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The role of interaction work in martensite deformation 相互作用功在马氏体变形中的作用
IF 5.3 2区 材料科学
Scripta Materialia Pub Date : 2024-10-30 DOI: 10.1016/j.scriptamat.2024.116433
J.F. Xiao, C. Cayron, R.E. Logé
{"title":"The role of interaction work in martensite deformation","authors":"J.F. Xiao,&nbsp;C. Cayron,&nbsp;R.E. Logé","doi":"10.1016/j.scriptamat.2024.116433","DOIUrl":"10.1016/j.scriptamat.2024.116433","url":null,"abstract":"<div><div>This study elucidates the evolution of martensite deformation via Interaction Work (IW). The IW is the mechanical work done by external loading, assisting deformation by competing with the energy barrier. This interplay establishes the maximum IW (IW<sub>max</sub>) criterion for variant selection of different deformation modes. Considering multiple deformation modes (A, B, …), the deformation mode with <span><math><mrow><mi>m</mi><mi>i</mi><mi>n</mi><mo>{</mo><mrow><mi>I</mi><msubsup><mi>W</mi><mrow><mi>m</mi><mi>a</mi><mi>x</mi></mrow><mi>A</mi></msubsup><mo>,</mo><mspace></mspace><mi>I</mi><msubsup><mi>W</mi><mrow><mi>m</mi><mi>a</mi><mi>x</mi></mrow><mi>B</mi></msubsup><mo>,</mo><mo>…</mo></mrow><mo>}</mo></mrow></math></span> is expected to be activated first due to a lower energy barrier when subjected to deformation, which hints the evolution of martensite microstructures with the increasing trajectory of IW<sub>max</sub> of various deformation modes. We validated this hypothesis by examining reorientation and deformation twinning in monoclinic martensite (B19’) in NiTi, orthorhombic (<em>α</em>’’), hexagonal martensite (<em>α</em>’) in Ti-based alloys, and γ’ martensite in CuAlNi shape memory alloys, and by comparing the predictions with existing literature.</div></div>","PeriodicalId":423,"journal":{"name":"Scripta Materialia","volume":"256 ","pages":"Article 116433"},"PeriodicalIF":5.3,"publicationDate":"2024-10-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142552878","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
3D micromechanical interaction of thin-film retained austenite and lath martensite by computational plasticity 通过计算塑性实现薄膜保留奥氏体和板条马氏体的三维微机械相互作用
IF 5.3 2区 材料科学
Scripta Materialia Pub Date : 2024-10-30 DOI: 10.1016/j.scriptamat.2024.116434
Tim Fischer , Mina Amiri , Joshua Kumpati , Peter Hedström , Annika Borgenstam
{"title":"3D micromechanical interaction of thin-film retained austenite and lath martensite by computational plasticity","authors":"Tim Fischer ,&nbsp;Mina Amiri ,&nbsp;Joshua Kumpati ,&nbsp;Peter Hedström ,&nbsp;Annika Borgenstam","doi":"10.1016/j.scriptamat.2024.116434","DOIUrl":"10.1016/j.scriptamat.2024.116434","url":null,"abstract":"<div><div>To exploit the full potential of advanced high-strength steels (AHSS), a more in-depth understanding of the complex micromechanical interaction of thin-film retained austenite (RA) and lath martensite is indispensable. Inspired by the medium-Mn steel microstructure, a three-dimensional micromechanical modeling approach is therefore proposed in the present work, embedding the thin RA films explicitly into the hierarchical lath martensite structure. This enables systematic studies of the effect of RA film thickness and volume fraction on the local stresses and strains as well as their partitioning within the microstructure. The investigations reveal that with shrinking RA volume fraction, both stress and especially strain heterogeneity in the thin-film RA intensifies. In the martensite blocks, stress and strain heterogeneity also intensifies, although stresses are generally more heterogeneously, and strains much more homogeneously, distributed than in RA. The results underline the key role of RA with thin-film morphology for further optimizing AHSS microstructures.</div></div>","PeriodicalId":423,"journal":{"name":"Scripta Materialia","volume":"256 ","pages":"Article 116434"},"PeriodicalIF":5.3,"publicationDate":"2024-10-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142552967","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Superhigh strength and ductile press-hardening steel produced by shortened austenitization of microstructure containing Mn/Cr-rich cementite particles 通过对含有富 Mn/Cr 雪明碳铁颗粒的微观结构进行短时奥氏体化生产超高强度和韧性压淬钢
IF 5.3 2区 材料科学
Scripta Materialia Pub Date : 2024-10-30 DOI: 10.1016/j.scriptamat.2024.116435
Cancan Ding , Chengyuan Deng , Qinyi Guo , Zhipeng Liu , Ru Ge , Bin Hu , Shilei Li , Haiwen Luo
{"title":"Superhigh strength and ductile press-hardening steel produced by shortened austenitization of microstructure containing Mn/Cr-rich cementite particles","authors":"Cancan Ding ,&nbsp;Chengyuan Deng ,&nbsp;Qinyi Guo ,&nbsp;Zhipeng Liu ,&nbsp;Ru Ge ,&nbsp;Bin Hu ,&nbsp;Shilei Li ,&nbsp;Haiwen Luo","doi":"10.1016/j.scriptamat.2024.116435","DOIUrl":"10.1016/j.scriptamat.2024.116435","url":null,"abstract":"<div><div>We developed a novel Si/Cr-alloyed martensitic press-hardening steel (PHS), which has ultimate tensile strength (UTS) of 2280 MPa and total elongation (TE) of 10.9 % after a short hot-forming process, far superior to the present 22MnB5 PHS. Such an unprecedented mechanical combination is primarily attributed to the sufficient retained austenite (RA) grains with evenly distributed mechanical stabilities, which is realized by dissolving nearly 50 % volume percentage of Mn/Cr-rich cementite particles during the short soaking with the guidance of the numerical simulations. As a result, some RA grains have the C/Mn/Cr-enriched cores and other have the cementite cores that are neighbored with high C/Mn/Cr concentrations and steep gradients. This leads to the great heterogeneity in the mechanical stabilities of RA grains in a wide range so that these RA grains are able to provide a continuous TRIP effect for sustainably enhanced work hardening during deformation.</div></div>","PeriodicalId":423,"journal":{"name":"Scripta Materialia","volume":"256 ","pages":"Article 116435"},"PeriodicalIF":5.3,"publicationDate":"2024-10-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142552875","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Formation of single-phased B2 multi-principal element intermetallics: From experiments to modeling 单相 B2 多主元素金属间化合物的形成:从实验到建模
IF 5.3 2区 材料科学
Scripta Materialia Pub Date : 2024-10-30 DOI: 10.1016/j.scriptamat.2024.116437
Weijiang Zhao , Hang Wang , Quanfeng He , Hu Li , Li Wang , Bin Liu , Yong Liu , Yong Yang
{"title":"Formation of single-phased B2 multi-principal element intermetallics: From experiments to modeling","authors":"Weijiang Zhao ,&nbsp;Hang Wang ,&nbsp;Quanfeng He ,&nbsp;Hu Li ,&nbsp;Li Wang ,&nbsp;Bin Liu ,&nbsp;Yong Liu ,&nbsp;Yong Yang","doi":"10.1016/j.scriptamat.2024.116437","DOIUrl":"10.1016/j.scriptamat.2024.116437","url":null,"abstract":"<div><div>In this study, a variety of Co-Ni-Ti-Zr alloys with various compositions were examined to identify potential single-phase B2 intermetallics. While classical theoretical models suggested that most compositions would present multiple phases or even amorphous phases, the equiatomic CoNiTiZr alloy revealed a stable single-phased B2 structure even under extended annealing at temperatures approaching its melting point. Notably, this alloy showcased desirable properties, such as a strong Elinvar effect and a high elastic strain limit. To aid in the design of B2 multi-principal elemental intermetallics (MPEIs), we proposed a pseudo-binary system model that counts for both chemical long-range order across two sublattices and random atom mixing within each sublattice. The outcome of this study is expected to accelerate the identification of valuable B2 MPEIs.</div></div>","PeriodicalId":423,"journal":{"name":"Scripta Materialia","volume":"256 ","pages":"Article 116437"},"PeriodicalIF":5.3,"publicationDate":"2024-10-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142552873","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
An atomistic structural description of the ferrielectric polar phase involving non-coplanar cation displacements 涉及非共面阳离子位移的铁电极相原子结构描述
IF 5.3 2区 材料科学
Scripta Materialia Pub Date : 2024-10-29 DOI: 10.1016/j.scriptamat.2024.116426
T. Pramanik , Cho Sandar Htet , Alicia Manjón-Sanz , J. Liu , S. Ullah , J. Kong , C. Babori , A. Brézard-Oudot , L. Daniel , S.T. Misture , A. Pramanick
{"title":"An atomistic structural description of the ferrielectric polar phase involving non-coplanar cation displacements","authors":"T. Pramanik ,&nbsp;Cho Sandar Htet ,&nbsp;Alicia Manjón-Sanz ,&nbsp;J. Liu ,&nbsp;S. Ullah ,&nbsp;J. Kong ,&nbsp;C. Babori ,&nbsp;A. Brézard-Oudot ,&nbsp;L. Daniel ,&nbsp;S.T. Misture ,&nbsp;A. Pramanick","doi":"10.1016/j.scriptamat.2024.116426","DOIUrl":"10.1016/j.scriptamat.2024.116426","url":null,"abstract":"<div><div>Materials with antipolar-polar transformation are attractive for their large functional responses. However, the antipolar state remains controversial in many materials. For example, recent studies on archetypical antiferroelectric (AFE) materials indicate an incomplete compensation of antiparallel dipoles, which prompted their alternative definition as ferrielectric. Here, we investigated the origin of the ferrielectric (FIE) state in a classical AFE material using X-ray and neutron total scattering. We show that the FIE state arises from 3-dimensional modulation of the cation-centric electric dipoles, which can be viewed as periodic arrangement of 180° twin boundaries with non-Ising characteristics.</div></div>","PeriodicalId":423,"journal":{"name":"Scripta Materialia","volume":"256 ","pages":"Article 116426"},"PeriodicalIF":5.3,"publicationDate":"2024-10-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142539073","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Simultaneously enhancing the optical transparency and Verdet constant of Tb-based magneto-optical ceramic via defect elimination 通过消除缺陷同时提高铽基磁光陶瓷的光学透明度和维尔德常数
IF 5.3 2区 材料科学
Scripta Materialia Pub Date : 2024-10-28 DOI: 10.1016/j.scriptamat.2024.116417
Haojie Zhang , Shuyi Zhu , Yanli Shi , Kailei Lu , Jianqi Qi , Tiecheng Lu
{"title":"Simultaneously enhancing the optical transparency and Verdet constant of Tb-based magneto-optical ceramic via defect elimination","authors":"Haojie Zhang ,&nbsp;Shuyi Zhu ,&nbsp;Yanli Shi ,&nbsp;Kailei Lu ,&nbsp;Jianqi Qi ,&nbsp;Tiecheng Lu","doi":"10.1016/j.scriptamat.2024.116417","DOIUrl":"10.1016/j.scriptamat.2024.116417","url":null,"abstract":"<div><div>Defects induced by air annealing pose a serious challenge to simultaneously achieve high transparency and high Verdet constant in Tb-based ceramics. Herein, an efficient strategy of air annealing followed by vacuum re-annealing is introduced in response to the dilemma. For the illustrative example, after a sequence of annealing treatments, the in-line transmittance of Tb<sub>2</sub>Hf<sub>2</sub>O<sub>7</sub> ceramics was elevated from 59.1 % to 71.2 % at ∼1440 nm, accompanied by significant increase in the Verdet constant (from -280 ± 3 rad·T<sup>−1</sup>·m<sup>−1</sup> to -307 ± 4 rad·T<sup>−1</sup>·m<sup>−1</sup> at 515 nm and -164 ± 2 rad·T<sup>−1</sup>·m<sup>−1</sup> to -181 ± 3 rad·T<sup>−1</sup>·m<sup>−1</sup> at 635 nm). This improvement was achieved through the elimination of defect clusters and antisite defects within the ceramic without introducing excess detrimental oxygen vacancies. The innovative strategy demonstrated here for Tb based ceramics to simultaneously enhance the optical transparency and Verdet constant may open up a path for developing high-performance MO materials for Faraday isolators.</div></div>","PeriodicalId":423,"journal":{"name":"Scripta Materialia","volume":"256 ","pages":"Article 116417"},"PeriodicalIF":5.3,"publicationDate":"2024-10-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142536310","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Beta phase controls hydride precipitation within alpha phase in dual-phase Zr-2.5Nb 贝塔相控制 Zr-2.5Nb 双相中阿尔法相内的氢化物沉淀
IF 5.3 2区 材料科学
Scripta Materialia Pub Date : 2024-10-28 DOI: 10.1016/j.scriptamat.2024.116419
Yu-Jie Jia, Wei-Zhong Han
{"title":"Beta phase controls hydride precipitation within alpha phase in dual-phase Zr-2.5Nb","authors":"Yu-Jie Jia,&nbsp;Wei-Zhong Han","doi":"10.1016/j.scriptamat.2024.116419","DOIUrl":"10.1016/j.scriptamat.2024.116419","url":null,"abstract":"<div><div>Formation of a new phase usually follows a fixed orientation relationship with matrix in metallic materials, i.e., hydrides prefer to form on the basal plane in hexagonal zirconium (Zr) under thermal equilibrium conditions. Here, we identify that hydride precipitation within α-Zr in dual-phase Zr-2.5Nb deviates from the traditional manner, being governed by β-Zr. Two types of orientation relationships between γ-ZrH and β-Zr are identified, namely Kurdjumov-Sachs and Pitsch. The habit plane of hydrides consistently aligns with {112}<sub>β</sub>. Hydrides can cross various colony boundaries but are obstructed by the β-Zr grain boundary. The high solubility and the fast diffusion rate of hydrogen inside body-centered cubic β-Zr are the origin of the unique hydride phase transformation in dual-phase Zircaloy. Our findings may provide some new understanding for solid-state phase transformation in dual-phase materials.</div></div>","PeriodicalId":423,"journal":{"name":"Scripta Materialia","volume":"256 ","pages":"Article 116419"},"PeriodicalIF":5.3,"publicationDate":"2024-10-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142536311","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Hydrogen diffusion-induced crystallographic changes in α + β titanium alloy 氢扩散诱导的 α + β 钛合金晶体学变化
IF 5.3 2区 材料科学
Scripta Materialia Pub Date : 2024-10-28 DOI: 10.1016/j.scriptamat.2024.116410
Qian Wang , Jianan Hu , Hanbo Weng , Tong Zhang , Lufeng Yang , Jie Chen , Sensen Huang , Min Qi , Yingjie Ma , Daokui Xu , Jiafeng Lei , Rui Yang
{"title":"Hydrogen diffusion-induced crystallographic changes in α + β titanium alloy","authors":"Qian Wang ,&nbsp;Jianan Hu ,&nbsp;Hanbo Weng ,&nbsp;Tong Zhang ,&nbsp;Lufeng Yang ,&nbsp;Jie Chen ,&nbsp;Sensen Huang ,&nbsp;Min Qi ,&nbsp;Yingjie Ma ,&nbsp;Daokui Xu ,&nbsp;Jiafeng Lei ,&nbsp;Rui Yang","doi":"10.1016/j.scriptamat.2024.116410","DOIUrl":"10.1016/j.scriptamat.2024.116410","url":null,"abstract":"<div><div>Hydrogen absorption can cause crystallographic changes in both α and β phase of Ti alloy. To understand them better, the hydrogen diffusion behavior in Ti-5Al-5Mo-2V-2Cr-2Sn-2Zr dual-phase Ti alloy is investigated based on multi-scale characterization. The hydrogen distribution change of electrochemical hydrogen charging sample during aging at room temperature is characterized by neutron imaging technique. The hydride decomposition and hydrogen induced cracking are observed by interrupted in-situ method. Besides, the spinodal decomposition structure is observed in β phase, which is widened by large lattice expansion due to hydrogen absorption. Finally, the interface of δ-hydride/α-Ti with the orientation relationship of <span><math><mrow><mo>{</mo><mn>0001</mn><mo>}</mo><mi>α</mi><mo>/</mo><mo>/</mo><mo>{</mo><mn>001</mn><mo>}</mo><mi>δ</mi></mrow></math></span> <span><math><mrow><mo>&lt;</mo><mn>1</mn><mover><mn>2</mn><mo>¯</mo></mover><mn>10</mn><mo>&gt;</mo><mi>α</mi><mo>/</mo><mo>/</mo><mo>&lt;</mo><mn>110</mn><mo>&gt;</mo><mi>δ</mi></mrow></math></span> is investigated. A new periodic structure formed by {<span><math><mrow><mn>10</mn><mover><mn>1</mn><mo>¯</mo></mover><mn>0</mn></mrow></math></span>} stacking faults is identified as intermediate state of hydride transformation.</div></div>","PeriodicalId":423,"journal":{"name":"Scripta Materialia","volume":"256 ","pages":"Article 116410"},"PeriodicalIF":5.3,"publicationDate":"2024-10-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142536308","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Mechanical properties of Ti/Mg bicontinuous composite by liquid metal replacement 通过液态金属置换获得钛/镁双连续复合材料的力学性能
IF 5.3 2区 材料科学
Scripta Materialia Pub Date : 2024-10-28 DOI: 10.1016/j.scriptamat.2024.116413
Yusuke Ohashi, Hidemi Kato
{"title":"Mechanical properties of Ti/Mg bicontinuous composite by liquid metal replacement","authors":"Yusuke Ohashi,&nbsp;Hidemi Kato","doi":"10.1016/j.scriptamat.2024.116413","DOIUrl":"10.1016/j.scriptamat.2024.116413","url":null,"abstract":"<div><div>A Ti/Mg composite with bicontinuous microstructure of α-Ti/α-Mg was fabricated using a Ti-<em>Sc</em> precursor's microstructure as a template. A Ti-<em>Sc</em> precursor alloy with α-Ti/α-<em>Sc</em> dual-phase microstructure was immersed in molten Mg, and using differences in chemical interactions between the alloy's components and the metallic melt, only α-<em>Sc</em> of the precursor was replaced by molten Mg. The Ti/Mg composite exhibited an ultimate tensile strength of 308.4 MPa and elongation of 6.8 % by a tensile test. The microstructure elongated in the tensile direction indicates that the α-Ti and α-Mg phases cooperatively deformed and contributed to ductility. The continuous microstructure in the tensile direction of the immiscible phases and the weak interface that does not separate because of geometric constraints may be the reason why the hardness properties of the composite follow the Voigt rule.</div></div>","PeriodicalId":423,"journal":{"name":"Scripta Materialia","volume":"256 ","pages":"Article 116413"},"PeriodicalIF":5.3,"publicationDate":"2024-10-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142536309","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
X-ray induced grain boundary formation and grain rotation in Bi2Se3 X 射线诱导的 Bi2Se3 晶界形成和晶粒旋转
IF 5.3 2区 材料科学
Scripta Materialia Pub Date : 2024-10-22 DOI: 10.1016/j.scriptamat.2024.116416
Kento Katagiri , Bernard Kozioziemski , Eric Folsom , Sebastian Göde , Yifan Wang , Karen Appel , Darshan Chalise , Philip K. Cook , Jon Eggert , Marylesa Howard , Sungwon Kim , Zuzana Konôpková , Mikako Makita , Motoaki Nakatsutsumi , Martin M. Nielsen , Alexander Pelka , Henning F. Poulsen , Thomas R. Preston , Tharun Reddy , Jan-Patrick Schwinkendorf , Leora E. Dresselhaus-Marais
{"title":"X-ray induced grain boundary formation and grain rotation in Bi2Se3","authors":"Kento Katagiri ,&nbsp;Bernard Kozioziemski ,&nbsp;Eric Folsom ,&nbsp;Sebastian Göde ,&nbsp;Yifan Wang ,&nbsp;Karen Appel ,&nbsp;Darshan Chalise ,&nbsp;Philip K. Cook ,&nbsp;Jon Eggert ,&nbsp;Marylesa Howard ,&nbsp;Sungwon Kim ,&nbsp;Zuzana Konôpková ,&nbsp;Mikako Makita ,&nbsp;Motoaki Nakatsutsumi ,&nbsp;Martin M. Nielsen ,&nbsp;Alexander Pelka ,&nbsp;Henning F. Poulsen ,&nbsp;Thomas R. Preston ,&nbsp;Tharun Reddy ,&nbsp;Jan-Patrick Schwinkendorf ,&nbsp;Leora E. Dresselhaus-Marais","doi":"10.1016/j.scriptamat.2024.116416","DOIUrl":"10.1016/j.scriptamat.2024.116416","url":null,"abstract":"<div><div>Optimizing grain boundary characteristics in polycrystalline materials can improve their properties. Many processing methods have been developed for grain boundary manipulation, including the use of intense radiation in certain applications. In this work, we used X-ray free electron laser pulses to irradiate single-crystalline bismuth selenide (Bi<sub>2</sub>Se<sub>3</sub>) and observed grain boundary formation and subsequent grain rotation in response to the X-ray radiation. Our observations with simultaneous transmission X-ray microscopy and X-ray diffraction demonstrate how intense X-ray radiation can rapidly change size and texture of grains.</div></div>","PeriodicalId":423,"journal":{"name":"Scripta Materialia","volume":"256 ","pages":"Article 116416"},"PeriodicalIF":5.3,"publicationDate":"2024-10-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142536307","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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