JOMPub Date : 2024-10-30DOI: 10.1007/s11837-024-06955-y
Ran Tian, Zhiwei Peng, Wanlong Fan, Guanwen Luo, Mingjun Rao
{"title":"Preheating Characteristics of Magnetite Pellets Under Microwave Irradiation","authors":"Ran Tian, Zhiwei Peng, Wanlong Fan, Guanwen Luo, Mingjun Rao","doi":"10.1007/s11837-024-06955-y","DOIUrl":"10.1007/s11837-024-06955-y","url":null,"abstract":"<div><p>The microwave preheating characteristics of magnetite pellets were investigated based on the microwave absorption capability analysis. With increasing microwave power from 1100 W to 1500 W, the initial heating rate of the pellets increased from 134.9°C/min to 233.0°C/min and then decreased because of the decrease in microwave magnetic loss induced by the oxidation of Fe<sub>3</sub>O<sub>4</sub> to Fe<sub>2</sub>O<sub>3</sub> and more heat loss from the pellets to the surroundings. With the same terminal temperature, the pellets after microwave preheating (MP pellets) obtained higher oxidation fraction and compressive strength and lower porosity than those produced by conventional preheating (CP pellets), associated with the variations of content and crystallite size of Fe<sub>2</sub>O<sub>3</sub>. Moreover, MP pellets had larger and more concentrated Fe<sub>2</sub>O<sub>3</sub> particles in their cores than their shells and the corresponding areas in CP pellets, demonstrating the advantages of microwave which intensified the oxidation of the pellets in the preheating process.</p></div>","PeriodicalId":605,"journal":{"name":"JOM","volume":"77 1","pages":"133 - 143"},"PeriodicalIF":2.1,"publicationDate":"2024-10-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142859673","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
JOMPub Date : 2024-10-30DOI: 10.1007/s11837-024-06930-7
Liang Meng, Raja Ahmad Azmeer Raja Ahmad Effendi, Wei Sun, Lili Mo, Ahmad Rizal Abdul Rahman, Yu-Lin Hsu, Deirdre Barron
{"title":"Deep Learning-Enhanced Jewelry Material Jadeite Jade Quality Assessment","authors":"Liang Meng, Raja Ahmad Azmeer Raja Ahmad Effendi, Wei Sun, Lili Mo, Ahmad Rizal Abdul Rahman, Yu-Lin Hsu, Deirdre Barron","doi":"10.1007/s11837-024-06930-7","DOIUrl":"10.1007/s11837-024-06930-7","url":null,"abstract":"<div><p>Jadeite jade, renowned for its unique texture and cultural significance, stands as the epitome of jade varieties, embodying the latest evolution of China's jade culture. This research endeavors to establish an AI model for precisely screening jadeite quality, employing deep learning techniques to revolutionize jadeite design and detection. The objective is to provide jewelry companies, designers, and customers with an unbiased means of grading and evaluating jadeite quality. We have meticulously curated a database of jadeite images, applied preprocessing techniques, and have harnessed convolutional neural networks (CNN) for feature extraction. The outcomes were promising, with the model achieving notable performance indicators: an accuracy rate of approximately 84.75%, a recall rate of about 84.94%, and an F1 score of roughly 73.76% in jade image classification tasks. These results underscore the model's effectiveness in the assessment of jadeite quality. Incorporating computer-aided technology into jadeite screening foreshadows a transformative era where artificial intelligence seamlessly integrates with traditional jade carving design, signifying a pivotal shift in the industry's landscape.</p></div>","PeriodicalId":605,"journal":{"name":"JOM","volume":"77 1","pages":"211 - 224"},"PeriodicalIF":2.1,"publicationDate":"2024-10-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142859672","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
JOMPub Date : 2024-10-29DOI: 10.1007/s11837-024-06904-9
Amir Parsian, Mohammad Akbari, Arash Karimipour, Mahdi Rafiei, Mohammad Mehdi Razzaghi
{"title":"Experimental Investigation of Temperature Field, Fusion Zone Microstructure and Mechanical Properties During Dissimilar Laser Welding of Nickel-Base Alloy and Duplex Stainless Steel","authors":"Amir Parsian, Mohammad Akbari, Arash Karimipour, Mahdi Rafiei, Mohammad Mehdi Razzaghi","doi":"10.1007/s11837-024-06904-9","DOIUrl":"10.1007/s11837-024-06904-9","url":null,"abstract":"<div><p>The current study delves into the dissimilar laser welding of nickel-base alloy and duplex stainless steel, specifically in circular and plate forms, using fiber laser technology. The study utilizes a design of experiments methodology, specifically employing a central composite design, to methodically evaluate how different laser welding parameters affect the properties of dissimilar welds. The methodology is the response surface methodology (RSM), allowing for a comprehensive evaluation of the effects. The study examines the influence of key welding parameters, such as laser power, welding speed, focal distance, and laser beam deviation from the joint’s center, on several response variables. These variables encompass the depth of the molten pool, the weld microstructure, and its mechanical characteristics. The depth of the molten pool, on the other hand, is primarily influenced by laser power and focal distance. Notably, a transition in microstructure is observed from columnar dendrites to a cellular configuration as one moves from the fusion line towards the center of the fusion zone. In the fusion zone of the duplex base metal, an unmixed zone is identifiable in the upper segments of the fusion line. This phenomenon arises due to incomplete melting at the fusion line.</p></div>","PeriodicalId":605,"journal":{"name":"JOM","volume":"77 1","pages":"193 - 210"},"PeriodicalIF":2.1,"publicationDate":"2024-10-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142859567","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
JOMPub Date : 2024-10-29DOI: 10.1007/s11837-024-06937-0
Ming Zhao, Huaying Li, Fang Huang, Yaohui Song, Guanzheng Su, Yibo Lu, Qi Chen, Yugui Li
{"title":"Study on Grain Boundary Characteristic Distribution of Nickel Base 625 Alloy Controlled by Deformation Heat-Treatment Process","authors":"Ming Zhao, Huaying Li, Fang Huang, Yaohui Song, Guanzheng Su, Yibo Lu, Qi Chen, Yugui Li","doi":"10.1007/s11837-024-06937-0","DOIUrl":"10.1007/s11837-024-06937-0","url":null,"abstract":"<div><p>Through a series of thermal–mechanical processing (TMP) routes with various ratios of cold rolling (CR) and subsequent high-temperature annealing, Inconel625 alloy samples with different strain states were prepared to investigate the evolution of grain boundary characteristic distribution (GBCD) in the process of grain boundary engineering (GBE). The effects of the TMP parameters on the microstructure of GBE were studied by electron backscattering (EBSD), and the effects of different TMP parameters on the microstructure and hardness of GBE were analyzed. The results show that different restraints have different mechanisms of grain boundary network formation, and that strain is the main mechanism of boundary migration. When the deformation is 5%, the proportion of low ΣCSL grain boundary is relatively large at each annealing temperature, and the proportion of low ΣCSL grain boundary reaches the maximum at 1075°C. With the increase of temperature and deformation, the dominant mechanism of grain boundary fracture gradually changes from the new twin mechanism to the ∑3 regeneration mechanism. The large initial grain size can delay the nucleation of strain-free grains during TMP treatment. Finally, the grain boundary evolution of the sample in each stage of GBE production and the change of hardness of the sample after GBE are described.</p></div>","PeriodicalId":605,"journal":{"name":"JOM","volume":"77 1","pages":"377 - 388"},"PeriodicalIF":2.1,"publicationDate":"2024-10-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142859612","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
JOMPub Date : 2024-10-29DOI: 10.1007/s11837-024-06935-2
John D. Shimanek, Zi-Kui Liu, Allison M. Beese
{"title":"Simultaneous Optimization of Crystal Plasticity Hardening Parameters","authors":"John D. Shimanek, Zi-Kui Liu, Allison M. Beese","doi":"10.1007/s11837-024-06935-2","DOIUrl":"10.1007/s11837-024-06935-2","url":null,"abstract":"<div><p>Crystal plasticity models relate macroscopic deformation behavior to the evolution of slip systems strength, but their parameterization is often non-unique, with multiple parameter sets being able to describe the same macroscopic behavior. To address this issue, the present work adopts a Bayesian optimization framework for the parameterization of face-centered cubic plasticity models while simultaneously considering multiple experimental datasets from the literature. For single crystal Cu, parameter optimization was guided by the tensile stress–strain curves along several crystallographic orientations, with an adequate fit being found for five orientations at once. While additional parameters allowed for the consideration of more physical mechanisms, like different slip system interaction strengths or misorientations inherent to the experimental data, the extra dimensionality was found to limit the efficiency of the global minimization procedure. For polycrystalline Ni, multiple grain sizes were considered together in a representative polycrystalline model, with the optimization able to reconcile the model with the data for three grain sizes at once. As meaningful interpretation of parameters relies on the uniqueness of their values, incorporating multiple datasets into this discerning parameterization procedure enables more robust prediction and application of crystal plasticity models.</p></div>","PeriodicalId":605,"journal":{"name":"JOM","volume":"77 1","pages":"324 - 335"},"PeriodicalIF":2.1,"publicationDate":"2024-10-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://link.springer.com/content/pdf/10.1007/s11837-024-06935-2.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142859611","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
JOMPub Date : 2024-10-24DOI: 10.1007/s11837-024-06840-8
Qianfei Zhao, Hongying Yang, Linlin Tong
{"title":"Evaluation of Cyanide Leaching Behavior of Typical Associated Copper Minerals in Gold Concentrates Based on Solution Chemistry and Interfacial Physicochemical Properties Analysis","authors":"Qianfei Zhao, Hongying Yang, Linlin Tong","doi":"10.1007/s11837-024-06840-8","DOIUrl":"10.1007/s11837-024-06840-8","url":null,"abstract":"<div><p>Copper minerals associated with gold concentrates are expelled alongside cyanide tailings. During cyanide leaching, prolonged exposure to cyanide alters the surface properties of minerals significantly, complicating copper recovery. This study focuses on the typical copper minerals in gold concentrates, including chalcopyrite, bornite, chalcocite, and malachite, to thoroughly examine the cyanide pulp properties and interface changes before and after cyanidation, using methods like leaching experiments, contact angle measurements, and analyses via FT − IR, XPS, and ToF-SIMS. Pulp chemical analysis revealed that copper minerals significantly deplete cyanide and dissolved oxygen. Surface analysis reveals that cyanidation enhances the wettability of copper minerals, transitioning them from hydrophobic to hydrophilic, thereby hindering the adsorption of flotation agents. The shift may result from CN<sup>−</sup> adsorption and the creation of hydrophilic compounds like CNO<sup>−</sup>, SCN<sup>−</sup>, CuCN, and CuSCN instead of iron-cyanide complexes. Further ToF-SIMS deep sputtering analysis shows that cyanide can infiltrate the surface layer of copper minerals, spreading into the bulk phase and contaminating the surface. The contaminated film’s thickness ranges from approximately 2.8–15 nm on copper mineral surfaces, complicating the copper mineral’s physicochemical properties and impacting copper recovery efficiency.</p></div>","PeriodicalId":605,"journal":{"name":"JOM","volume":"76 12","pages":"7218 - 7230"},"PeriodicalIF":2.1,"publicationDate":"2024-10-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142737318","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
JOMPub Date : 2024-10-24DOI: 10.1007/s11837-024-06932-5
Amirhossein Sadeghi Larimi, Hassan Jafari, Ahmad Sadeghzadeh
{"title":"Developing Sol–Gel Hydroxyapatite-Bone Powder Composite Coatings on Mg-Zn-Ca Alloy and Studying Their Corrosion Behavior","authors":"Amirhossein Sadeghi Larimi, Hassan Jafari, Ahmad Sadeghzadeh","doi":"10.1007/s11837-024-06932-5","DOIUrl":"10.1007/s11837-024-06932-5","url":null,"abstract":"<div><p>Hydroxyapatite/bone powder composite coatings on ZX504 alloy have been developed using the sol–gel process and their corrosion behavior has been explored. The alloy was anodized in 1 M NaOH + 0.5 M Na<sub>2</sub>SiO<sub>3</sub> solution. An 0.5 P<sub>2</sub>O<sub>5</sub> + z 1.67 Ca(NO<sub>3</sub>)<sub>2</sub>.4H<sub>2</sub>O solution with 10 g/L, 20 g/L, and 30 g/L bone powder concentrations and 50 s, 100 s, and 150 s dip-coating durations, followed by calcination at 400°C, was used to develop the coatings. Microscopic analysis results disclosed the formation of a uniform and highly porous MgO film on the alloy to guarantee the subsequent coating adhesion. The results also confirmed the fruitful formation of smoother hydroxyapatite + bone powder composite coatings on the film. Electrochemical corrosion tests revealed that the alloy exhibited the lowest corrosion resistance, while the hydroxyapatite + 30 g/L bone powder composite-coated alloy possessed the best performance with a significantly low corrosion rate of 0.07 mm/year, suggesting the composite-coated alloy is a desired candidate for implant application.</p></div>","PeriodicalId":605,"journal":{"name":"JOM","volume":"76 12","pages":"7186 - 7197"},"PeriodicalIF":2.1,"publicationDate":"2024-10-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142737319","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
JOMPub Date : 2024-10-21DOI: 10.1007/s11837-024-06924-5
Rahul Mukherjee, Shubhabrata Datta
{"title":"Materials Informatics Driven Designing Mg Alloys for Biodegradable Short-Term Implants Using Machine Learning","authors":"Rahul Mukherjee, Shubhabrata Datta","doi":"10.1007/s11837-024-06924-5","DOIUrl":"10.1007/s11837-024-06924-5","url":null,"abstract":"<div><p>Due to their non-toxic nature, high strength-to-weight ratio, and low density, which is nearly identical to human cortical bone, and notable biocompatibility and biodegradability, magnesium alloys have attracted the attention of researchers in the field of new age biomaterials during the past 2 decades. The Mg alloys are the ideal option for modern biodegradable biomaterial because they will degrade inside the human body and lower medical expenses of the second surgery to remove the short-term implant. It is important to have an in-depth understanding of the role of the alloying elements for designing Mg alloys with improved properties, i.e., higher strength with required/higher corrosion resistance, for better implant performance. Here, a materials informatics approach using four distinct machine learning techniques has been implemented to analyze Mg alloy databases to understand the role of the alloying elements in achieving the above features. The analyses show that Mn, Y and some other rare earth elements are suitable to improving the strength and corrosion properties of Mg alloys with enhanced performance as the material for short-term implants.</p></div>","PeriodicalId":605,"journal":{"name":"JOM","volume":"77 1","pages":"20 - 38"},"PeriodicalIF":2.1,"publicationDate":"2024-10-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142859802","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
JOMPub Date : 2024-10-21DOI: 10.1007/s11837-024-06898-4
Qing Liu, Min Wang, Weiguang Pang, Lidong Xing, Yanping Bao
{"title":"Effect of Deoxidation Sequence on Inclusions in Oriented Silicon Steel","authors":"Qing Liu, Min Wang, Weiguang Pang, Lidong Xing, Yanping Bao","doi":"10.1007/s11837-024-06898-4","DOIUrl":"10.1007/s11837-024-06898-4","url":null,"abstract":"<div><p>In this study, industrial experiments and thermodynamic calculations were performed to compare the effects of different deoxidation methods on inclusions. The thermodynamic equilibrium between slag and liquid oriented silicon steel was studied at 1873 K (1600°C) to understand the influence of slag composition on oxygen content and the ability to absorb Al<sub>2</sub>O<sub>3</sub>. Thermodynamic calculations showed that the refining slag (w(CaO)/w(SiO<sub>2</sub>) = 2.54, w(CaO)/w(Al<sub>2</sub>O<sub>3</sub>) = 2.51) under the process of adding Fe-Si alloys first and then Fe-Al alloys during the tapping process had a stronger adsorption capacity for aluminum inclusions than that of the process of adding Fe-Al alloys first and then Fe-Si alloys, and resulted in a higher of molten steel cleanliness and fewer inclusions. A mathematical model was established to describe and predict the adsorption and removal of oxidized inclusions by slag through the study of slag viscosity and interfacial tension between slag and inclusions. The critical size of oxide inclusions in refining slag was calculated under different deoxidation methods.</p></div>","PeriodicalId":605,"journal":{"name":"JOM","volume":"76 12","pages":"7290 - 7303"},"PeriodicalIF":2.1,"publicationDate":"2024-10-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142737133","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
JOMPub Date : 2024-10-17DOI: 10.1007/s11837-024-06894-8
Jianzhi Zhang, Zhiwei Peng, Tong Zhang, Guanwen Luo
{"title":"Exploring Mechanism of H2 Adsorption on Surfaces of Iron Oxides by Density Functional Theory Calculation","authors":"Jianzhi Zhang, Zhiwei Peng, Tong Zhang, Guanwen Luo","doi":"10.1007/s11837-024-06894-8","DOIUrl":"10.1007/s11837-024-06894-8","url":null,"abstract":"<div><p>With the advance of low-carbon transformation of ironmaking and steelmaking, it is crucial to understand the adsorption and reduction mechanisms of hydrogen during the reduction of Fe<sub>2</sub>O<sub>3</sub> to Fe for the improvement and widespread adoption of hydrogen-based direct reduction technologies. Density functional theory (DFT) calculations, known for their exceptional ability to calculate adsorption sites, adsorption energies, and electron transfer processes, have become an essential tool for investigating the mechanisms of gas adsorption on iron oxide surfaces. This paper reviews the research progress on the adsorption behavior of gas molecules during the hydrogen reduction of iron oxides, namely Fe<sub>2</sub>O<sub>3</sub>, Fe<sub>3</sub>O<sub>4</sub>, and FeO, using DFT computational methods, focusing on the adsorption mechanisms of H<sub>2</sub> on various oxide surfaces. H<sub>2</sub> adsorption usually involves interactions with surface oxygen atoms, leading to dissociative adsorption and a spontaneous exothermic process. Owing to different surface structures of the oxides and variations in computational methods, there are significant differences in the adsorption behavior and mechanisms of H<sub>2</sub> on these surfaces. Therefore, this work also discusses the influence of methodological parameters of DFT calculations, expecting to fully understand H<sub>2</sub> adsorption behaviors in the Fe<sub>2</sub>O<sub>3</sub> reduction process.</p></div>","PeriodicalId":605,"journal":{"name":"JOM","volume":"77 1","pages":"144 - 155"},"PeriodicalIF":2.1,"publicationDate":"2024-10-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142859630","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}