{"title":"Preparation and Characterization of Biopolymeric Nanoparticles as Drug Delivery Vehicles","authors":"S. S. Sagiri, S. Nayak, S. Lakshmi, K. Pal","doi":"10.4018/978-1-7998-8591-7.ch069","DOIUrl":"https://doi.org/10.4018/978-1-7998-8591-7.ch069","url":null,"abstract":"In recent years, the use of biopolymeric nanoparticles as vehicles for drug delivery has increased exponentially. In the present study, chitosan and gelatin nanoparticles were prepared by ionic gelation and desolvation methods, respectively. Salicylic acid was used as the model drug. The nanoparticles were characterized using SEM, XRD analysis and FTIR spectrophotometric studies. In vitro drug release experiments were carried out to understand the mechanism of drug release. SEM micrographs showed the formation of spherical nanoparticles. XRD studies indicated a higher crystalline nature of the chitosan nanoparticles as compared to the gelatin nanoparticles. FTIR studies indicated the presence of salicylic acid within the drug- loaded nanoparticles. Drug release studies indicated that the developed nanoparticles may be used as carriers for various bioactive agents.","PeriodicalId":145165,"journal":{"name":"Research Anthology on Synthesis, Characterization, and Applications of Nanomaterials","volume":"17 3 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"123647206","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Transport Properties of Silicene Nanotube- and Silicene Nanoribbon-Based FETs","authors":"Deep Kamal Kaur Randhawa, Paramjot Singh, Tarun","doi":"10.4018/978-1-7998-1393-4.ch010","DOIUrl":"https://doi.org/10.4018/978-1-7998-1393-4.ch010","url":null,"abstract":"Silicene is one of the most interesting nanomaterials. In this chapter, computational studies have been done on Silicene nanotube and nanoribbon-based FETs to analyze their transport properties. The FET is designed from armchair nanoribbon and single wall nanotube. The scattering region is capped by a dielectric and a metallic layer to form a gate. The conductance versus gate bias voltage, conductance versus temperature up to 2000K, and electrode temperature versus current characteristics are calculated and plotted along with the design of the equivalent model of the structure. Extended Huckel-based calculations were used, and the analysis shows the transport properties of both structures.","PeriodicalId":145165,"journal":{"name":"Research Anthology on Synthesis, Characterization, and Applications of Nanomaterials","volume":"1 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"122347123","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
S. Valange, G. Châtel, P. Amaniampong, R. Behling, F. Jérôme
{"title":"Ultrasound-Assisted Synthesis of Nanostructured Oxide Materials","authors":"S. Valange, G. Châtel, P. Amaniampong, R. Behling, F. Jérôme","doi":"10.4018/978-1-7998-8591-7.ch007","DOIUrl":"https://doi.org/10.4018/978-1-7998-8591-7.ch007","url":null,"abstract":"This chapter is focused on the use of high intensity ultrasound for the preparation of nanostructured materials with an emphasis on recent prominent examples of the production of dense or porous metal oxides through sonochemical and ultrasonic spray pyrolysis routes. Sonochemistry enables the synthesis of oxides that are often unachievable by traditional methods or affords known materials with shape, size, and nano/microstructure control under fast reaction conditions. The fundamental principles of acoustic cavitation, as well as the main ultrasonic parameters affecting the cavitation phenomenon, are first summarized. Next, the applications of ultrasound in the synthesis of nanostructured oxide materials following both preparation methods are reviewed. Particular focus is given to the ultrasound-assisted synthesis of metal oxide nanoparticles for energy applications.","PeriodicalId":145165,"journal":{"name":"Research Anthology on Synthesis, Characterization, and Applications of Nanomaterials","volume":"13 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"127218569","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Nanotechnology Safety and Security","authors":"Janette Alba, Petra Roupcová, K. Klouda","doi":"10.4018/978-1-7998-3059-7.ch012","DOIUrl":"https://doi.org/10.4018/978-1-7998-3059-7.ch012","url":null,"abstract":"Because of their unique characteristics, research and development of new nanomaterials is one of the major disciplines of the twenty-first century, and examining their special properties, especially toxicity, is therefore necessary. As well as their benefits (technological improvements, specific material properties, improved resistance to natural effects), new materials also bring new risks requiring assessment in terms of occupational health and safety and their abuse as potential biological carriers or other materials. The study presents general information about nanoparticles and their distribution and properties in relation to entering aquatic, soil, and atmospheric environments. The study describes and cites examples of measurements conducted on the exposure of different nanomaterials to the work environment. Risk assessments of nanomaterials according to the available methodologies, measures to protect against nanoparticles, and importantly, the abuse of nanoparticles as a potential threat to the CZ population are also described.","PeriodicalId":145165,"journal":{"name":"Research Anthology on Synthesis, Characterization, and Applications of Nanomaterials","volume":"7 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"117046526","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Principles and Advantages of Microwave-Assisted Methods for the Synthesis of Nanomaterials for Water Purification","authors":"T. Saleh, S. Majeed, A. Nayak, B. Bhushan","doi":"10.4018/978-1-5225-2136-5.CH003","DOIUrl":"https://doi.org/10.4018/978-1-5225-2136-5.CH003","url":null,"abstract":"Nanomaterials are the pillars of nanoscience and nanotechnology and to realize their full potential in various potential applications, synthetic methodologies/routes need to be established that are simple, fast and cost-effective. Wet-chemical approaches for nanomaterial synthesis have proven to be among the most versatile and effective routes to finely tailor nanocrystals with varying compositional and architectural complexity. Microwave-assisted solution route represents an efficient wet-chemical approach for the synthesis of nanomaterials that offers additional advantages, such as rapid volumetric heating, high reaction rates, size and shape control by tuning reaction parameters, and energy efficiency. In addition, the homogenous heating of the reactants in microwave synthesis minimizes thermal gradients and provides uniform nucleation and growth conditions that leads to the formation of nanomaterials with uniform size distribution. This chapter deals with the basics of microwave chemistry and its applications towards the synthesis of nanomaterials for catalytic applications.","PeriodicalId":145165,"journal":{"name":"Research Anthology on Synthesis, Characterization, and Applications of Nanomaterials","volume":"44 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"126904173","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
D. Babatunde, I. Denwigwe, O. Babatunde, O. Agboola, Gbemisola Deborah Akinsipe
{"title":"Relevance of Chemically Functionalized Nano-Fillers and Modified Nanocomposite in Energy Systems","authors":"D. Babatunde, I. Denwigwe, O. Babatunde, O. Agboola, Gbemisola Deborah Akinsipe","doi":"10.4018/978-1-5225-7838-3.CH002","DOIUrl":"https://doi.org/10.4018/978-1-5225-7838-3.CH002","url":null,"abstract":"Reliable energy systems and advances in nanotechnology together will play key role in channeling future cutting edge inventions and developments in all spheres. In this review article, the pertinence of functionalizing nanofillers and modifying nanocomposites for improved performance in various energy applications such as energy conversion, energy efficiency, energy storage, alternative energy and energy saving are expounded. This article also presents structures and unique properties of commonly used nanofillers; advances, improvement potentials and characterization of nanocomposites used in energy systems. Theoretical and experimental literature reviewed revealed that nanofillers engender improved properties in polymeric matrices. Functionalization is applicable to all types of nanofillers in use today, a number of functionalized nanofillers are already commercially available; and more extensive research is needed to achieve optimal improved results with the use of nanofillers and nanocomposites in various fields of applications.","PeriodicalId":145165,"journal":{"name":"Research Anthology on Synthesis, Characterization, and Applications of Nanomaterials","volume":"1 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"129749917","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Recent Advancements in Photocatalytic Nanocomposites","authors":"A. Shajkumar, Ananthakumar Ramadoss","doi":"10.4018/978-1-7998-1530-3.ch006","DOIUrl":"https://doi.org/10.4018/978-1-7998-1530-3.ch006","url":null,"abstract":"Photocatalysts utilize light energy or photons to catalyze a reaction. The most significant characteristics of a photocatalyst lies in its ability to simultaneously oxidize a donor molecule and reduce an acceptor through the electron-hole pair generated upon excitation. With the emergence of nanotechnology, the utilization of nanomaterials for their photocatalytic properties has gained a new pace. TiO2 and ZnO nanoparticles are exploited widely for their photocatalytic properties. The recent trends concentrate on devising composite nanostructures that utilize both the properties of the photocatalyst and supporting materials such as graphene, carbon nanotubes, or noble metal nanoparticles to enhance the photocatalytic properties of the semiconductor metal oxide. The main areas of application of such structures lie in the field of water purification and energy harvesting. This chapter outlines an overview of the photocatalytic process and the existing technologies followed by the application areas and the recent advancements lying in that area.","PeriodicalId":145165,"journal":{"name":"Research Anthology on Synthesis, Characterization, and Applications of Nanomaterials","volume":"1 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"128979717","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Nanomaterials and Nanocomposites for Adsorptive Desulfurization","authors":"Saddam A. Al-Hammadi","doi":"10.4018/978-1-7998-2146-5.ch002","DOIUrl":"https://doi.org/10.4018/978-1-7998-2146-5.ch002","url":null,"abstract":"Desulfurization (removal of S compounds) of fuels is an important research topic in recent years. Several techniques have been reported to remove the sulfur-containing compounds in fuels. One of these techniques is adsorptive desulfurization (removal based on chemisorption and physisorption), which has received much attention because of low energy consumption and facile operation condition. This chapter discusses the methods employed under this technique and the types of nanocomposites and hybrid materials (adsorbents) that have been investigated as potential adsorbents. The strategies to enhance sulfur adsorption capacity and main challenges will be discussed.","PeriodicalId":145165,"journal":{"name":"Research Anthology on Synthesis, Characterization, and Applications of Nanomaterials","volume":"18 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"133811900","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Diverse Applications of Graphene-Based Polymer Nanocomposites","authors":"P. Majumdar, Amartya Chakrabarti","doi":"10.4018/978-1-7998-1530-3.ch003","DOIUrl":"https://doi.org/10.4018/978-1-7998-1530-3.ch003","url":null,"abstract":"Polymer nanocomposites are unique materials reinforced with nanoscale additives. Among a variety of nanomaterials available to act as filler additives in different polymer matrices, graphene is the most versatile one. Graphene-based polymer nanocomposites have improved electrical, mechanical, chemical, and thermal properties, which make them suitable for applications in the electronics, energy, sensor, and space sectors. Graphene, the nanosized filler, can be prepared using either a top-down or a bottom-up approach and dispersed in the polymer matrix utilizing different conventional techniques. The nanocomposite materials find usage in suitable area of applications depending on their specific characteristics. This chapter discusses the current state-of-the-art manufacturing techniques for graphene and graphene-based nanocomposite materials. Application of graphene-based polymer nanocomposites in the various fields with an emphasis on the areas high heat flux applications requiring enhanced thermal conductivity will be an additional major focus of this chapter.","PeriodicalId":145165,"journal":{"name":"Research Anthology on Synthesis, Characterization, and Applications of Nanomaterials","volume":"50 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"115567456","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
R. Naik, Revathi V., S. Prashantha, H. Nagabhushana
{"title":"Synthesis of Magnesium Based Nanophosphors and Nanocomposites by Different Techniques","authors":"R. Naik, Revathi V., S. Prashantha, H. Nagabhushana","doi":"10.4018/978-1-7998-8591-7.ch011","DOIUrl":"https://doi.org/10.4018/978-1-7998-8591-7.ch011","url":null,"abstract":"This chapter consists of systematic synthesis of magnesium silicate nanoparticles by solution combustion method using ODH fuel. Compared to other fuels, ODH has the better advantages of obtaining crystalline nanomaterials without post calcinations. By doping different rare earth ions to magnesium silicate, the product can be used for luminescent applications. Synthesis of magnesium ferrite nanoparticle is done using molten salt method followed by the synthesis of polymer composite in the form of fibers by the process of electrospinning.","PeriodicalId":145165,"journal":{"name":"Research Anthology on Synthesis, Characterization, and Applications of Nanomaterials","volume":"1 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"128761698","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}