Journal of Synchrotron Radiation最新文献

Towards a new vision of PaNET: enhancing reasoning capabilities for better photon and neutron data discovery. 迈向PaNET的新愿景：增强推理能力以更好地发现光子和中子数据。

IF 3 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2025-09-01 Epub Date: 2025-07-30 DOI: 10.1107/S1600577525005272

Terence Tan, Balázs Bagó, Sebastian Busch, Renaud Duyme, Guillaume Gaisné, Alejandra Noemí González Beltrán, Heike Görzig, Giannis Koumoutsos, Rolf Krahl, Paul Millar, Carlo Minotti, Melanie Nentwich, Lajos Schrettner, Kirsty Syder, Philippe Rocca-Serra, Susanna Assunta Sansone, Stephen P Collins

{"title":"Towards a new vision of PaNET: enhancing reasoning capabilities for better photon and neutron data discovery.","authors":"Terence Tan, Balázs Bagó, Sebastian Busch, Renaud Duyme, Guillaume Gaisné, Alejandra Noemí González Beltrán, Heike Görzig, Giannis Koumoutsos, Rolf Krahl, Paul Millar, Carlo Minotti, Melanie Nentwich, Lajos Schrettner, Kirsty Syder, Philippe Rocca-Serra, Susanna Assunta Sansone, Stephen P Collins","doi":"10.1107/S1600577525005272","DOIUrl":"10.1107/S1600577525005272","url":null,"abstract":"The Photon and Neutron Experimental Techniques (PaNET) ontology was released in 2021 as an ontology for two major European research infrastructure communities. It provides a standardized taxonomy of experimental techniques employed across the photon and neutron scientific domain, and is part of a wider effort to apply the FAIR (findable, accessible, interoperable, reusable) principles within the community. Specifically, it is used to enhance the quality of metadata in photon and neutron data catalogue services. However, PaNET currently relies on a manual definition approach, which is time consuming and incomplete. A new structure of PaNET is proposed to address this by including logical frameworks that enable automatic reasoning as opposed to the manual approach in the original ontology, resulting in over a hundred new technique subclass relationships that are currently missing in PaNET. These new relationships, which are evaluated by the PaNET working group and other domain experts, will improve data catalogue searches by connecting users to more relevant datasets, thereby enhancing data discoverability. In addition, the results of this work serve as a validation mechanism for PaNET, as the very process of building the logical frameworks, as well as any incorrect inferences made by the reasoner, has exposed existing issues within the original ontology.","PeriodicalId":48729,"journal":{"name":"Journal of Synchrotron Radiation","volume":" ","pages":"1361-1369"},"PeriodicalIF":3.0,"publicationDate":"2025-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC12416419/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144754857","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Eikonal Phase Retrieval: unleashing the potential of fourth-generation sources for enhanced propagation-based tomography on biological samples. Eikonal相位检索：释放第四代源的潜力，增强生物样品的基于传播的断层扫描。

IF 3 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2025-09-01 Epub Date: 2025-07-17 DOI: 10.1107/S1600577525005223

Alessandro Mirone, Joseph Brunet, Theresa Urban, Hector Dejea, Leandre Admans, Renaud Boistel, Morgane Sowinski, Pierre Paleo, Henry Payno, Stijn E Verleden, Camille Berruyer, Elodie Boller, Claire L Walsh, Peter D Lee, Paul Tafforeau

{"title":"Eikonal Phase Retrieval: unleashing the potential of fourth-generation sources for enhanced propagation-based tomography on biological samples.","authors":"Alessandro Mirone, Joseph Brunet, Theresa Urban, Hector Dejea, Leandre Admans, Renaud Boistel, Morgane Sowinski, Pierre Paleo, Henry Payno, Stijn E Verleden, Camille Berruyer, Elodie Boller, Claire L Walsh, Peter D Lee, Paul Tafforeau","doi":"10.1107/S1600577525005223","DOIUrl":"10.1107/S1600577525005223","url":null,"abstract":"The evolution of synchrotrons towards higher brilliance beams has increased the possible sample-to-detector propagation distances for which the source confusion circle does not lead to geometrical blurring. This makes it possible to push near-field propagation-driven phase-contrast enhancement to the limit, revealing low-contrast features that would otherwise remain hidden under excessive noise. Until now, this possibility was hindered in many objects of scientific interest by the simultaneous presence of strong phase gradient regions and low contrast features. The strong gradients, when enhanced with the now possible long propagation distances, induce such strong phase effects that the linearization assumptions of current state-of-the-art single-distance phase retrieval filters are broken, and the resulting image quality is jeopardized. Here, we introduce a new iterative phase retrieval algorithm and compare it with the Paganin phase retrieval algorithm, in both the monochromatic and polychromatic cases. In the polychromatic case the comparison was done with an extrapolated Paganin algorithm obtained by reintroducing, into our phase retrieval algorithm, the linearization approximations underlying the Paganin forward model. Our work provides an innovative algorithm that efficiently performs the phase retrieval task over the entire near-field range, producing images of superior quality for mixed attenuation objects. Our tests on data with shorter propagation distances show that the artifacts, which our algorithm effectively addresses, are present already in more standard third-generation synchrotron setups. This highlights the potential broad applicability of the Eikonal Phase Retrieval method.","PeriodicalId":48729,"journal":{"name":"Journal of Synchrotron Radiation","volume":" ","pages":"1291-1301"},"PeriodicalIF":3.0,"publicationDate":"2025-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC12416417/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144650979","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Measurements of source emittance and beam coherence properties of the upgraded Advanced Photon Source. 升级后的先进光子源发射度和光束相干性的测量。

IF 3 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2025-09-01 Epub Date: 2025-08-15 DOI: 10.1107/S160057752500579X

Xianbo Shi, Yu Chung Lin, Jiyong Zhao, Thomas Toellner, Michael Y Hu, Soenke Seifert, Byeongdu Lee, Walan Grizolli, Michael J Wojcik, Luca Rebuffi, Lahsen Assoufid, Vadim Sajaev

{"title":"Measurements of source emittance and beam coherence properties of the upgraded Advanced Photon Source.","authors":"Xianbo Shi, Yu Chung Lin, Jiyong Zhao, Thomas Toellner, Michael Y Hu, Soenke Seifert, Byeongdu Lee, Walan Grizolli, Michael J Wojcik, Luca Rebuffi, Lahsen Assoufid, Vadim Sajaev","doi":"10.1107/S160057752500579X","DOIUrl":"10.1107/S160057752500579X","url":null,"abstract":"The Advanced Photon Source (APS) has been upgraded with a multi-bend achromat lattice, achieving significantly reduced electron beam emittance and enhanced X-ray coherence. Precise characterization of these properties is essential for optimizing beamline performance and enabling new experiments that take full advantage of the upgraded source. We report on measurements of source size and transverse coherence properties using grating interferometry at two beamlines: the APS 3-ID-B undulator beamline and the 1-BM-B bending magnet beamline. The results confirm the world-record horizontal emittance of the upgraded APS below 30 pm rad and validate the theoretical design parameters. We further investigate the impact of optical aberrations and mechanical vibrations at the 12-ID-C beamline on coherence preservation. These measurements establish a benchmark for future beamline enhancements and demonstrate the effectiveness of grating interferometry for high-precision beam characterization. Our findings provide critical insights into synchrotron beam dynamics, coherence degradation mechanisms, and strategies for optimizing beamline X-ray optics at next-generation light sources.","PeriodicalId":48729,"journal":{"name":"Journal of Synchrotron Radiation","volume":" ","pages":"1152-1161"},"PeriodicalIF":3.0,"publicationDate":"2025-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC12416411/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144859821","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Arbitrary thickness profile metrology of low-Z and monolithic material components with a single X-ray projection. 用单个x射线投影测量低z和单片材料组件的任意厚度剖面。

IF 3 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2025-09-01 Epub Date: 2025-07-31 DOI: 10.1107/S1600577525005521

Wenjie Hao, Feixiang Wang, Fucheng Yu, Kang Du, Ke Li, Junxiong Fang, Tiqiao Xiao

{"title":"Arbitrary thickness profile metrology of low-Z and monolithic material components with a single X-ray projection.","authors":"Wenjie Hao, Feixiang Wang, Fucheng Yu, Kang Du, Ke Li, Junxiong Fang, Tiqiao Xiao","doi":"10.1107/S1600577525005521","DOIUrl":"10.1107/S1600577525005521","url":null,"abstract":"Low-Z and monolithic material components with arbitrary thickness profiles are extensively utilized in heat conduction, biocompatible implants, microfluidics and integrated optics, where precise thickness measurement is crucial for quality control and performance analysis. X-ray micro-computed tomography (micro-CT) is widely employed for thickness metrology of such samples due to its nondestructive nature, high resolution and 3D imaging capabilities. However, the time-consuming projection acquisition and image reconstruction processes hinder it from efficient or dynamic thickness measurements. Additionally, micro-CT struggles with laminar samples. To overcome these limitations, we introduce X-ray phase contrast imaging for the thickness metrology of low-Z materials with arbitrary profiles by accurately retrieving the phase shift of X-rays passing through the sample from a single projection. Calibration using a standard nylon fiber demonstrates that within a 1.33 mm field of view (FOV) the method achieves a mean absolute error of 0.68 µm for cylindrical fibers with diameters of 407.14 µm. We further demonstrate the method's capability for efficient measurement and damage assessment using a worn fiber with complex geometry. Additionally, we applied this method to the thickness measurement and error analysis of a microlens array with varying sub-lens parameters. The 3D profiles of all sub-lenses were obtained from a single projection, facilitating error analysis of height, symmetry and eccentricity. The results highlight the method's advantages, including being in situ, non-contact and high precision, and having a large FOV, flexible adjustability and penetrative measurement capabilities. Our open device design suggests potential applications for dynamic thickness measurements and real-time monitoring of samples within in situ loading devices.","PeriodicalId":48729,"journal":{"name":"Journal of Synchrotron Radiation","volume":" ","pages":"1310-1318"},"PeriodicalIF":3.0,"publicationDate":"2025-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC12416431/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144762044","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

A new framework for X-ray absorption spectroscopy data analysis based on machine learning: XASDAML. 基于机器学习的x射线吸收光谱数据分析新框架：XASDAML。

IF 3 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2025-09-01 Epub Date: 2025-07-21 DOI: 10.1107/S1600577525005351

Xue Han, Haodong Yao, Fei Zhan, Xueqi Song, Junfang Zhao, Haifeng Zhao

{"title":"A new framework for X-ray absorption spectroscopy data analysis based on machine learning: XASDAML.","authors":"Xue Han, Haodong Yao, Fei Zhan, Xueqi Song, Junfang Zhao, Haifeng Zhao","doi":"10.1107/S1600577525005351","DOIUrl":"10.1107/S1600577525005351","url":null,"abstract":"X-ray absorption spectroscopy (XAS) is a critical analytical technique for comprehensively characterizing the electronic configurations and atomic structures of materials. The rapid growth in both data volume and complexity, driven by modern synchrotron radiation facilities, necessitates computational frameworks capable of efficiently processing large-scale XAS datasets. To address this need, we introduce XASDAML, a machine-learning-based platform that integrates the entire data processing workflow. The framework coordinates key operational processes, including spectral-structural descriptor generation, predictive modeling and performance validation, while facilitating statistical analyses through principal component decomposition and clustering algorithms to uncover latent patterns within datasets. Designed with modular architecture, the system enables independent modification or enhancement of individual components, ensuring flexibility to meet evolving analytical demands. Implemented through a Jupyter Notebook-based interface, the platform ensures accessibility for researchers. The framework is validated with two case studies: (i) copper-foil EXAFS data show that it can predict coordination numbers and radial distribution functions; and (ii) XANES spectra of the spin-crossover complex Fe(phen)3 uncover bond-length changes between the low-spin and high-spin states. Comprehensive validation highlights robust toolkit functionalities, including statistical descriptor analyses, spectral visualization, and prediction of widely employed structural descriptors closely reflecting local atomic environments. By establishing standardized and extensible procedures for integrating machine learning into XAS analysis, XASDAML enhances research efficiency, promotes richer data insights, and provides a versatile computational resource tailored to the expanding needs of XAS research.","PeriodicalId":48729,"journal":{"name":"Journal of Synchrotron Radiation","volume":" ","pages":"1244-1256"},"PeriodicalIF":3.0,"publicationDate":"2025-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC12416422/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144676237","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Compression-tension cell with sample manipulator for in situ X-ray nanotomography experiments. 用于现场x射线纳米层析成像实验的带有样品机械手的压缩-张力单元。

IF 3 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2025-09-01 Epub Date: 2025-07-14 DOI: 10.1107/S1600577525005053

Arun J Bhattacharjee, Harold S Barnard, Alastair MacDowell, Dilworth Parkinson, Harrison P Lisabeth

{"title":"Compression-tension cell with sample manipulator for in situ X-ray nanotomography experiments.","authors":"Arun J Bhattacharjee, Harold S Barnard, Alastair MacDowell, Dilworth Parkinson, Harrison P Lisabeth","doi":"10.1107/S1600577525005053","DOIUrl":"10.1107/S1600577525005053","url":null,"abstract":"In situ X-ray nanotomography experiments where tensile or compressive force is applied on the sample require specialized equipment. A compression-tension device with fluid flow-through capability has been designed for X-ray nanotomography beamlines. The compression-tension cell is equipped with a triaxial stage for sample alignment and a high sensitivity loadcell for measurement of applied force. To handle the <100 µm samples used for X-ray nanotomography imaging and for loading samples on the compression-tension cell a sample manipulator has been built. The sample manipulator is capable of selecting a single <100 µm particle for nanotomography scanning while viewing multiple samples under an optical microscope. To test the functionality of these two devices an initial compression experiment involving two glass beads was performed. To demonstrate instrument stability two spherical glass beads were compressed from a no load condition until one of the beads fractured. Nanotomography data were collected at each step of increasing compressive force. The experimentally observed contact area of the spherical glass beads was compared with the theoretical estimate using the Hertz analysis. To demonstrate the fluid flow capability, two calcite grains were compressed against each other under a calcite saturated solution. Surface topological changes were observed for the stressed grain contact area.","PeriodicalId":48729,"journal":{"name":"Journal of Synchrotron Radiation","volume":" ","pages":"1282-1290"},"PeriodicalIF":3.0,"publicationDate":"2025-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC12416415/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144638477","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

X-ray fluorescence holography under high-pressure conditions. 高压条件下的x射线荧光全息术。

IF 3 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2025-09-01 Epub Date: 2025-07-18 DOI: 10.1107/S1600577525005284

Xinhui Zhan, Naoki Ishimatsu, Koji Kimura, Naohisa Happo, Halubai Sekhar, Tomoko Sato, Nobuo Nakajima, Naomi Kawamura, Kotaro Higashi, Oki Sekizawa, Hirokazu Kadobayashi, Ritsuko Eguchi, Yoshihiro Kubozono, Hiroo Tajiri, Shinya Hosokawa, Tomohiro Matsushita, Toru Shinmei, Tetsuo Irifune, Koichi Hayashi

{"title":"X-ray fluorescence holography under high-pressure conditions.","authors":"Xinhui Zhan, Naoki Ishimatsu, Koji Kimura, Naohisa Happo, Halubai Sekhar, Tomoko Sato, Nobuo Nakajima, Naomi Kawamura, Kotaro Higashi, Oki Sekizawa, Hirokazu Kadobayashi, Ritsuko Eguchi, Yoshihiro Kubozono, Hiroo Tajiri, Shinya Hosokawa, Tomohiro Matsushita, Toru Shinmei, Tetsuo Irifune, Koichi Hayashi","doi":"10.1107/S1600577525005284","DOIUrl":"10.1107/S1600577525005284","url":null,"abstract":"This study reports the first application of X-ray fluorescence holography (XFH) under high-pressure conditions. We integrated XFH with a diamond anvil cell to investigate the local structure around Sr atoms in single-crystal SrTiO3 under high pressure. By utilizing nano-polycrystalline diamond anvils and a yttrium filter, we effectively eliminated significant background noise from both the anvils and the gasket. This optimized experimental configuration enabled the measurement of Sr Kα holograms of the SrTiO3 sample at pressures up to 13.3 GPa. The variation of lattice constants with pressure was calculated by the shifts of Kossel lines, and real-space images of the atomic structures were reconstructed from the Sr Kα holograms at different pressures. This work successfully demonstrates the feasibility of employing XFH under high-pressure conditions as a novel method for visualizing pressure-induced changes in the three-dimensional local structure around the specified element.","PeriodicalId":48729,"journal":{"name":"Journal of Synchrotron Radiation","volume":" ","pages":"1302-1309"},"PeriodicalIF":3.0,"publicationDate":"2025-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC12416426/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144660851","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Optical kicking of liquid droplets for sample delivery in ultrafast soft X-ray experiments. 超快软x射线实验中液滴光踢送样品。

IF 3 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2025-09-01 Epub Date: 2025-07-21 DOI: 10.1107/S1600577525005430

Zeinab Ebrahimpour, Dan Cojoc, Emiliano Principi, Riccardo Mincigrucci

{"title":"Optical kicking of liquid droplets for sample delivery in ultrafast soft X-ray experiments.","authors":"Zeinab Ebrahimpour, Dan Cojoc, Emiliano Principi, Riccardo Mincigrucci","doi":"10.1107/S1600577525005430","DOIUrl":"10.1107/S1600577525005430","url":null,"abstract":"We present a technique based on the optical force of a femtosecond laser acting on liquid micro-droplets for their precise manipulation in a vacuum, enabling an efficient sample delivery system for soft X-ray experiments. Conventional liquid jet methods, which are utilized in soft X-ray experiments, consume large sample volumes and offer limited control over droplet trajectories, leading to significant sample waste. Our approach uses optical forces from a femtosecond-pulsed focused laser to deflect free-falling droplets, guiding them with high precision toward the interaction region. This significantly reduces sample waste while enabling real-time control over droplet positioning. To understand the behavior of droplets in vacuum and their interaction with the focused laser beam, we employ theoretical analysis and numerical simulations. Hertz-Knudsen equations describe the thermodynamics of free-falling and deflected droplets, allowing estimation of their temperature and size as a function of time and position. The optical force acting on the droplets is determined using the transfer matrix method and Lorenz-Mie theory. The proposed technique provides fine tuning over delivery time and thermodynamic properties of the liquid sample, offering a promising platform for investigating supercooled liquid micro-droplets and phase transitions. It is a particularly well suited liquid sample delivery method for ultrafast X-ray experiments using tabletop sources, as well as current and future free-electron laser and high harmonic generation facilities.","PeriodicalId":48729,"journal":{"name":"Journal of Synchrotron Radiation","volume":" ","pages":"1184-1193"},"PeriodicalIF":3.0,"publicationDate":"2025-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC12416435/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144676239","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Crystal-field splitting strength of U-6d orbitals in NaUO₃, KUO₃ and RbUO₃. nao3、KUO3和rbuoy中U-6d轨道的晶体场分裂强度。

IF 3 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2025-09-01 Epub Date: 2025-07-30 DOI: 10.1107/S1600577525005156

Simon Orlat, Igor Prozheev, Ine Arts, Gregory Leinders, Elena Bazarkina, Kristina Kvashnina, Filip Tuomisto, Philippe Martin, Philippe Moisy, René Bes

引用次数: 0

A high throughput and micrometre spatial resolution design for a versatile resonant inelastic X-ray scattering spectrometer. 一种多用途共振非弹性x射线散射光谱仪的高通量和微米空间分辨率设计。

IF 3 3区物理与天体物理

Journal of Synchrotron Radiation Pub Date : 2025-09-01 Epub Date: 2025-07-17 DOI: 10.1107/S1600577525005314

Ruijie Wang, Pengjun Zhang, Qingchen Li, Yujian Xia, Lisheng Qian, Xuefei Feng, Shuangming Chen, Xiaosong Liu

{"title":"A high throughput and micrometre spatial resolution design for a versatile resonant inelastic X-ray scattering spectrometer.","authors":"Ruijie Wang, Pengjun Zhang, Qingchen Li, Yujian Xia, Lisheng Qian, Xuefei Feng, Shuangming Chen, Xiaosong Liu","doi":"10.1107/S1600577525005314","DOIUrl":"10.1107/S1600577525005314","url":null,"abstract":"A versatile scheme has been meticulously engineered for a resonant inelastic X-ray scattering spectrometer, enabling free switching between high throughput configurations with narrow spatial-resolution and low throughput setups boasting broad spatial-resolution capabilities. The high throughput mode enhances signal intensity threefold compared with setups with only the dispersive subassembly, while achieving 2.7 µm resolution within a 16 µm range. Alternatively, the broad spatial-resolution mode achieves 2.7 µm resolution across the entire optical footprint. Furthermore, the incorporation of specialized mirrors not only facilitates focusing but also paves the way for potential enhancements to the strip-shaped detector, thereby augmenting its resolution. By employing a vertically compact beam spot in conjunction with the Hettrick-Underwood optical configuration, this spectrometer attains a resolving power surpassing 12000 for 284-780 eV. This work provides an exhaustive exploration of the multifaceted attributes to the spectrometer's optical design, highlighting its adaptability and high performance in diverse experimental scenarios.","PeriodicalId":48729,"journal":{"name":"Journal of Synchrotron Radiation","volume":" ","pages":"1235-1243"},"PeriodicalIF":3.0,"publicationDate":"2025-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC12416433/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144650978","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0