JOMPub Date : 2025-03-14DOI: 10.1007/s11837-025-07270-w
Daniel Valdés, Juan Manuel García Zapata, Irene Limón, Belén Torres, Joaquín Rams, Marta Multigner
{"title":"Innovative Stent Test Specimen by Additive Manufacturing for Reliable Mechanical Testing and Simulation","authors":"Daniel Valdés, Juan Manuel García Zapata, Irene Limón, Belén Torres, Joaquín Rams, Marta Multigner","doi":"10.1007/s11837-025-07270-w","DOIUrl":"10.1007/s11837-025-07270-w","url":null,"abstract":"<div><p>Cardiovascular diseases are the leading cause of mortality globally, underscoring the importance of reliable treatments such as cardiovascular stents, which prevent arterial collapse and improve blood flow. Despite their widespread use, stents face challenges in mechanical performance and biological compatibility. This study focuses on the mechanical characterization of biodegradable metallic stents, addressing limitations in current testing methods and simulations. Novel specimen geometries, designed for tensile strength testing, were developed using additive manufacturing (AM) to minimize damage from gripping clamps during testing. Finite element modeling simulations and experimental tests were conducted to evaluate the mechanical behavior of stents under ideal and real-world conditions. The results revealed that the values provided by the most common mechanical tests and simulations do not correspond to the actual values of the meshed structure. The proposed geometries demonstrated consistent mechanical behavior, effectively mitigating stress concentrations and enabling reliable data acquisition. These findings highlight the potential of AM in stent testing and validate the integration of experimental and simulation approaches for optimizing stent design and performance. This study establishes a framework for future research aimed at improving stent safety and reliability.</p></div>","PeriodicalId":605,"journal":{"name":"JOM","volume":"77 6","pages":"4430 - 4444"},"PeriodicalIF":2.1,"publicationDate":"2025-03-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://link.springer.com/content/pdf/10.1007/s11837-025-07270-w.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144091050","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
JOMPub Date : 2025-03-13DOI: 10.1007/s11837-025-07304-3
Madhavan Radhakrishnan, Shashank Sharma, Selvamurugan Palaniappan, K. N. Chaithanya Kumar, Krishna Kamlesh Verma, Narendra B. Dahotre
{"title":"Processing Conditions Dependent Evolution of Microstructure in Laser Additive Manufactured HT-9 Ferritic Martensitic Steel","authors":"Madhavan Radhakrishnan, Shashank Sharma, Selvamurugan Palaniappan, K. N. Chaithanya Kumar, Krishna Kamlesh Verma, Narendra B. Dahotre","doi":"10.1007/s11837-025-07304-3","DOIUrl":"10.1007/s11837-025-07304-3","url":null,"abstract":"<div><p>This study examined the effects of laser processing conditions on the evolution of microstructure and phase fractions in HT9 ferritic/martensitic (F/M) steels fabricated using laser powder bed fusion (L-PBF) and laser-directed energy deposition (L-DED). Electron backscattered diffraction (EBSD) micrographs of the cross-sections of the laser-processed builds showed the presence of <i>α</i>-ferrite, <i>α</i>′-martensite, and retained austenite (<i>γ</i>). Distinct differences were observed in the <i>γ</i> phase fraction between the L-PBF and L-DED microstructures. To correlate the observed phase fractions with process-induced thermokinetic effects, a multiscale multiphysics thermal model was used. The modeling results confirmed the experimental data and provided insight into the relationship between temperature changes during processing and phase evolution in HT9 steel.</p></div>","PeriodicalId":605,"journal":{"name":"JOM","volume":"77 5","pages":"2888 - 2896"},"PeriodicalIF":2.1,"publicationDate":"2025-03-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143835532","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
JOMPub Date : 2025-03-12DOI: 10.1007/s11837-025-07162-z
Duncan W. Gibbons, Andre F. van der Merwe
{"title":"Pin-Type Bearing Strength and Fracture Behaviour of Ductile LPBF Ti-6Al-4V ELI Produced with Extensively Reused Powder","authors":"Duncan W. Gibbons, Andre F. van der Merwe","doi":"10.1007/s11837-025-07162-z","DOIUrl":"10.1007/s11837-025-07162-z","url":null,"abstract":"<div><p>Metal additive manufacturing is a manufacturing technology that is being investigated for critical industrial applications in industries such as aerospace, nuclear, and medical. A degree of uncertainty remains around these technologies largely due to process and material repeatability, production controls, and a lack of application-specific material data. This research aimed to investigate the effects of extensively reused (175 reuse cycles) Ti-6Al-4V ELI powder feedstock and build orientation on the produced material. Material chemistry, metallography, pin-type bearing strength, and tensile properties were characterized at different build locations and principal orientations. The literature on pin-type bearing strength for both traditionally and additively manufactured material is lacking. Such information is of value for the design of bolted structural joints and fixtures. The results suggest that although extensively reused powder feedstock does experience drift in material properties due to the reuse process, it can still fulfil feedstock material specification requirements. Furthermore, this powder is capable of producing material that meets produced material specification requirements, exhibits minimal orthotropy in mechanical properties, and has ultimate bearing strength that exceeds Ti-6Al-4V grade 5 wrought material allowables. This research provides valuable information for designing structural joints and contributes to the further industrialization of laser powder bed fusion for critical applications.</p></div>","PeriodicalId":605,"journal":{"name":"JOM","volume":"77 4","pages":"1885 - 1897"},"PeriodicalIF":2.1,"publicationDate":"2025-03-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://link.springer.com/content/pdf/10.1007/s11837-025-07162-z.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143668069","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
JOMPub Date : 2025-03-12DOI: 10.1007/s11837-025-07274-6
Abdelhakim Cherqaoui, Quang Nguyen Cao, Carlo Paternoster, Simon Gélinas, Magdalena Bieda, Anna Jarzębska, Carl Blais, Diego Mantovani
{"title":"Two-Month In Vitro Degradation of 3D-Printed Biodegradable FeMnC Alloys for Biomedical Applications","authors":"Abdelhakim Cherqaoui, Quang Nguyen Cao, Carlo Paternoster, Simon Gélinas, Magdalena Bieda, Anna Jarzębska, Carl Blais, Diego Mantovani","doi":"10.1007/s11837-025-07274-6","DOIUrl":"10.1007/s11837-025-07274-6","url":null,"abstract":"<div><p>Over the last decade, Fe-Mn-based bioresorbable implants have attracted significant interest due to their outstanding mechanical properties, including ductility and strength, and their ability to degrade over medium-to-long healing periods, eliminating the need for secondary surgeries for implant removal. However, their slow degradation under physiological conditions limits their practical use, especially for short-term degradable implants. Additive manufacturing facilitates rapid production with tailored compositions, offering advantages over traditional casting methods. Yet, the structure, the microstructure, the degradation behavior, and the mechanical properties are known to be impacted by the fabrication methods. In this context, this study investigates the degradation behavior of 3D-printed FeMnC alloys produced via laser powder bed fusion using volumetric energy densities from 75 J/mm<sup>3</sup> to 87 J/mm<sup>3</sup>. Microstructure and degradation rate relationships were explored through microstructural characterization (SEM, XRD, EBSD) and static immersion tests in modified Hanks' solution over 60 days. XRD confirmed a fully austenitic microstructure in all conditions, while SEM and EBSD revealed refined structures along the building direction. The alloy printed at 87 J/mm<sup>3</sup> exhibited the lowest degradation rate for both immersion periods, with values near 0.04 mm/year after 14 days and 0.03 mm/year after 60 days.</p></div>","PeriodicalId":605,"journal":{"name":"JOM","volume":"77 6","pages":"4414 - 4429"},"PeriodicalIF":2.1,"publicationDate":"2025-03-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://link.springer.com/content/pdf/10.1007/s11837-025-07274-6.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144091207","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
JOMPub Date : 2025-03-11DOI: 10.1007/s11837-025-07242-0
Eitan Hershkovitz, Timothy Yoo, Flavia da Cruz Gallo, Garrett Baucom, Michele V. Manuel, Honggyu Kim
{"title":"Anisotropic Suppression of Martensitic Transformation in Precipitation-Hardened NiTiHf High-Temperature Shape Memory Alloys","authors":"Eitan Hershkovitz, Timothy Yoo, Flavia da Cruz Gallo, Garrett Baucom, Michele V. Manuel, Honggyu Kim","doi":"10.1007/s11837-025-07242-0","DOIUrl":"10.1007/s11837-025-07242-0","url":null,"abstract":"<div><p>The reversible and diffusionless martensitic transformation of shape memory alloys (SMAs) has spurred their development for shape memory-based devices such as nano- and micro-electromechanical systems. However, when the size of a SMA is reduced to the scale of a few hundred nanometers, its shape memory effect becomes diminished and can eventually be suppressed. To investigate the microscopic origin of this behavior, we have characterized the thermally-induced martensitic transformation in precipitation-hardened NiTiHf high-temperature SMAs, using four-dimensional scanning transmission electron microscopy and in situ heating experiments. We show a distinct anisotropic suppression of the martensitic phase transformation, where B19′ martensite is successfully transformed into B2 austenite, while the reverse transformation is completely suppressed. Quantitative phase and strain analysis reveal strain accumulation in the austenite matrix, specifically a unique buildup of shear strain surrounding precipitates embedded in the matrix phase. This result indicates that the suppression of the martensitic transformation in precipitation-hardened SMAs is not solely due to extrinsic effects like the buildup of non-transforming oxides on the alloy surface, and that there is an additional intrinsic mechanism inhibiting the full shape memory transformation. Our findings encourage future research on the feasibility of scalable shape memory devices in the sub-hundred nanometer regime.</p></div>","PeriodicalId":605,"journal":{"name":"JOM","volume":"77 5","pages":"2852 - 2861"},"PeriodicalIF":2.1,"publicationDate":"2025-03-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143835625","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
JOMPub Date : 2025-03-10DOI: 10.1007/s11837-025-07297-z
Phillip Mackey, William Culver
{"title":"Dr. James Douglas: The Founder of American Copper","authors":"Phillip Mackey, William Culver","doi":"10.1007/s11837-025-07297-z","DOIUrl":"10.1007/s11837-025-07297-z","url":null,"abstract":"","PeriodicalId":605,"journal":{"name":"JOM","volume":"77 4","pages":"1713 - 1716"},"PeriodicalIF":2.1,"publicationDate":"2025-03-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143667848","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
JOMPub Date : 2025-03-06DOI: 10.1007/s11837-025-07299-x
Megan Enright
{"title":"Artificial Intelligence, ICME, and 3D Materials Science Meet at TMS Specialty Congress 2025","authors":"Megan Enright","doi":"10.1007/s11837-025-07299-x","DOIUrl":"10.1007/s11837-025-07299-x","url":null,"abstract":"","PeriodicalId":605,"journal":{"name":"JOM","volume":"77 4","pages":"1722 - 1725"},"PeriodicalIF":2.1,"publicationDate":"2025-03-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143667832","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}