Small MethodsPub Date : 2025-02-16DOI: 10.1002/smtd.202401957
Boguen Kim, Saehun Kim, Dong Gyu Lee, Donghyun Lee, Junsu Son, Hyeonseok Seong, Bumjoon J Kim, Tae Kyung Lee, Nam-Soon Choi
{"title":"Succinonitrile-Rich Electrolyte Solvation Structure Enables Wide-Temperature-Range Operation of Lithium-Metal Batteries.","authors":"Boguen Kim, Saehun Kim, Dong Gyu Lee, Donghyun Lee, Junsu Son, Hyeonseok Seong, Bumjoon J Kim, Tae Kyung Lee, Nam-Soon Choi","doi":"10.1002/smtd.202401957","DOIUrl":"https://doi.org/10.1002/smtd.202401957","url":null,"abstract":"<p><p>Stable lithium-metal batteries (LMBs) with wide-temperature-range operability can be achieved through the rational design of electrolytes based on their physicochemical and electrochemical characteristics, such as their freezing behavior and functional integrity at battery heterointerfaces. This study demonstrates that succinonitrile (SN)-dominated solvation chemistry and fluoroethylene carbonate (FEC)-derived interface engineering can enable the wide-temperature-range operation of LMBs while optimally tuning the microstructures of the electrolyte for facile Li-ion conduction. A mechanically and chemically stable LiF-rich primary solid-electrolyte interphase (SEI) is constructed using FEC and 1,1,2,2-tetrafluoroethyl 2,2,3,3-tetrafluoropropyl ether (TTE). Subsequently, lithium bis(trifluoromethanesulfonyl) imide and SN are utilized to produce ion-conductive Li<sub>3</sub>N in the SEI. SN promoted the build-up of an electron- and N-rich C≡N based cathode-electrolyte interface that could mitigate transition metal-ion dissolution, microcrack formation, and structural degradation in a LiNi<sub>0.8</sub>Co<sub>0.1</sub>Mn<sub>0.1</sub>O<sub>2</sub> (NCM811) cathode. TTE, which exhibits low solvation power, enabled the formation of desirable Li-ion conduction pathways, including a deep depression of the melting point of the electrolyte and low-viscosity Li-ion channels, for low-temperature operation. The integration of interface engineering and electrolyte chemistry provides an efficient strategy for preparing Li|NCM811 full cells demonstrating stable operation under various temperature conditions.</p>","PeriodicalId":229,"journal":{"name":"Small Methods","volume":" ","pages":"e2401957"},"PeriodicalIF":10.7,"publicationDate":"2025-02-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143424726","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Time-resolved Solvothermal Synthesis for Controlling Lateral Size of 2D Metal-Organic Layers.","authors":"Jiawei Chen, Yuhang Song, Yumeng Gan, Wanzhen Cai, Haoshang Wang, Huichong Liu, Bingling Dai, Yuanzhao Peng, Cheng Wang","doi":"10.1002/smtd.202402078","DOIUrl":"https://doi.org/10.1002/smtd.202402078","url":null,"abstract":"<p><p>Metal-Organic Layers (MOLs), 2D analogs of Metal-Organic Frameworks (MOFs), feature monolayer structures with the potential for various applications. Controlling the lateral size of MOLs is essential for enhancing their dispersibility in solvents and optimizing performance. However, reducing lateral dimensions while preserving monolayer thickness presents a challenge due to the precise conditions required for monolayer formation. This study utilizes a time-resolved solvothermal synthesis method, employing flow chemistry to adjust reaction conditions dynamically during different stages of MOL growth. Fast nucleation is triggered initially to generate numerous nuclei, followed by a shift to slower growth rates, limiting further expansion and preventing the formation of amorphous structures. This approach effectively refines the lateral dimensions of nano-MOLs while maintaining monolayer integrity. The reduction in lateral dimensions has a direct effect on improving catalytic performance, demonstrating the potential for fine-tuned nanosized MOLs in advanced applications.</p>","PeriodicalId":229,"journal":{"name":"Small Methods","volume":" ","pages":"e2402078"},"PeriodicalIF":10.7,"publicationDate":"2025-02-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143424727","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Controllable Growth of Wafer-Scale Te<sub>1-x</sub>Se<sub>x</sub> Thin Films Based on Selenium Phase Change-Induced Strategy for Single-Pixel Imaging.","authors":"Xuemei Lu, Yulong Hao, Shijie Hao, Shiwei Zhang, Huan Zhou, Yunbo Lu, Jie Zhou, Yongqiang Yu, Guolin Hao","doi":"10.1002/smtd.202402014","DOIUrl":"https://doi.org/10.1002/smtd.202402014","url":null,"abstract":"<p><p>Recently, Te<sub>1-x</sub>Se<sub>x</sub> films have shown significant potential for infrared detection. However, the conventional deposition process of Te<sub>1-x</sub>Se<sub>x</sub> films typically requires a cooled substrate, which results in the formation of poorly crystallized materials. Achieving controlled synthesis of large-area Te<sub>1-x</sub>Se<sub>x</sub> films remains a major challenge. Herein, two-inch Te<sub>1-x</sub>Se<sub>x</sub> films is successfully prepared using a low-pressure chemical vapor deposition technique based on a selenium phase transition-induced strategy. The chemical compositions of Te<sub>1-x</sub>Se<sub>x</sub> (x ranging from 0 to 1) films can be precisely controlled by adjusting the molar ratio of Te and Se powders. The phase change of amorphous Se at elevated temperatures generates additional dangling bonds on its surface, which facilitates the incorporation of Te atoms into Se chains forming Te<sub>1-x</sub>Se<sub>x</sub> alloys. COMSOL simulations reveal that maintaining uniform concentration and temperature during the growth process is essential for the formation of Te<sub>1-x</sub>Se<sub>x</sub> films. Importantly, the Te<sub>0.4</sub>Se<sub>0.6</sub> film detector realizes high-performance near-infrared single-pixel imaging with a resolution of 128 × 128 pixels. This work has fabricated wafer-scale Te<sub>1-x</sub>Se<sub>x</sub> alloy thin films, which exhibit excellent properties, providing important experimental and theoretical support for exploring the applications in the fields of electronics, photonics, and optoelectronics.</p>","PeriodicalId":229,"journal":{"name":"Small Methods","volume":" ","pages":"e2402014"},"PeriodicalIF":10.7,"publicationDate":"2025-02-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143424722","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Battery Cathode Recycling With Superior Dissolution Kinetics by Laser Augmentation.","authors":"Zixu Wang, Xin Hu, Hao Zhang, Yaduo Song, Yonggang Yao, Yunhui Huang","doi":"10.1002/smtd.202401975","DOIUrl":"https://doi.org/10.1002/smtd.202401975","url":null,"abstract":"<p><p>The application of lithium-ion batteries challenges environmental sustainability and calls for efficient recycling toward circular economics. Hydrometallurgical recycling, despite being commercialized, still faces challenges such as harsh chemicals, high secondary waste generation, and low efficiencies. Intuitively, higher temperature leads to exponentially higher reaction kinetics (following Arrhenius's law), yet the dissolution temperature is limited to below 100 °C while heating the solution means more energy consumption. This study presents a laser-assisted wet leaching (Laser-WL) method that enables decoupled particle/solution temperatures, where the cathode particles are effectively heated by laser adsorption (30 W) to accelerate the dissolution kinetics (7-10 fold) while the solution remains cool for energy saving. Besides, physical laser ablation helps remove the robust solid electrolyte interface and cracks the particles to expose active materials, shortening the diffusion pathways and further enhancing the leaching kinetics. Therefore, Laser-WL can achieve an extraction rate of 95.6% in 15 min (traditional method >3 h). It reduced the consumption of concentrated HCl by 87%, and water consumption by 27%. The method is applicable to various cathode materials and works for weak acids, thus presenting a sustainable and economically viable solution for metal recycling.</p>","PeriodicalId":229,"journal":{"name":"Small Methods","volume":" ","pages":"e2401975"},"PeriodicalIF":10.7,"publicationDate":"2025-02-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143424649","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Enhancing Water Electrolysis Performance by Bubble Behavior Management.","authors":"Jiaxuan Qiu, Jiayi Yao, Zhe Feng, Baoyu Huang, Zhongzhong Luo, Longlu Wang","doi":"10.1002/smtd.202402105","DOIUrl":"https://doi.org/10.1002/smtd.202402105","url":null,"abstract":"<p><p>Electrocatalytic water splitting for hydrogen generation plays a crucial role in promoting the energy transition and achieving the goals of carbon neutrality. Nevertheless, in the context of water electrolysis, the generated bubbles have an adverse impact on energy consumption and mass transfer efficiency. To address this challenge, a variety of strategies are investigated to accelerate bubble detachment and transport. It is of utmost significance to summarize those strategies for facilitating the advancement of water electrolysis performance. In this review, a comprehensive account of strategies are presented for enhancing water electrolysis performance through bubble behavior management. First, the impact of the electrolyte on bubbles is discussed. Then, optimized interactions between bubbles and the electrode surface are introduced, which focus on reducing adhesion forces and implementing other forces. Next, dynamic bubbling of deformable catalysts is discussed, such as fern- and caterpillar-like catalysts. Following that, bubble-bubble interactions are investigated as bubble coalescence is proved to be beneficial for earlier bubble departure compared to buoyancy effect alone. Finally, outlooks are presented for future development of efficient bubble removal strategies for enhanced water electrolysis performance. The review aims to deepen the comprehension of bubbles interactions and stimulate the development of management strategies, thereby further enhancing the performance of water electrolysis.</p>","PeriodicalId":229,"journal":{"name":"Small Methods","volume":" ","pages":"e2402105"},"PeriodicalIF":10.7,"publicationDate":"2025-02-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143424723","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Small MethodsPub Date : 2025-02-14DOI: 10.1002/smtd.202402095
Xu Yang, Chenhong Yu, Bei Yang, Chu Jiang, Rui Gao, Weiying Li, Jianbang Wang, Tao Zhang, Huajie Liu, Dongsheng Liu
{"title":"DNA-Enabled Self-Resetting Electrochemical Sensor for microRNA Detection.","authors":"Xu Yang, Chenhong Yu, Bei Yang, Chu Jiang, Rui Gao, Weiying Li, Jianbang Wang, Tao Zhang, Huajie Liu, Dongsheng Liu","doi":"10.1002/smtd.202402095","DOIUrl":"https://doi.org/10.1002/smtd.202402095","url":null,"abstract":"<p><p>Nucleic acids, such as microRNA and circulating tumor DNA, are widely utilized potential biomarkers for early disease diagnosis. Electrochemical sensors with high sensitivity play a significant role in quantitative bioanalysis, however, target molecules during detection usually bind to probes and limit their reusability. Powered by DNA/RNA fuel and enzyme-based fuel consumption unit, dissipative DNA systems can perform periodic tasks in a self-resettable manner. Here, a self-resetting electrochemical sensor is reported for miRNA detection based on dissipative DNA networks. The target microRNA-21 (miRNA-21) invades the incumbent strand and activates the strand displacement process. Released ferrocene-modified strands bind to the probe on the electrode surface for accurate detection. The miRNA within RNA/DNA heteroduplex will then be digested by RNase H to free the incumbent strand which replaces the ferrocene strand and restores the probe to the initial state. It is found that the detection limit of this self-resetting electrochemical sensor is 0.35 pM for the third cycle. The self-resetting electrochemical sensor can not only achieve lower detection limits, and maintain repeatability and stability in complex matrices, but also reduce the detection cost of electrochemical sensors. It is envisioned that many real-life applications can be initiated such as analyzing various oligonucleotide biomarkers during early cancer diagnosis and bioanalysis.</p>","PeriodicalId":229,"journal":{"name":"Small Methods","volume":" ","pages":"e2402095"},"PeriodicalIF":10.7,"publicationDate":"2025-02-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143412632","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Small MethodsPub Date : 2025-02-14DOI: 10.1002/smtd.202401697
Chengcheng Zhu, Xi Liu, Chang Li, Yan Chen, Xinyu Guo, Dawei Luo, Wenhai Ji, Wenjun Deng, Rui Li
{"title":"Sodium-Deficient NASICON Na<sub>3+</sub> <sub>x</sub>VFe(PO<sub>4</sub>)<sub>3</sub> Cathode for High-Performance Sodium-Ion Batteries.","authors":"Chengcheng Zhu, Xi Liu, Chang Li, Yan Chen, Xinyu Guo, Dawei Luo, Wenhai Ji, Wenjun Deng, Rui Li","doi":"10.1002/smtd.202401697","DOIUrl":"https://doi.org/10.1002/smtd.202401697","url":null,"abstract":"<p><p>NASICON-type Na<sub>3</sub>V<sub>2</sub>(PO<sub>4</sub>)<sub>3</sub>(NVP) material possesses robust 3D structure and high sodium diffusivity, thus showcasing its immense potential in sodium-ion batteries (SIBs). However, considering the perspective of environmental conservation, it is imperative to substitute vanadium with elements that are both cost-effective and non-toxic in order to further enhance its application in SIBs. Herein, Fe is utilized to replace the V site in the sodium vanadium phosphate structure and successfully prepared a pure phase sodium-deficient NASICON (sodium superionic conductor) Na<sub>3.15</sub>VFe<sub>0.86</sub>(PO<sub>4</sub>)<sub>3</sub> (NVFP-650) cathode. It is found that the regulation of sintering temperature for Na<sub>3+</sub> <sub>x</sub>VFe(PO<sub>4</sub>)<sub>3</sub>(NVFP) material can effectively mitigate the formation of secondary phases and enhance the electrochemical properties of the resulting product. The sodium-deficient cathode shows enhanced electrochemical performance and sodium ion diffusion kinetics. It exhibits a high capacity of 102.8 mAh g<sup>-1</sup> at 0.1 C, and exhibits a high-capacity retention of 95.7% after 2000 cycles at 20 C. The energy storage mechanism and structural evolution are further investigated through SEM, TEM, XPS, and in situ XRD characterizations. The compositional modulation of sodium-deficient NVFP and the elucidation of its cycling mechanisms in this work would provide valuable insights for enhancing the performance of sodium energy storage systems.</p>","PeriodicalId":229,"journal":{"name":"Small Methods","volume":" ","pages":"e2401697"},"PeriodicalIF":10.7,"publicationDate":"2025-02-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143412634","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Small MethodsPub Date : 2025-02-14DOI: 10.1002/smtd.202401945
Fang Qi, Hong-Juan Feng, Jia-Yao Li, Yi Peng, Lin-Han Jiang, Ying-Ze Li, Le Zeng, Ling Huang
{"title":"Amino Acids-Enabled Fast-Restore of Triplet-Triplet Annihilation Upconversion Luminescence for Background-Free Sensing of Herbicides.","authors":"Fang Qi, Hong-Juan Feng, Jia-Yao Li, Yi Peng, Lin-Han Jiang, Ying-Ze Li, Le Zeng, Ling Huang","doi":"10.1002/smtd.202401945","DOIUrl":"https://doi.org/10.1002/smtd.202401945","url":null,"abstract":"<p><p>Overuse of herbicides poses a serious threat to ecosystems and human health; thus, the accurate determination of herbicide residue is very meaningful. Thanks to the advantage of no background fluorescence interference, the upconversion luminescence allows for reliable analysis of target molecules in complicated samples. Here, through screening of 20 natural amino acids, it is discovered that the photooxidation of methionine exhibited the fastest recovery rate of triplet-triplet annihilation upconversion (TTA-UC) luminescence via oxygen consumption, which is 400-fold faster compared to the well-known photooxidation of oleic acid. Furthermore, oxygen-resistant, small-size, red-to-blue TTA-UC nanoparticles with a record upconversion efficiency (7.2%, normalized to 100%) are prepared using hydrophobic butyl methionine as an oxygen scavenger. Surface negatively charged TTA-UC nanoparticles are able to selectively enrich positively charged paraquat on their surface. Accordingly, a photoinduced electron transfer process occurred between the triplet excited state of the photosensitizer and the electron-deficient paraquat, quenching the upconversion luminescence. Relying on this principle, TTA-UC-based paraquat sensing is achieved with a fast response (less than 1 s), high selectivity, and a low limit of detection (1.54 µg mL<sup>-1</sup>). Further, the TTA-UC nanoparticles are utilized to implement paraquat analysis in lake water without sample pretreatment.</p>","PeriodicalId":229,"journal":{"name":"Small Methods","volume":" ","pages":"e2401945"},"PeriodicalIF":10.7,"publicationDate":"2025-02-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143412631","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"The Direct Air Synthesis of Hydrogen Peroxide Induced by The Giant Built-In Electric Field of Trz-CN.","authors":"Haoyang Ma, Wenjun Jiang, Yinhua Ma, Yulin Song, Liubin Pei, Hui Ban, Su Zhan, Feng Zhou","doi":"10.1002/smtd.202401347","DOIUrl":"https://doi.org/10.1002/smtd.202401347","url":null,"abstract":"<p><p>Graphitic carbon nitride (C<sub>3</sub>N<sub>4</sub>) has been identified as an optimal material for hydrogen peroxide (H<sub>2</sub>O<sub>2</sub>) photosynthesis, although its utility is hampered by a high photocarrier recombination rate. Herein, a novel carbon nitride material with a giant built-in electric field (BEF), Trz-CN, is synthesized through a hydrothermal-calcination tandem strategy. The giant BEF (4.8-fold) induced by the large dipole moment facilitated the efficient separation and directional migration of photogenerated carriers. Trz-CN exhibited an H<sub>2</sub>O<sub>2</sub> production rate of 569.9 µmol·g<sup>-1</sup>·h<sup>-1</sup> using O<sub>2</sub> as feedstock under visible light (λ > 420 nm), marking an impressive 11.2-fold enhancement compared to bulk C<sub>3</sub>N<sub>4</sub>. Utilizing air instead of pure O<sub>2</sub> as feedstock resulted in a trivial 1.6% decrease in the H<sub>2</sub>O<sub>2</sub> generation by Trz-CN while maintaining a substantial production rate of 560.6 µmol·g<sup>-1</sup>·h<sup>-1</sup>. Notably, Trz-CN showcased a sterilization rate of 99.9% against Escherichia coli (E. coli) in natural seawater. Density functional theory (DFT) calculations revealed that incorporating a nitrogen-rich skeleton into the C<sub>3</sub>N<sub>4</sub> enhanced its oxygen adsorption capacity and lowered the energy barrier for H<sub>2</sub>O<sub>2</sub> formation. This leads to enhanced photocatalytic performance for H<sub>2</sub>O<sub>2</sub> generation under ambient air conditions. Trz-CN provides a new exploratory idea for direct air synthesis of H<sub>2</sub>O<sub>2</sub> and ballast water treatment.</p>","PeriodicalId":229,"journal":{"name":"Small Methods","volume":" ","pages":"e2401347"},"PeriodicalIF":10.7,"publicationDate":"2025-02-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143412635","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Facile Growth of h-BN Films by Using Surface-Activated h-BN Powders as Precursors.","authors":"Chen Chen, Qiang Wang, Zongyuan Zhang, Zhibo Liu, Chuan Xu, Wencai Ren","doi":"10.1002/smtd.202401422","DOIUrl":"https://doi.org/10.1002/smtd.202401422","url":null,"abstract":"<p><p>Atomically thick hexagonal boron nitride (h-BN) films have gained increasing interest, such as nanoelectronics and protection coatings. Chemical vapor deposition (CVD) has been proven to be an efficient method for synthesizing h-BN thin films, but its precursors are still limited. Here, it is reported that a novel and easily available precursor, surface-activated h-BN (As-hBN), with NH<sub>3</sub>/N<sub>2</sub> as an additional nitrogen source is used for CVD growth of monolayer h-BN films on the Cu foils. The as-grown h-BN films can significantly enhance the anti-oxidation ability of copper. Molecular dynamics simulations reveal that the reactivity of the As-hBN precursors is attributed to the decomposition of unstable BO<sub>3</sub> and O-terminal edges on the surface under H<sub>2</sub> atmosphere. This method provides a more reliable approach for fabricating h-BN films.</p>","PeriodicalId":229,"journal":{"name":"Small Methods","volume":" ","pages":"e2401422"},"PeriodicalIF":10.7,"publicationDate":"2025-02-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143412633","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}