{"title":"Corrosion and metallographic insights into lead-based artefacts from Khirbet Yajuz, Jordan","authors":"Ahmad N. Abu-Baker","doi":"10.1016/j.nimb.2025.165754","DOIUrl":"10.1016/j.nimb.2025.165754","url":null,"abstract":"<div><div>This study analysed three lead-based archaeological artefacts from Khirbet Yajuz, Jordan: a hook, a steelyard weight, and a stone pendant with a lead-alloy bail. X-ray diffraction identified lead corrosion products, including litharge, cerussite, hydrocerussite, phosphohedyphane, and cotunnite, across the three artefacts, along with the tin corrosion product cassiterite in the pendant’s bail and soapstone-associated minerals in the pendant’s stone. SEM-EDX revealed the hook’s pure lead composition, the weight’s low-tin pewter, and the pendant’s bail as a near-eutectic lead–tin alloy. EDX mapping showed elemental distribution across corrosion layers and original materials. Metallographic analysis highlighted α-Pb dendrites, recrystallized lead-rich α-crystals, and tin-rich β-grains. These findings provide insights into corrosion mechanisms, burial impacts, and manufacturing techniques.</div></div>","PeriodicalId":19380,"journal":{"name":"Nuclear Instruments & Methods in Physics Research Section B-beam Interactions With Materials and Atoms","volume":"565 ","pages":"Article 165754"},"PeriodicalIF":1.4,"publicationDate":"2025-05-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144138629","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Kazuki Komiya , Yoshikazu Teranishi , Hidehiko Yamaoka , Shuichi Date , Ming Yang
{"title":"Development of imprint mold with F+ ion implantation for detachability","authors":"Kazuki Komiya , Yoshikazu Teranishi , Hidehiko Yamaoka , Shuichi Date , Ming Yang","doi":"10.1016/j.nimb.2025.165753","DOIUrl":"10.1016/j.nimb.2025.165753","url":null,"abstract":"<div><div>In this study, F<sup>+</sup> ions were implanted into SiO<em>x</em> films using an accelerator to improve the peelability of nanoimprints. Various properties, including wettability, surface roughness, lateral friction force, and surface hardness, were evaluated. The results indicated that increasing the implantation dose of F<sup>+</sup> ions improved the transverse friction coefficient but decreased the surface hardness. It was also determined that an implantation dose of 1.0 × 10<sup>14</sup> ions/cm<sup>2</sup> was optimal for hydrophobicity because of an increased surface roughness.</div></div>","PeriodicalId":19380,"journal":{"name":"Nuclear Instruments & Methods in Physics Research Section B-beam Interactions With Materials and Atoms","volume":"565 ","pages":"Article 165753"},"PeriodicalIF":1.4,"publicationDate":"2025-05-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144123777","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Robert Koch , Stefanie Eckner , Marcel Gerold , Shavkat Akhmadaliev , Michael Rüb
{"title":"Novel energy-filtered implantation technique for field stop formation in silicon power devices","authors":"Robert Koch , Stefanie Eckner , Marcel Gerold , Shavkat Akhmadaliev , Michael Rüb","doi":"10.1016/j.nimb.2025.165715","DOIUrl":"10.1016/j.nimb.2025.165715","url":null,"abstract":"<div><div>Insulated Gate Bipolar Transistors (IGBTs) power devices require high blocking capability, low on-resistance as well as adaptable switching behaviour. The technique presented in this work aims to realize continuous deep (<span><math><mrow><mo>></mo><mn>40</mn><mspace></mspace><mi>μ</mi><mi>m</mi></mrow></math></span>) n-type profiles as field stop structures in high voltage silicon IGBTs (1200 V) to adjust the switching capability. Hydrogen-related donor (HD) defect complexes perform as n-type dopants in single crystalline silicon. Up to now, these IGBT field stop profiles are generated using multiple high energy (up to <span><math><mrow><mn>2</mn><mspace></mspace><mi>MeV</mi></mrow></math></span>) implantation steps. In contrast, we achieve continuous deep HD profiles in a single implantation step by inserting a micro-patterned silicon membrane (energy filter) into the primary ion beam at an energy of <span><math><mrow><mn>2</mn><mo>.</mo><mn>5</mn><mspace></mspace><mi>MeV</mi></mrow></math></span> to provide a beam with a broad customized energy distribution. In this work, we investigate how filter structure, implanted fluence <span><math><mi>Φ</mi></math></span> (from <span><math><mrow><mn>1</mn><msup><mrow><mn>0</mn></mrow><mrow><mn>13</mn></mrow></msup></mrow></math></span> cm<sup>−2</sup> to <span><math><mrow><mn>5</mn><mo>×</mo><mn>1</mn><msup><mrow><mn>0</mn></mrow><mrow><mn>15</mn></mrow></msup></mrow></math></span> cm<sup>−2</sup>) and annealing conditions affect the depth distribution of HD defect complexes. We found that the electrically active dose divided by the implanted fluence before the energy filter, depends on the pattern type of the membrane (long grooves or squares), the implanted fluence and the annealing hold temperature (<span><math><mrow><mn>320</mn><msup><mrow><mspace></mspace></mrow><mrow><mo>∘</mo></mrow></msup></mrow></math></span>C to <span><math><mrow><mn>420</mn><msup><mrow><mspace></mspace></mrow><mrow><mo>∘</mo></mrow></msup></mrow></math></span>C).</div></div>","PeriodicalId":19380,"journal":{"name":"Nuclear Instruments & Methods in Physics Research Section B-beam Interactions With Materials and Atoms","volume":"565 ","pages":"Article 165715"},"PeriodicalIF":1.4,"publicationDate":"2025-05-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144099221","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Assessing the L X ray satellite emissions of zirconium through wavelength Dispersion X ray fluorescence (WDXRF) analysis","authors":"Penta Sowjanya , Balireddy Vasundhara , Dasari Kishore Babu , Suresh Maddila , Ponnada Tejeswara Rao , Ram Kumar Nodagala","doi":"10.1016/j.nimb.2025.165740","DOIUrl":"10.1016/j.nimb.2025.165740","url":null,"abstract":"<div><div>The technique known as Electron Probe Microanalysis (EPMA) is used to precisely identify the elemental composition of small regions in solid materials. A concentrated electron beam is directed onto the sample, producing distinctive X-rays in the process. After that, the elements’ presence and concentration in the material are ascertained by analyzing these X-rays. For this analyzing purpose, Wavelength<!--> <!-->dispersive X-ray fluorescence (WDXRF) is used because of its high accuracy compared to Energy dispersive X-ray Fluorescence (EDXRF). In this work zirconium foil is analyzed and the experimental values to the theoretical energies of these satellite lines was confirmed using the literature by using WDXRF. And using two crystal changers, Poly Ethylene Terephthalate (PET) and Extended selection of Germanium Crystal (XS-Ge), WDXRF was used to compare the theoretical values from X-Ray Data to the experimental values from the WDXRF Technique, and found the transitions of L<sub>2</sub>O<sub>1</sub> and L<sub>3</sub>O<sub>1</sub> experimental values which are not found theoretically, chemical effect, such as energy shift, intensity ratio, and transition energy corresponding to emission X-ray intensity and their respective functions of zirconium foil.</div></div>","PeriodicalId":19380,"journal":{"name":"Nuclear Instruments & Methods in Physics Research Section B-beam Interactions With Materials and Atoms","volume":"565 ","pages":"Article 165740"},"PeriodicalIF":1.4,"publicationDate":"2025-05-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144090236","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Marcus Christl, Habacuc Perez-Tribouillier, Philip Gautschi
{"title":"Results from the Zurich sea water (ZSW) intercomparison study for U- and Pu-isotopes","authors":"Marcus Christl, Habacuc Perez-Tribouillier, Philip Gautschi","doi":"10.1016/j.nimb.2025.165750","DOIUrl":"10.1016/j.nimb.2025.165750","url":null,"abstract":"<div><div>Approximately 350L of sea water samples were collected to prepare a large volume (Zurich Sea Water, ZSW) intercomparison sample for <sup>236</sup>U and other actinides. Here we report the results of the intercomparison study for U- and Pu-isotopes. ZSW was processed in six different chemistry labs and measured on five AMS systems and one MC-ICP-MS system, respectively. The analysis of the reported U-isotopic data shows that the scatter, indicated by the one sigma uncertainty for a single measurement, of the <sup>236</sup>U/<sup>238</sup>U ratios and the <sup>236, 238</sup>U-concentrations is 5 % and 3 %, respectively. A Chi-squared analysis shows that the external error (lab-scatter) is 1–2 % and 3 % for the <sup>236, 238</sup>U-concentrations and the <sup>236</sup>U/<sup>238</sup>U ratios, respectively.</div><div>The fact that ZSW has been characterized by many different (A)MS labs makes it a valuable internal standard for quality control for the analysis of anthropogenic U- and Pu-isotopes in seawater.</div></div>","PeriodicalId":19380,"journal":{"name":"Nuclear Instruments & Methods in Physics Research Section B-beam Interactions With Materials and Atoms","volume":"565 ","pages":"Article 165750"},"PeriodicalIF":1.4,"publicationDate":"2025-05-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144083933","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Marek Zmeškal , Petr Burian , Michal Košťál , Tomáš Czakoj , Tomáš Peltan , Jan Šimon , Pavel Broulím , Ondřej Růžička , Šimon Vadják
{"title":"Energy and profile of the proton beam of the IBA Cyclone 18/9","authors":"Marek Zmeškal , Petr Burian , Michal Košťál , Tomáš Czakoj , Tomáš Peltan , Jan Šimon , Pavel Broulím , Ondřej Růžička , Šimon Vadják","doi":"10.1016/j.nimb.2025.165710","DOIUrl":"10.1016/j.nimb.2025.165710","url":null,"abstract":"<div><div>The characteristics of the proton beam produced by the IBA Cyclone 18/9 medical cyclotron were investigated, focusing on its energy and profile. The proton beam energy was measured as <span><math><mrow><mn>18</mn><mo>.</mo><mn>25</mn><mo>±</mo><mn>0</mn><mo>.</mo><mn>25</mn></mrow></math></span> <!--> <!-->MeV using activation foil detectors. The beam profile was characterized using the Timepix3 based detector, revealing a Gaussian distribution with consistent widths and slight asymmetry in the horizontal plane. This study presents a straightforward methodology for evaluating cyclotron beam parameters using activation foils and pixel detectors, providing a tool for optimizing target design and expanding the applications of medical cyclotrons beyond radiopharmaceutical production.</div></div>","PeriodicalId":19380,"journal":{"name":"Nuclear Instruments & Methods in Physics Research Section B-beam Interactions With Materials and Atoms","volume":"565 ","pages":"Article 165710"},"PeriodicalIF":1.4,"publicationDate":"2025-05-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144090235","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Kristina L. Small , Deepa Angal-Kalinin , James K. Jones , Roger M. Jones
{"title":"VHEE facilities in Europe with the potential for FLASH dose irradiation: Conspectus and dose rate parameterisation","authors":"Kristina L. Small , Deepa Angal-Kalinin , James K. Jones , Roger M. Jones","doi":"10.1016/j.nimb.2025.165752","DOIUrl":"10.1016/j.nimb.2025.165752","url":null,"abstract":"<div><div>Very High Energy Electrons (VHEE) are gaining significant interest in combination with FLASH radiotherapy as a potential cancer treatment with potential reduction in side effects. This study reviews European VHEE facilities, their FLASH capabilities and applications to radiobiological research, with study objectives:<ul><li><span>1.</span><span><div>Determining FLASH capabilities through Monte Carlo beam modelling and fitting to analytical functions.</div></span></li><li><span>2.</span><span><div>Assessing VHEE facility infrastructure suitability for radiobiological research.</div></span></li></ul>Parameter variation studies were performed to determine dose dependency on beam dimension and source-to-surface distance (SSD). The dose rate was calculated from surface dose, linearly scaled based on the beamline. Empirical dose rate functions were developed, with an average discrepancy < 3 % between simulation and fit data. Dose rates were compared to the FLASH threshold of 40 Gy/s.</div><div>Further parameter and infrastructure considerations provided an overview of each facility’s radiobiological experiment capabilities, providing researchers with a useful resource in designing and planning of future VHEE-FLASH experiments.</div></div>","PeriodicalId":19380,"journal":{"name":"Nuclear Instruments & Methods in Physics Research Section B-beam Interactions With Materials and Atoms","volume":"565 ","pages":"Article 165752"},"PeriodicalIF":1.4,"publicationDate":"2025-05-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144072531","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"NXSIM: A normalized XRF standardless iterative simulation method for qualitative and quantitative XRF analysis via MCNP","authors":"K. Yavaş, O. Toker, Ö. Akcali, O. İçelli","doi":"10.1016/j.nimb.2025.165739","DOIUrl":"10.1016/j.nimb.2025.165739","url":null,"abstract":"<div><div>A normalized XRF standardless iterative simulation method (NXSIM) is proposed. Various methods are available to perform quantitative analysis with the XRF method. Many of these methods have laborious and costly processes that require sample preparations, specific reference materials, and repeated measurements. For such reasons, researchers continue to search for methods that provide more accurate and faster results. The main goals of this study are to obtain much faster results with acceptable accuracy by eliminating the need for repeated experimental measurements and reference samples. In this study, XRF spectrometry simulations were carried out with the scattering geometry designed in the MCNP 6.2 code system. The obtained results were used to perform quantitative analysis for experimentally prepared samples. After six samples with different element content and composition were prepared by the press pellet method, XRF spectra were obtained experimentally. Simulations were run with random element weight percentages using the elements in the sample. The elemental compositions of the samples were determined by the iteration method developed from the simulation results and experimental results. According to the results obtained, it has been demonstrated that XRF quantitative analysis can be performed by NXSIM with acceptable precision and accuracy.</div></div>","PeriodicalId":19380,"journal":{"name":"Nuclear Instruments & Methods in Physics Research Section B-beam Interactions With Materials and Atoms","volume":"565 ","pages":"Article 165739"},"PeriodicalIF":1.4,"publicationDate":"2025-05-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144071148","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Ahsan Ejaz , Limin Zhang , Zhiqiang Wang , Muhammad Bilal , Xuan Meng , Tong Liu , Madiha Shadab , Tieshan Wang
{"title":"Y2O3 and Y2Ti2O7 nanoparticles stability in oxide dispersion strengthened steels under hydrogen irradiation at elevated temperature","authors":"Ahsan Ejaz , Limin Zhang , Zhiqiang Wang , Muhammad Bilal , Xuan Meng , Tong Liu , Madiha Shadab , Tieshan Wang","doi":"10.1016/j.nimb.2025.165741","DOIUrl":"10.1016/j.nimb.2025.165741","url":null,"abstract":"<div><div>Oxide dispersion-strengthened steels with Y<sub>2</sub>O<sub>3</sub> and Y<sub>2</sub>Ti<sub>2</sub>O<sub>7</sub> nanoparticles (NPs) and Chinese low-activation ferritic/martensitic steel (CLF) samples were fabricated by the mechanical alloying method and sequentially irradiated at 550 °C with 50 keV H<sub>2</sub><sup>+</sup> ions to various fluences. The hydrogen-bubble density and average bubble size are significantly higher in CLF steel. After irradiation, the size of NPs in YTO and YO steel reduced to ∼ 7 nm and ∼ 15 nm; finer NPs in YTO steel enhanced the resistance to the irradiation-induced defects. The absence of NPs in CLF causes the formation of dislocation networks. Y<sub>2</sub>Ti<sub>2</sub>O<sub>7</sub> NPs phases in YTO steel are highly stable and show semi-coherent orientation, while YAlO<sub>3</sub> NPs phases show incoherent orientation with the matrix. Y<sub>2</sub>Ti<sub>2</sub>O<sub>7</sub> NPs resist defect formation by reducing the internal stresses and obstructing dislocation networks. This study suggests that introducing Y<sub>2</sub>Ti<sub>2</sub>O<sub>7</sub> NP into ODS steel presents a promising approach to improving the resistance towards irradiation damage.</div></div>","PeriodicalId":19380,"journal":{"name":"Nuclear Instruments & Methods in Physics Research Section B-beam Interactions With Materials and Atoms","volume":"565 ","pages":"Article 165741"},"PeriodicalIF":1.4,"publicationDate":"2025-05-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143942727","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Oscar Marchhart , Markus Schiffer , Martin Martschini , Gereon Weingarten , Peter Steier , Elisa Linnartz , Erik Strub , Tibor Dunai , Dennis Mücher , Robin Golser
{"title":"First performance tests of the new advanced radiofrequency quadrupole for ALIS at the test bench setup at VERA","authors":"Oscar Marchhart , Markus Schiffer , Martin Martschini , Gereon Weingarten , Peter Steier , Elisa Linnartz , Erik Strub , Tibor Dunai , Dennis Mücher , Robin Golser","doi":"10.1016/j.nimb.2025.165751","DOIUrl":"10.1016/j.nimb.2025.165751","url":null,"abstract":"<div><div>A new advanced radiofrequency quadrupole (RFQ) ion cooler for accelerator mass spectrometry has been developed for the Anion Laser Isobar Separator (ALIS) at CologneAMS. Based on the Ion-Laser Interaction Mass Spectrometry (ILIAMS) setup at the Vienna Environmental Research Accelerator (VERA), it features new guiding electrodes and ion optics trying to solve challenges in decelerating and trapping intense heavy molecular ion beams, such as SrF<sub>3</sub><sup>−</sup>. Initial tests with <sup>27</sup>AlO<sup>−</sup> and <sup>63</sup>Cu<sup>−</sup> show ∼ 30% transmission and millisecond ion residence times, demonstrating that the cooler is functioning properly. While promising, further optimizations are needed to fully achieve the desired efficiency and stability.</div></div>","PeriodicalId":19380,"journal":{"name":"Nuclear Instruments & Methods in Physics Research Section B-beam Interactions With Materials and Atoms","volume":"565 ","pages":"Article 165751"},"PeriodicalIF":1.4,"publicationDate":"2025-05-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143942726","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}