idene]meth-yl}-3-methyl-1-phenyl-5-(1H-pyrrol-1-yl)-1H-pyrazole. (E)-4-{[2-(2,4-二硝基苯基)肼-1-基-二硝基]甲基}-3-甲基-1-苯基-5-(1h -吡咯-1-基)- 1h -吡唑的晶体结构。
IF 0.9
Acta crystallographica. Section E, Structure reports online Pub Date : 2014-11-08 eCollection Date: 2014-12-01 DOI: 10.1107/S1600536814024039
Joel T Mague, Shaaban K Mohamed, Mehmet Akkurt, Hussein M S El-Kashef, Mustafa R Albayati
{"title":"Crystal structure of (E)-4-{[2-(2,4-di-nitro-phen-yl)hydrazin-1-yl-idene]meth-yl}-3-methyl-1-phenyl-5-(1H-pyrrol-1-yl)-1H-pyrazole.","authors":"Joel T Mague,&nbsp;Shaaban K Mohamed,&nbsp;Mehmet Akkurt,&nbsp;Hussein M S El-Kashef,&nbsp;Mustafa R Albayati","doi":"10.1107/S1600536814024039","DOIUrl":"https://doi.org/10.1107/S1600536814024039","url":null,"abstract":"<p><p>The title compound, C21H17N7O4, is in an 'extended' conformation aided by an intra-molecular N-H⋯O hydrogen bond. The pyrazole ring makes dihedral angles of 29.17 (6), 65.47 (4) and 9.91 (7)°, respectively, with the phenyl, pyrrole and benzene rings. In the crystal, mol-ecules are connected by pairs of N-H⋯O and C-H⋯O hydrogen bonds, forming inversion dimers which associate into ribbons running along the b axis through complementary C-H⋯O inter-actions. </p>","PeriodicalId":7117,"journal":{"name":"Acta crystallographica. Section E, Structure reports online","volume":null,"pages":null},"PeriodicalIF":0.9,"publicationDate":"2014-11-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1107/S1600536814024039","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"32945290","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Crystal structure of {3-[3,5-bis-(2,6-di-methyl-phen-yl)-1,2-phenyl-ene]-1-(2,6,2'',6''-tetra-methyl-1,1':3',1''-ter-phen-yl-5'-yl)imidazol-2-yl-idene}chlorido-(η(6)-p-cymene)ruthenium(II) benzene disolvate. 水晶的学院——3——[3,5-bis (2,6-di-methyl-phen-yl) -1,2-phenyl-ene]达到华(2,6,2 " 6 " -tetra-methyl-1,1: 3 (" 1 " -ter-phen-yl-5 -yl) imidazol-2-yl-idene chlorido……-(η(6)-p-cymene钌(II) benzene disolvate .
IF 0.9
Acta crystallographica. Section E, Structure reports online Pub Date : 2014-11-08 eCollection Date: 2014-12-01 DOI: 10.1107/S160053681402399X
Shohei Sase, Yuriko Ikehara, Kei Goto
{"title":"Crystal structure of {3-[3,5-bis-(2,6-di-methyl-phen-yl)-1,2-phenyl-ene]-1-(2,6,2'',6''-tetra-methyl-1,1':3',1''-ter-phen-yl-5'-yl)imidazol-2-yl-idene}chlorido-(η(6)-p-cymene)ruthenium(II) benzene disolvate.","authors":"Shohei Sase,&nbsp;Yuriko Ikehara,&nbsp;Kei Goto","doi":"10.1107/S160053681402399X","DOIUrl":"https://doi.org/10.1107/S160053681402399X","url":null,"abstract":"<p><p>The title compound, [Ru(C47H43N2)Cl(C10H14)]·2C6H6, crystallized with two independent mol-ecules of benzene. One of the N-aryl moieties of the N-heterocyclic carbene (NHC) ligand underwent cyclo-metallation to form a five-membered ruthenacycle. The complex has a three-legged piano-stool structure with two C atoms incorporated in the five-membered ruthenacycle and a Cl atom as legs. The ruthenacycle is essentially coplanar with the imidazole ring of the NHC ligand, making a dihedral angle of 0.85 (8)°. </p>","PeriodicalId":7117,"journal":{"name":"Acta crystallographica. Section E, Structure reports online","volume":null,"pages":null},"PeriodicalIF":0.9,"publicationDate":"2014-11-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1107/S160053681402399X","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"32945363","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal structure of (2-{3-[4-(4'-cyano-biphenyl-4-yl-oxy)but-oxy]pyridin-2-yl-κN}-5-(dodec-yloxy)phenyl-κC (1))(9-oxo-tetra-cos-7-en-7-olato-κ(2) O,O')platinum(II). （2-{3-[4-（4'-氰基-联苯-4-基-氧基）但氧基]吡啶-2-基-kN}-5-（十二酰氧基）苯基kC（1））（9-氧代-四-cos-7-en-7-olato-k（2）O，O’）铂（II）的晶体结构。
IF 0.9
Acta crystallographica. Section E, Structure reports online Pub Date : 2014-11-05 eCollection Date: 2014-12-01 DOI: 10.1107/S1600536814021928
Kaijun Luo, Hanlin Liu, Qing Guo, Daibing Luo
{"title":"Crystal structure of (2-{3-[4-(4'-cyano-biphenyl-4-yl-oxy)but-oxy]pyridin-2-yl-κN}-5-(dodec-yloxy)phenyl-κC (1))(9-oxo-tetra-cos-7-en-7-olato-κ(2) O,O')platinum(II).","authors":"Kaijun Luo,&nbsp;Hanlin Liu,&nbsp;Qing Guo,&nbsp;Daibing Luo","doi":"10.1107/S1600536814021928","DOIUrl":"https://doi.org/10.1107/S1600536814021928","url":null,"abstract":"<p><p>The central Pt(II) atom in the title compound, [Pt(C40H47N2O3)(C24H45O2)], has a slightly distorted square-planar coordination environment. The dihedral angle between the plane formed by Pt and the chelating C and N atoms and that formed by Pt and the chelating O atoms is 2.1 (3)°. The angle between the planes of the two rings in the biphenyl-4-carbo-nitrile unit is 35.1 (5)°. One lateral alkane chain is disordered over two sets of sites with site occupancy factors in a 0.595 (7):0.405 (7) ratio. </p>","PeriodicalId":7117,"journal":{"name":"Acta crystallographica. Section E, Structure reports online","volume":null,"pages":null},"PeriodicalIF":0.9,"publicationDate":"2014-11-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1107/S1600536814021928","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"32945362","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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