Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes最新文献

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Biophoton emission-based approach of the effects of systemic insecticides on the survival of Eurydema ventralis Kolenati, 1846 (Hemiptera: Pentatomidae) and on the photosynthetic activity of oilseed rape. 基于生物光子发射的系统杀虫剂对 Eurydema ventralis Kolenati, 1846 (Hemiptera: Pentatomidae) 存活率和油菜光合作用活性影响的研究方法。
IF 2 4区 农林科学
Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes Pub Date : 2024-01-01 Epub Date: 2024-05-28 DOI: 10.1080/03601234.2024.2358632
Bálint Gerbovits, Sándor Keszthelyi, Ildikó Jócsák
{"title":"Biophoton emission-based approach of the effects of systemic insecticides on the survival of <i>Eurydema ventralis</i> Kolenati, 1846 (Hemiptera: Pentatomidae) and on the photosynthetic activity of oilseed rape.","authors":"Bálint Gerbovits, Sándor Keszthelyi, Ildikó Jócsák","doi":"10.1080/03601234.2024.2358632","DOIUrl":"10.1080/03601234.2024.2358632","url":null,"abstract":"<p><p>The choice of effective crop protection technologies is a key factors in the economical production of oilseed rape. Insecticides belonging to the group of active substances butenolides and diamides are active substances available as seed treatments in oilseed rape and promising control tools in the crop protection technologies. Our laboratory experiment demonstrated that the experimental insecticides flupyradifurone and cyantraniliprole are both effective against <i>Eurydema ventralis</i> (Hemiptera: Pentatomidae) when used as a seed and in-crop treatments, but there is a fundamental difference in their insect mortality inducing effects. Flupyradifurone was found to have a total mortality 96 h after application based on basipetal translocation. In the case of cyantraniliprole, the insecticidal effect of the same treatment was 27% less. The experiment showed that the acropetal translocation of the tested active substances after seed treatment did not induce efficacy comparable to that of the basipetal translocation. The study of the biophoton emission of the plants demonstrated a verifiable correlation between the different application methods of the insecticides and the photon emission intensity per unit plant surface area. In conclusion, the systematic insecticides tested, in addition to having the expected insecticidal effect, interfere with plant life processes by enhancing photosynthetic activity.</p>","PeriodicalId":15720,"journal":{"name":"Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes","volume":" ","pages":"417-424"},"PeriodicalIF":2.0,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141158315","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Occurrence, distribution and health risk assessment of quinolone residues in cultured fish in southeast China. 中国东南部养殖鱼类中喹诺酮类药物残留的发生、分布和健康风险评估。
IF 1.4 4区 农林科学
Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes Pub Date : 2024-01-01 Epub Date: 2024-10-25 DOI: 10.1080/03601234.2024.2418719
Rong Bao, Yan Yang, Hongjing Chen, Yuxiang Li
{"title":"Occurrence, distribution and health risk assessment of quinolone residues in cultured fish in southeast China.","authors":"Rong Bao, Yan Yang, Hongjing Chen, Yuxiang Li","doi":"10.1080/03601234.2024.2418719","DOIUrl":"10.1080/03601234.2024.2418719","url":null,"abstract":"<p><p>Quinolone antibiotics are widely utilized in aquaculture, but little is known about the health effects of their residues. This study used UPLC-MS/MS to analyze the distribution of 11 quinolone antibiotics in cultured fish sold in a coastal city in southeast China - Fujian Province and to assess their health risks. The study found 35.77% of 260 cultured fish samples detected quinolones, with three exceeding the MRL and one containing the banned drug ofloxacin. Of the 11 quinolones tested, three were found in cultured fish, with enrofloxacin at up to 246.0 μg kg<sup>-1</sup>, followed by ciprofloxacin and ofloxacin. The distribution of antibiotic detection rates showed no significant differences across regions or time periods; however, notable variations were observed among different fish species. The dietary exposure assessment revealed that consuming cultured fish does not pose a health risk to residents. Nevertheless, there are still instances that exceed regulatory limits. Therefore, routine monitoring and risk assessment are essential for enhancing regulatory measures and protecting public health.</p>","PeriodicalId":15720,"journal":{"name":"Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes","volume":" ","pages":"714-724"},"PeriodicalIF":1.4,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142501645","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Dissipation and residues of imidacloprid in amaranth under greenhouse and open field cultivations. 温室和露地栽培苋菜中吡虫啉的消散和残留。
IF 2 4区 农林科学
Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes Pub Date : 2024-01-01 Epub Date: 2024-05-24 DOI: 10.1080/03601234.2024.2356991
Yidong Guan, Feifei Huang, Chunwei Ma, Jianlin Fan, Guohui Hao
{"title":"Dissipation and residues of imidacloprid in amaranth under greenhouse and open field cultivations.","authors":"Yidong Guan, Feifei Huang, Chunwei Ma, Jianlin Fan, Guohui Hao","doi":"10.1080/03601234.2024.2356991","DOIUrl":"10.1080/03601234.2024.2356991","url":null,"abstract":"<p><p>Despite the extensive exposure to imidacloprid residues in food plants, there has been little research on imidacloprid residues in amaranth. The dissipation trend and residue behavior of imidacloprid were evaluated to provide guidelines for imidacloprid application on amaranth under open field and greenhouse. The dissipation rate of imidacloprid in amaranth conformed to the first-order kinetic equation, and the half-lives of imidacloprid in amaranth ranged from 0.29 days in open field to 1.29 days in the greenhouse. After 7 and 14 days from the application of imidacloprid (pesticide dosage, 45 or 67.5 g a.i./ha), the amaranth under the open field and greenhouse growth could be consumed safely with average residues of 0.19 and 0.38 mg/kg, respectively. This result demonstrated that the cultivation has the dominant influence on imidacloprid residue, and the residue of imidacloprid in amaranth planting on open field was much lower than that in the greenhouse, indicating a significant difference in the pesticide residues between the two cultivations with a p-value less than 0.05.</p>","PeriodicalId":15720,"journal":{"name":"Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes","volume":" ","pages":"390-398"},"PeriodicalIF":2.0,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141093209","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Automated, cryogen-free headspace-trap with gas chromatography-mass spectrometry analysis of ethylene oxide and 2-chloroethanol as residual fumigants in foods. 利用气相色谱-质谱联用技术对食品中残留的熏蒸剂环氧乙烷和 2-氯乙醇进行自动无低温顶空阱分析。
IF 2 4区 农林科学
Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes Pub Date : 2024-01-01 Epub Date: 2024-01-05 DOI: 10.1080/03601234.2023.2298169
Lucy Hearn, Rachael Szafnauer, Rebecca Cole, Bob Green, Jan Peter Mayser, Vikas Tomar, Kaushik Banerjee, Priyesh Amin
{"title":"Automated, cryogen-free headspace-trap with gas chromatography-mass spectrometry analysis of ethylene oxide and 2-chloroethanol as residual fumigants in foods.","authors":"Lucy Hearn, Rachael Szafnauer, Rebecca Cole, Bob Green, Jan Peter Mayser, Vikas Tomar, Kaushik Banerjee, Priyesh Amin","doi":"10.1080/03601234.2023.2298169","DOIUrl":"10.1080/03601234.2023.2298169","url":null,"abstract":"<p><p>Ethylene oxide (EtO), although banned for use, is still being detected in foodstuffs that have been fumigated to eradicate pests during storage and transport. Residual levels over the European Union's (EU) maximum residue limit (MRL) pose severe health concerns. Recent detection of EtO and its by-product 2-chloroethanol (2-CE) at alarming levels have led to product recalls throughout the EU. Here, a simple, automated headspace (HS)-trap method for the simultaneous determination of EtO and its derivative 2-CE by gas chromatography-mass spectrometry (GC-MS) at the required MRL of ≤ 0.05 mg/kg has been implemented. Syringe-based HS combined with backflushed trapping technology provided enrichment of multiple extractions from the same sample vial (known as multi-step enrichment or MSE®) to increase sensitivity for EtO and 2-CE analysis by GC-MS using single-ion-monitoring (SIM) mode. Method detection limits (MDLs) of 0.00059 mg/kg and 0.00219 mg/kg for EtO and 2-CE, respectively, were obtained without the need for manual handling, solvent extraction or derivatization methods. Recoveries were shown to average (<i>n</i> = 5) at 98% and 107% for EtO and 2-CE, respectively, and the reproducibility was <10% for both compounds.</p>","PeriodicalId":15720,"journal":{"name":"Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes","volume":" ","pages":"81-87"},"PeriodicalIF":2.0,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139097997","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Mycoremediation of the novel fungicide ametoctradin by different agricultural soils and accelerated degradation utilizing selected fungal strains. 不同农业土壤对新型杀菌剂阿米曲丁的菌核修复作用以及利用精选真菌菌株加速降解。
IF 2 4区 农林科学
Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes Pub Date : 2024-01-01 Epub Date: 2024-03-27 DOI: 10.1080/03601234.2024.2331951
Sara Majid, Khuram Shahzad Ahmad, Ghulam Abbas Ashraf, Wahidah H Al-Qahtani
{"title":"Mycoremediation of the novel fungicide ametoctradin by different agricultural soils and accelerated degradation utilizing selected fungal strains.","authors":"Sara Majid, Khuram Shahzad Ahmad, Ghulam Abbas Ashraf, Wahidah H Al-Qahtani","doi":"10.1080/03601234.2024.2331951","DOIUrl":"10.1080/03601234.2024.2331951","url":null,"abstract":"<p><p>Accelerating safety assessments for novel agrochemicals is imperative, advocating for <i>in vitro</i> setups to present pesticide biodegradation by soil microbiota before field studies. This approach enables metabolic profile generation in a controlled laboratory environment eliminating extrinsic factors. In the current study, ten different soil samples were utilized to check their capability to degrade Ametoctradin by their microbiota. Furthermore, five different fungal strains (<i>Aspergillus niger</i>, <i>Aspergillus flavus</i>, <i>Aspergillus fumigatus, Lasiodiplodia theobromae</i>, and <i>Penicillium chrysogenum</i>) were utilized to degrade Ametoctradin in aqueous media. A degradation pathway was established using the metabolic patterns created during the biodegradation of Ametoctradin. In contrast to 47% degradation (T<sub>1/2</sub> of 34 days) when Ametoctradin was left in the soil samples, the fungal strain <i>Aspergillus fumigatus</i> demonstrated 71% degradation of parent Ametoctradin with a half-life (T<sub>1/2</sub>) of 16 days. In conclusion, soil rich in microorganisms effectively cleans Ametoctradin-contaminated areas while Fungi have also been shown to be an effective, affordable, and promising way to remove Ametoctradin from the environment.</p>","PeriodicalId":15720,"journal":{"name":"Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes","volume":" ","pages":"233-247"},"PeriodicalIF":2.0,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140293699","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Microbiome analyses of poultry feeds: Part I. Comparison of five different DNA extraction methods. 家禽饲料微生物组分析:第一部分:五种不同 DNA 提取方法的比较。
IF 2 4区 农林科学
Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes Pub Date : 2024-01-01 Epub Date: 2024-05-23 DOI: 10.1080/03601234.2024.2353002
E G Olson, D K Dittoe, A C Micciche, D A Stock, P M Rubinelli, M J Rothrock, S C Ricke
{"title":"Microbiome analyses of poultry feeds: Part I. Comparison of five different DNA extraction methods.","authors":"E G Olson, D K Dittoe, A C Micciche, D A Stock, P M Rubinelli, M J Rothrock, S C Ricke","doi":"10.1080/03601234.2024.2353002","DOIUrl":"10.1080/03601234.2024.2353002","url":null,"abstract":"<p><p>Given extensive variability in feed composition, the absence of a dedicated DNA extraction kit for poultry feed underscores the need for an optimized extraction technique for reliable downstream sequencing analyses. This study investigates the impact of five DNA extraction techniques: Qiagen QIAamp DNA Stool Mini Kit (Qiagen), modified Qiagen with Lysing Matrix B (MQ), modified Qiagen with celite purification (MQC), polyethylene glycol (PEG), and 1-Day Direct. Genomic DNA amplification and Illumina MiSeq sequencing were conducted. QIIME2-2021.4 facilitated data analysis, revealing significant diversity and compositional differences influenced by extraction methods. Qiagen exhibited lower evenness and richness compared to other methods. 1-Day Direct and PEG enhanced bacterial diversities by employing bead beating and lysozyme. Despite similar taxonomic resolution, the Qiagen kit provides a rapid, consistent method for assessing poultry feed microbiomes. Modified techniques (MQ and MQC) improve DNA purification, reducing bias in commercial poultry feed samples. PEG and 1-Day Direct methods were effective but may require standardization. Overall, this study underscores the importance of optimized extraction techniques in poultry feed analysis, with potential implications for future standardization of effective methods.</p>","PeriodicalId":15720,"journal":{"name":"Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes","volume":" ","pages":"378-389"},"PeriodicalIF":2.0,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141081725","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Root exudation of glyphosate in Eucalyptus urophylla S.T. Blake. 草甘膦在 Eucalyptus urophylla S.T. Blake 根部的渗出。
IF 1.4 4区 农林科学
Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes Pub Date : 2024-01-01 Epub Date: 2024-11-06 DOI: 10.1080/03601234.2024.2422719
Rodrigo Eduardo Barros, Matheus Mendes Reis, Leonardo David Tuffi Santos, João Paulo Fernandes Tiago, Érika Manuela Gonçalves Lopes, Luan Mateus Silva Donato
{"title":"Root exudation of glyphosate in <i>Eucalyptus urophylla</i> S.T. Blake.","authors":"Rodrigo Eduardo Barros, Matheus Mendes Reis, Leonardo David Tuffi Santos, João Paulo Fernandes Tiago, Érika Manuela Gonçalves Lopes, Luan Mateus Silva Donato","doi":"10.1080/03601234.2024.2422719","DOIUrl":"10.1080/03601234.2024.2422719","url":null,"abstract":"<p><p>Glyphosate stands out in the eucalyptus management, which makes it essential to know its behavior, its effects on the plant, and possible environmental impacts. This study aimed to identify and quantify the root exudation of glyphosate and aminomethylphosphonic acid (AMPA) by <i>Eucalyptus urophylla</i> with chromatographic and biological methods. The five glyphosate doses were tested (0, 360, 720, 1080 and 1440 g a.e ha<sup>-1</sup>) on <i>E. urophylla</i> plants. The physiological and intoxication evaluations were performed after herbicide application. Water samples remaining from the pots were used for chemical quantification of root exudation of glyphosate and AMPA in high-performance liquid chromatography. <i>Cucurbita pepo</i> plants were used as bioindicators of glyphosate in the water remaining in the pots after applying herbicide. The increase in glyphosate doses promoted linear growth in <i>E. urophylla</i> intoxication and significantly reduced total dry mass and root production. <i>E. urophylla</i> plants had their photosynthetic, transpiratory, and stomatal conductance rates reduced as the herbicide doses increased. The AMPA root exudation was not detected, but it was possible to identify the presence of glyphosate by bioassay and chemical methods. Root exudation of glyphosate by eucalyptus can result in lesser herbicide action in plant control and cause contamination of deeper soil layers.</p>","PeriodicalId":15720,"journal":{"name":"Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes","volume":" ","pages":"749-757"},"PeriodicalIF":1.4,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142590637","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Pre-emergence herbicides mixture in soybeans: Amaranthus hybridus control and crop selectivity on cover crops soil. 大豆播前除草剂混合物:杂交苋在覆盖作物土壤上的控制和作物选择性。
IF 1.4 4区 农林科学
Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes Pub Date : 2024-01-01 Epub Date: 2024-07-03 DOI: 10.1080/03601234.2024.2372920
Modesto Roque Mita, Kassio Ferreira Mendes
{"title":"Pre-emergence herbicides mixture in soybeans: <i>Amaranthus hybridus</i> control and crop selectivity on cover crops soil.","authors":"Modesto Roque Mita, Kassio Ferreira Mendes","doi":"10.1080/03601234.2024.2372920","DOIUrl":"10.1080/03601234.2024.2372920","url":null,"abstract":"<p><p>The objective was to evaluate the efficacy of pre-emergence herbicides mixture applied to the soil with and without dead cover crops (<i>Sorghum bicolor</i>) for the control of <i>Amaranthus hybridus</i> L. (smooth pigweed) and its selectivity in soybeans. This study was structured in split plot (2 × 6 + 2), where factor A plots (with and without dead cover) and factor B six herbicides mixture: flumioxazin + S-metolachlor (50.4 + 1,008 g a.i. ha<sup>-1</sup>), flumioxazin + imazethapyr (60 + 127.2 g a.i. ha<sup>-1</sup>), pyroxasulfone + sulfentrazone (137.6 + 160 g a.i. ha<sup>-1</sup>), diuron + sulfentrazone (400 + 200 g a.i. ha<sup>-1</sup>), metribuzin + S-metolachlor (326.4 + 1,344 g a.i. ha<sup>-1</sup>) and sulfentrazone + imazethapyr (200 + 100 g a.i. ha<sup>-1</sup>) and two untreated control plots. As for the results, the herbicides flumioxazin + S-metolachlor, flumioxazin + imazethapyr and pyroxasulfone + sulfentrazone showed excellent control (97-99%) and were not influenced by the plot with and without dead cover. They also showed higher yield soybeans (<2,244 kg ha<sup>-1</sup>). All herbicides were selective to the soybeans. Overall, pre-emergence herbicides and cover crops were efficient methods for the control of <i>A. hybridus</i>, which farmers should use to avoid losses in yield soybeans due to weed competition.</p>","PeriodicalId":15720,"journal":{"name":"Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes","volume":" ","pages":"497-506"},"PeriodicalIF":1.4,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141492232","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Quantification of cresols in liquid smoke samples employing liquid-liquid extraction with low-temperature purification and analysis by gas chromatography-mass spectrometry. 利用液液萃取和低温净化以及气相色谱-质谱分析法对液体烟雾样本中的甲酚进行定量。
IF 1.4 4区 农林科学
Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes Pub Date : 2024-01-01 Epub Date: 2024-07-29 DOI: 10.1080/03601234.2024.2384717
Marina Ranna Pinheiro Vasconcelos, Lucélio Marques Alves Costa, Flaviano Oliveira Silvério, Gevany Paulino de Pinho
{"title":"Quantification of cresols in liquid smoke samples employing liquid-liquid extraction with low-temperature purification and analysis by gas chromatography-mass spectrometry.","authors":"Marina Ranna Pinheiro Vasconcelos, Lucélio Marques Alves Costa, Flaviano Oliveira Silvério, Gevany Paulino de Pinho","doi":"10.1080/03601234.2024.2384717","DOIUrl":"10.1080/03601234.2024.2384717","url":null,"abstract":"<p><p>Liquid smoke is a food additive and cresols are among its chemical constituents, potentially toxic to human health. Thus, the objective of this study was to develop a method to quantify cresols in liquid smoke. First, the liquid-liquid extraction with low temperature purification (LLE-LTP) was validated for cresols in water, as there are no cresol-free liquid smoke samples. Analyzes were performed by gas chromatography coupled to mass spectrometry in full scan mode. LLE-LTP was subsequently applied in five commercial samples of liquid smoke. Validation results showed that the proposed extraction method was selective for cresols, linear in the range of 0.5 to 35 mg L<sup>-1</sup>, limit of quantification of 0.5 mg L<sup>-1</sup>, recovery rate between 90% and 104% and relative standard deviation lower than 10%. The quantification of cresols in liquid smoke samples ranged from 3.0 to 38.3 mg L<sup>-1</sup> and the concentration of these chemical contaminants in liquid smoke remained constant for at least 21 days at 25 °C.</p>","PeriodicalId":15720,"journal":{"name":"Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes","volume":" ","pages":"562-570"},"PeriodicalIF":1.4,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141788176","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Herbicides in the initial growth and chlorophyll indices of sugarcane in pre-sprouted seedlings. 除草剂对甘蔗发芽前幼苗的初始生长和叶绿素指数的影响。
IF 2 4区 农林科学
Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes Pub Date : 2024-01-01 Epub Date: 2024-03-25 DOI: 10.1080/03601234.2024.2331946
Ana Ligia Giraldeli, André Felipe Moreira Silva, Gustavo Soares da Silva, Lucas da Silva Araújo, Luísa Carolina Baccin, Giovani Apolari Ghirardello, Ricardo Victoria Filho
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