Journal of Synchrotron Radiation最新文献_第8页

In situ characterization of stresses, deformation and fracture of thin films using transmission X-ray nanodiffraction microscopy. Corrigendum. 利用透射 X 射线纳米衍射显微镜对薄膜的应力、变形和断裂进行现场表征。更正。

IF 2.5 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2024-09-01 Epub Date: 2024-08-06 DOI: 10.1107/S1600577524006283

Gudrun Lotze, Anand H S Iyer, Olof Bäcke, Sebastian Kalbfleisch, Magnus Hörnqvist Colliander

引用次数: 0

Accelerating imaging research at large-scale scientific facilities through scientific computing. 通过科学计算加速大型科学设施的成像研究。

IF 2.5 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2024-09-01 Epub Date: 2024-08-27 DOI: 10.1107/S1600577524007239

Chunpeng Wang, Xiaoyun Li, Rongzheng Wan, Jige Chen, Jing Ye, Ke Li, Aiguo Li, Renzhong Tai, Alessandro Sepe

{"title":"Accelerating imaging research at large-scale scientific facilities through scientific computing.","authors":"Chunpeng Wang, Xiaoyun Li, Rongzheng Wan, Jige Chen, Jing Ye, Ke Li, Aiguo Li, Renzhong Tai, Alessandro Sepe","doi":"10.1107/S1600577524007239","DOIUrl":"10.1107/S1600577524007239","url":null,"abstract":"To date, computed tomography experiments, carried-out at synchrotron radiation facilities worldwide, pose a tremendous challenge in terms of the breadth and complexity of the experimental datasets produced. Furthermore, near real-time three-dimensional reconstruction capabilities are becoming a crucial requirement in order to perform high-quality and result-informed synchrotron imaging experiments, where a large amount of data is collected and processed within a short time window. To address these challenges, we have developed and deployed a synchrotron computed tomography framework designed to automatically process online the experimental data from the synchrotron imaging beamlines, while leveraging the high-performance computing cluster capabilities to accelerate the real-time feedback to the users on their experimental results. We have, further, integrated it within a modern unified national authentication and data management framework, which we have developed and deployed, spanning the entire data lifecycle of a large-scale scientific facility. In this study, the overall architecture, functional modules and workflow design of our synchrotron computed tomography framework are presented in detail. Moreover, the successful integration of the imaging beamlines at the Shanghai Synchrotron Radiation Facility into our scientific computing framework is also detailed, which, ultimately, resulted in accelerating and fully automating their entire data processing pipelines. In fact, when compared with the original three-dimensional tomography reconstruction approaches, the implementation of our synchrotron computed tomography framework led to an acceleration in the experimental data processing capabilities, while maintaining a high level of integration with all the beamline processing software and systems.","PeriodicalId":48729,"journal":{"name":"Journal of Synchrotron Radiation","volume":" ","pages":"1317-1326"},"PeriodicalIF":2.5,"publicationDate":"2024-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11371030/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142082367","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Hyperspectral full-field quick-EXAFS imaging at the ROCK beamline for monitoring micrometre-sized heterogeneity of functional materials under process conditions. 在 ROCK 光束线进行高光谱全场快速-EXAFS 成像，用于监测加工条件下功能材料的微米级异质性。

IF 2.5 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2024-09-01 Epub Date: 2024-08-23 DOI: 10.1107/S1600577524006581

Valérie Briois, Jean Paul Itié, Alain Polian, Andrew King, Aliou Sadia Traore, Eric Marceau, Ovidiu Ersen, Camille La Fontaine, Laurent Barthe, Anthony Beauvois, Olga Roudenko, Stéphanie Belin

{"title":"Hyperspectral full-field quick-EXAFS imaging at the ROCK beamline for monitoring micrometre-sized heterogeneity of functional materials under process conditions.","authors":"Valérie Briois, Jean Paul Itié, Alain Polian, Andrew King, Aliou Sadia Traore, Eric Marceau, Ovidiu Ersen, Camille La Fontaine, Laurent Barthe, Anthony Beauvois, Olga Roudenko, Stéphanie Belin","doi":"10.1107/S1600577524006581","DOIUrl":"10.1107/S1600577524006581","url":null,"abstract":"Full-field transmission X-ray microscopy has been recently implemented at the hard X-ray ROCK-SOLEIL quick-EXAFS beamline, adding micrometre spatial resolution to the second time resolution characterizing the beamline. Benefiting from a beam size versatility due to the beamline focusing optics, full-field hyperspectral XANES imaging has been successfully used at the Fe K-edge for monitoring the pressure-induced spin transition of a 150 µm × 150 µm Fe(o-phen)2(NCS)2 single crystal and the charge of millimetre-sized LiFePO4 battery electrodes. Hyperspectral imaging over 2000 eV has been reported for the simultaneous monitoring of Fe and Cu speciation changes during activation of a FeCu bimetallic catalyst along a millimetre-sized catalyst bed. Strategies of data acquisition and post-data analysis using Jupyter notebooks and multivariate data analysis are presented, and the gain obtained using full-field hyperspectral quick-EXAFS imaging for studies of functional materials under process conditions in comparison with macroscopic information obtained by non-spatially resolved quick-EXAFS techniques is discussed.","PeriodicalId":48729,"journal":{"name":"Journal of Synchrotron Radiation","volume":" ","pages":"1084-1104"},"PeriodicalIF":2.5,"publicationDate":"2024-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11371034/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142044229","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

New achievements in orbital angular momentum beam characterization using a Hartmann wavefront sensor and the Kirkpatrick-Baez active optical system KAOS. 利用哈特曼波前传感器和 Kirkpatrick-Baez 主动光学系统 KAOS 进行轨道角动量光束鉴定的新成果。

IF 2.5 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2024-09-01 Epub Date: 2024-08-16 DOI: 10.1107/S160057752400626X

Luka Novinec, Matteo Pancaldi, Flavio Capotondi, Giovanni De Ninno, Francesco Guzzi, George Kourousias, Emanuele Pedersoli, Barbara Ressel, Benedikt Rösner, Alberto Simoncig, Marco Zangrando, Michele Manfredda

{"title":"New achievements in orbital angular momentum beam characterization using a Hartmann wavefront sensor and the Kirkpatrick-Baez active optical system KAOS.","authors":"Luka Novinec, Matteo Pancaldi, Flavio Capotondi, Giovanni De Ninno, Francesco Guzzi, George Kourousias, Emanuele Pedersoli, Barbara Ressel, Benedikt Rösner, Alberto Simoncig, Marco Zangrando, Michele Manfredda","doi":"10.1107/S160057752400626X","DOIUrl":"10.1107/S160057752400626X","url":null,"abstract":"Advances in physics have been significantly driven by state-of-the-art technology, and in photonics and X-ray science this calls for the ability to manipulate the characteristics of optical beams. Orbital angular momentum (OAM) beams hold substantial promise in various domains such as ultra-high-capacity optical communication, rotating body detection, optical tweezers, laser processing, super-resolution imaging etc. Hence, the advancement of OAM beam-generation technology and the enhancement of its technical proficiency and characterization capabilities are of paramount importance. These endeavours will not only facilitate the use of OAM beams in the aforementioned sectors but also extend the scope of applications in diverse fields related to OAM beams. At the FERMI Free-Electron Laser (Trieste, Italy), OAM beams are generated either by tailoring the emission process on the undulator side or, in most cases, by coupling a spiral zone plate (SZP) in tandem with the refocusing Kirkpatrick-Baez active optic system (KAOS). To provide a robust and reproducible workflow to users, a Hartmann wavefront sensor (WFS) is used for both optics tuning and beam characterization. KAOS is capable of delivering both tightly focused and broad spots, with independent control over vertical and horizontal magnification. This study explores a novel non-conventional `near collimation' operational mode aimed at generating beams with OAM that employs the use of a lithographically manufactured SZP to achieve this goal. The article evaluates the mirror's performance through Hartmann wavefront sensing, offers a discussion of data analysis methodologies, and provides a quantitative analysis of these results with ptychographic reconstructions.","PeriodicalId":48729,"journal":{"name":"Journal of Synchrotron Radiation","volume":" ","pages":"1058-1066"},"PeriodicalIF":2.5,"publicationDate":"2024-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11371050/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141989247","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

A 1D imaging soft X-ray spectrometer for the small quantum systems instrument at the European XFEL. 用于欧洲 XFEL 小型量子系统仪器的一维成像软 X 射线光谱仪。

IF 2.5 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2024-09-01 Epub Date: 2024-07-30 DOI: 10.1107/S1600577524005988

Marcus Agåker, Johan Söderström, Thomas M Baumann, Carl Johan Englund, Ludvig Kjellsson, Rebecca Boll, Alberto De Fanis, Simon Dold, Tommaso Mazza, Jacobo Montaño, Astrid Münnich, Terence Mullins, Yevheniy Ovcharenko, Nils Rennhack, Philipp Schmidt, Björn Senfftleben, Monica Turcato, Sergey Usenko, Michael Meyer, Joseph Nordgren, Jan Erik Rubensson

引用次数: 0

TEMPUS, a Timepix4-based system for the event-based detection of X-rays. TEMPUS 是一个基于 Timepix4 的系统，用于对 X 射线进行基于事件的检测。

IF 2.5 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2024-09-01 Epub Date: 2024-07-23 DOI: 10.1107/S1600577524005319

Jonathan Correa, Alexandr Ignatenko, David Pennicard, Sabine Lange, Sergei Fridman, Sebastian Karl, Leon Lohse, Björn Senfftleben, Ilya Sergeev, Sven Velten, Deepak Prajapat, Lars Bocklage, Hubertus Bromberger, Andrey Samartsev, Aleksandr Chumakov, Rudolf Rüffer, Joachim von Zanthier, Ralf Röhlsberger, Heinz Graafsma

引用次数: 0

VUV absorption spectra of water and nitrous oxide by a double-duty differentially pumped gas filter. 通过双作用差泵气体过滤器获得水和一氧化二氮的紫外吸收光谱。

IF 2.5 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2024-09-01 Epub Date: 2024-07-23 DOI: 10.1107/S1600577524005423

Andras Bodi, Jonas Knurr, Patrick Ascher, Patrick Hemberger, Christoph Bostedt, Andre Al Haddad

{"title":"VUV absorption spectra of water and nitrous oxide by a double-duty differentially pumped gas filter.","authors":"Andras Bodi, Jonas Knurr, Patrick Ascher, Patrick Hemberger, Christoph Bostedt, Andre Al Haddad","doi":"10.1107/S1600577524005423","DOIUrl":"10.1107/S1600577524005423","url":null,"abstract":"The differentially pumped rare-gas filter at the end of the VUV beamline of the Swiss Light Source has been adapted to house a windowless absorption cell for gases. Absorption spectra can be recorded from 7 eV to up to 21 eV photon energies routinely, as shown by a new water and nitrous oxide absorption spectrum. By and large, the spectra agree with previously published ones both in terms of resonance energies and absorption cross sections, but that of N2O exhibits a small shift in the {tilde{bf D}} band and tentative fine structures that have not yet been fully described. This setup will facilitate the measurement of absorption spectra in the VUV above the absorption edge of LiF and MgF2 windows. It will also allow us to carry out condensed-phase measurements on thin liquid sheets and solid films. Further development options are discussed, including the recording of temperature-dependent absorption spectra, a stationary gas cell for calibration measurements, and the improvement of the photon energy resolution.","PeriodicalId":48729,"journal":{"name":"Journal of Synchrotron Radiation","volume":" ","pages":"1257-1263"},"PeriodicalIF":2.5,"publicationDate":"2024-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11371026/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141753121","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Development of a flat jet delivery system for soft X-ray spectroscopy at MAX IV. 开发用于 MAX IV 软 X 射线光谱分析的平面射流传输系统。

IF 2.5 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2024-09-01 Epub Date: 2024-08-22 DOI: 10.1107/S1600577524006611

Tamires Gallo, Luigi Adriano, Michael Heymann, Agnieszka Wrona, Noelle Walsh, Gunnar Öhrwall, Flavia Callefo, Slawomir Skruszewicz, Mahesh Namboodiri, Ricardo Marinho, Joachim Schulz, Joana Valerio

{"title":"Development of a flat jet delivery system for soft X-ray spectroscopy at MAX IV.","authors":"Tamires Gallo, Luigi Adriano, Michael Heymann, Agnieszka Wrona, Noelle Walsh, Gunnar Öhrwall, Flavia Callefo, Slawomir Skruszewicz, Mahesh Namboodiri, Ricardo Marinho, Joachim Schulz, Joana Valerio","doi":"10.1107/S1600577524006611","DOIUrl":"10.1107/S1600577524006611","url":null,"abstract":"One of the most challenging aspects of X-ray research is the delivery of liquid sample flows into the soft X-ray beam. Currently, cylindrical microjets are the most commonly used sample injection systems for soft X-ray liquid spectroscopy. However, they suffer from several drawbacks, such as complicated geometry due to their curved surface. In this study, we propose a novel 3D-printed nozzle design by introducing microscopic flat sheet jets that provide micrometre-thick liquid sheets with high stability, intending to make this technology more widely available to users. Our research is a collaboration between the EuXFEL and MAX IV research facilities. This collaboration aims to develop and refine a 3D-printed flat sheet nozzle design and a versatile jetting platform that is compatible with multiple endstations and measurement techniques. Our flat sheet jet platform improves the stability of the jet and increases its surface area, enabling more precise scanning and differential measurements in X-ray absorption, scattering, and imaging applications. Here, we demonstrate the performance of this new arrangement for a flat sheet jet setup with X-ray photoelectron spectroscopy, photoelectron angular distribution, and soft X-ray absorption spectroscopy experiments performed at the photoemission endstation of the FlexPES beamline at MAX IV Laboratory in Lund, Sweden.","PeriodicalId":48729,"journal":{"name":"Journal of Synchrotron Radiation","volume":" ","pages":"1285-1292"},"PeriodicalIF":2.5,"publicationDate":"2024-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11371042/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142019258","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

A versatile sample-delivery system for X-ray photoelectron spectroscopy of in-flight aerosols and free nanoparticles at MAX IV Laboratory. MAX IV 实验室用于飞行气溶胶和游离纳米粒子 X 射线光电子能谱分析的多功能样品输送系统。

IF 2.5 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2024-09-01 Epub Date: 2024-08-07 DOI: 10.1107/S1600577524005411

C Preger, J Rissler, A Kivimäki, A C Eriksson, N Walsh

{"title":"A versatile sample-delivery system for X-ray photoelectron spectroscopy of in-flight aerosols and free nanoparticles at MAX IV Laboratory.","authors":"C Preger, J Rissler, A Kivimäki, A C Eriksson, N Walsh","doi":"10.1107/S1600577524005411","DOIUrl":"10.1107/S1600577524005411","url":null,"abstract":"Aerosol science is of utmost importance for both climate and public health research, and in recent years X-ray techniques have proven effective tools for aerosol-particle characterization. To date, such methods have often involved the study of particles collected onto a substrate, but a high photon flux may cause radiation damage to such deposited particles and volatile components can potentially react with the surrounding environment after sampling. These and many other factors make studies on collected aerosol particles challenging. Therefore, a new aerosol sample-delivery system dedicated to X-ray photoelectron spectroscopy studies of aerosol particles and gas molecules in-flight has been developed at the MAX IV Laboratory. The aerosol particles are brought from atmospheric pressure to vacuum in a continuous flow, ensuring that the sample is constantly renewed, thus avoiding radiation damage, and allowing measurements on the true unsupported aerosol. At the same time, available gas molecules can be used for energy calibration and to study gas-particle partitioning. The design features of the aerosol sample-delivery system and important information on the operation procedures are described in detail here. Furthermore, to demonstrate the experimental range of the aerosol sample-delivery system, results from aerosol particles of different shape, size and composition are presented, including inorganic atmospheric aerosols, secondary organic aerosols and engineered nanoparticles.","PeriodicalId":48729,"journal":{"name":"Journal of Synchrotron Radiation","volume":" ","pages":"1382-1392"},"PeriodicalIF":2.5,"publicationDate":"2024-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11371056/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141903285","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Development and commissioning of a broadband online X-ray spectrometer for the SXFEL Facility. 为 SXFEL 设施开发和调试宽带在线 X 射线光谱仪。

IF 2.5 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2024-09-01 Epub Date: 2024-07-29 DOI: 10.1107/S1600577524005812

Zhicheng Yang, Ximing Zhang, Heping Geng, Jiahua Chen, Chao Feng, Bo Liu, Bin Li

引用次数: 0