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Selective detection of picolinic acid by molecularly imprinted polymer based electrochemical sensor 分子印迹聚合物电化学传感器对吡啶酸的选择性检测
IF 0.8 4区 材料科学
International Journal of Materials Research Pub Date : 2023-08-29 DOI: 10.1557/s43578-023-01136-0
Nur Asyiqin Zulkefli, F. S. Mehamod, A. Jani, Nur Habibah Safiyyah Jusoh, F. Suah
{"title":"Selective detection of picolinic acid by molecularly imprinted polymer based electrochemical sensor","authors":"Nur Asyiqin Zulkefli, F. S. Mehamod, A. Jani, Nur Habibah Safiyyah Jusoh, F. Suah","doi":"10.1557/s43578-023-01136-0","DOIUrl":"https://doi.org/10.1557/s43578-023-01136-0","url":null,"abstract":"Picolinic acid (PIC) is a key metabolite found in the amino acid tryptophan. While it has been well-studied for its significant role in mental health disorders, there has been little research into developing a rapid sensor to detect PIC. In this preliminary work, we sought to develop a molecularly imprinted polymers (MIPs)-based electrochemical sensor that could rapidly and selectively detect PIC. The electrochemical sensor performance was evaluated using differential pulse voltammetry (DPV) in a linear range between 1 and 5 mM, with a limit of detection of 0.6 mM (S/N = 3) and a limit of quantification of 1.7 mM (S/N = 10). The interference analysis was also conducted on the MIPs sensor to evaluate its ability to selectively detect PIC in the presence of other interfering molecules. Overall, the results demonstrate that this sensor has significant potential for use in the rapid and selective detection of PIC by electrochemical analysis.","PeriodicalId":14079,"journal":{"name":"International Journal of Materials Research","volume":"52 1","pages":"4214 - 4224"},"PeriodicalIF":0.8,"publicationDate":"2023-08-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"87846407","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Preparation of lightweight, high hardness multi-component systems induced by partial oxidation and hard intermetallic phase formation 由部分氧化和金属间相形成诱发的轻质、高硬度多组分体系的制备
IF 0.8 4区 材料科学
International Journal of Materials Research Pub Date : 2023-08-29 DOI: 10.1557/s43578-023-01137-z
S. Lee, C. Chokradjaroen, Yasuyuki Sawada, N. Saito
{"title":"Preparation of lightweight, high hardness multi-component systems induced by partial oxidation and hard intermetallic phase formation","authors":"S. Lee, C. Chokradjaroen, Yasuyuki Sawada, N. Saito","doi":"10.1557/s43578-023-01137-z","DOIUrl":"https://doi.org/10.1557/s43578-023-01137-z","url":null,"abstract":"The ternary Mg–Al–Ti and quaternary Mg–Al–Ti–Cu systems were prepared by mechanical alloying in oxygen-lean atmosphere followed by spark plasma sintering. The ternary Mg–Al–Ti and quaternary Mg–Al–Ti–Cu systems which were sintered at 750 °C after 16 h milling showed the highest hardness of 509 and 947 HV with low densities of 2.9 and 3.9 g/cm3, respectively. The decrease in particle size and uniform dispersion of elements through optimization of the MA process induced the formation of uniform composite microstructure after SPS. Moreover, the addition of the fourth element, Cu, showed a significant impact on the improvement in hardness. This result was explained from the perspective of the microstructure and the electronic nature of elements. Our results provide a facile method for synthesizing oxide/metal composites from elemental powders without a separate oxidation process.","PeriodicalId":14079,"journal":{"name":"International Journal of Materials Research","volume":"12 1","pages":"4235 - 4246"},"PeriodicalIF":0.8,"publicationDate":"2023-08-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"81546562","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of particle size and distribution of hollow spheres on the compressive behavior of aluminum matrix syntactic foams 中空球体粒径及分布对铝基复合泡沫压缩性能的影响
IF 0.8 4区 材料科学
International Journal of Materials Research Pub Date : 2023-08-29 DOI: 10.1557/s43578-023-01153-z
Yong Mei, Chao Fu, Ying Fu, E. Wang, Quanzhan Yang, Yong Ding
{"title":"Effect of particle size and distribution of hollow spheres on the compressive behavior of aluminum matrix syntactic foams","authors":"Yong Mei, Chao Fu, Ying Fu, E. Wang, Quanzhan Yang, Yong Ding","doi":"10.1557/s43578-023-01153-z","DOIUrl":"https://doi.org/10.1557/s43578-023-01153-z","url":null,"abstract":"Aluminum matrix syntactic foams (AMSFs) reinforced by Al2O3 hollow sphere (HS) with three different distributions of the particles were successfully produced by a self-developed counter-gravity infiltration casting technique. The effects of the size and distribution of particles on the quasi-static compressive behavior and failure mechanisms of the AMSFs was investigated. Microstructural images showed a clear interface between the fillers and matrix and no obvious shrinkage cavity was detected. The quasi-static compressive stress–strain curve of the AMSFs underwent three stages, namely linear-elastic, plateau, and then densification stages. The long plateau stage indicated that the AMSFs have excellent energy absorption capacity. The compressive strength and specific energy absorption capacity of the syntactic foam was lower when smaller particles were used and the compressive strength of bimodal AMSFs was much lower than that of monomodal AMSFs. The deformation of the AMSFs under compressive load, indicates that the distribution of the particles has an important influence on the failure mechanism of the AMSFs.","PeriodicalId":14079,"journal":{"name":"International Journal of Materials Research","volume":"5 1","pages":"4408 - 4419"},"PeriodicalIF":0.8,"publicationDate":"2023-08-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76122050","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Thermodynamic modeling of the Sb–Te system supported by DSC measurement and ab initio calculations 由DSC测量和从头计算支持的Sb-Te体系热力学模型
IF 0.8 4区 材料科学
International Journal of Materials Research Pub Date : 2023-08-29 DOI: 10.1557/s43578-023-01140-4
Cheng-Yu Liu, Yu-Yun Liu, Su-Hua Chen, Sinn-Wen Chen, A. Dębski, W. Gasior, W. Gierlotka
{"title":"Thermodynamic modeling of the Sb–Te system supported by DSC measurement and ab initio calculations","authors":"Cheng-Yu Liu, Yu-Yun Liu, Su-Hua Chen, Sinn-Wen Chen, A. Dębski, W. Gasior, W. Gierlotka","doi":"10.1557/s43578-023-01140-4","DOIUrl":"https://doi.org/10.1557/s43578-023-01140-4","url":null,"abstract":"Nowadays, thermoelectric materials became important sources of renewable energy. Among various materials that show this property, the Sb2Te3 attracts attention due to its excellent properties. Recent experimental information revealed a new phase equilibrium data; therefore, it is reasonable to elaborate a state-of-art thermodynamic model of the binary Sb–Te system. In this work, a new thermodynamic description is proposed based on the available experimental data. In addition, a new DSC measurement of heat and temperature of fusion of Sb2Te3 as well as ab initio calculation of Sb2Te3 were included in the experimental dataset. The homogeneity range of Sb2Te3 was modeled according to the stability of defects obtained from first-principle calculations. The morphology of the optimized phase diagram follows the latest findings, which means that the Ksi phase has replaced the delta and gamma phases. The elaborated thermodynamic parameters allow for a good reproduction of experimental data as well as for future modeling of higher-ordered systems.","PeriodicalId":14079,"journal":{"name":"International Journal of Materials Research","volume":"34 1","pages":"4287 - 4302"},"PeriodicalIF":0.8,"publicationDate":"2023-08-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"91174226","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
DGM – Deutsche Gesellschaft für Materialkunde (德国情报协会
4区 材料科学
International Journal of Materials Research Pub Date : 2023-08-25 DOI: 10.1515/ijmr-2023-2009
{"title":"DGM – Deutsche Gesellschaft für Materialkunde","authors":"","doi":"10.1515/ijmr-2023-2009","DOIUrl":"https://doi.org/10.1515/ijmr-2023-2009","url":null,"abstract":"","PeriodicalId":14079,"journal":{"name":"International Journal of Materials Research","volume":"9 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-08-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135237228","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Correction: In vitro evaluation of pH-sensitive liposomes loaded with d-limonene in targeting human malignant glioma cells 更正:在体外评估负载d-柠檬烯的ph敏感脂质体靶向人类恶性胶质瘤细胞
IF 0.8 4区 材料科学
International Journal of Materials Research Pub Date : 2023-08-25 DOI: 10.1557/s43578-023-01131-5
Vinitha Rani, J. Venkatesan, A. Prabhu
{"title":"Correction: In vitro evaluation of pH-sensitive liposomes loaded with d-limonene in targeting human malignant glioma cells","authors":"Vinitha Rani, J. Venkatesan, A. Prabhu","doi":"10.1557/s43578-023-01131-5","DOIUrl":"https://doi.org/10.1557/s43578-023-01131-5","url":null,"abstract":"This article was updated to correct Fig. 7. The correct Fig. 7 is also reproduced here. Correction: In vitro evaluation of pH‐sensitive liposomes loaded with d‐limonene in targeting human malignant glioma cells Vinitha Rani1, Jayachandran Venkatesan1, Ashwini Prabhu1,a) 1 Yenepoya Research Centre, Yenepoya (Deemed to be University), Deralakatte, Mangalore, Karnataka 575018, India a) Address all correspondence to this author. e-mail: ashwiniprabhu@yenepoya.edu.in","PeriodicalId":14079,"journal":{"name":"International Journal of Materials Research","volume":"149 1","pages":"4334 - 4334"},"PeriodicalIF":0.8,"publicationDate":"2023-08-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"89037425","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Automated classification of granular bainite and polygonal ferrite by electron backscatter diffraction verified through local structural and mechanical analyses 通过局部结构和力学分析，验证了电子背散射衍射对粒状贝氏体和多边形铁素体的自动分类
IF 0.8 4区 材料科学
International Journal of Materials Research Pub Date : 2023-08-24 DOI: 10.1557/s43578-023-01113-7
R. Jentner, S. Tsai, A. Welle, K. Srivastava, S. Scholl, J. Best, C. Kirchlechner, G. Dehm
{"title":"Automated classification of granular bainite and polygonal ferrite by electron backscatter diffraction verified through local structural and mechanical analyses","authors":"R. Jentner, S. Tsai, A. Welle, K. Srivastava, S. Scholl, J. Best, C. Kirchlechner, G. Dehm","doi":"10.1557/s43578-023-01113-7","DOIUrl":"https://doi.org/10.1557/s43578-023-01113-7","url":null,"abstract":"Differentiation of granular bainite and polygonal ferrite in high-strength low-alloy (HSLA) steels possesses a significant challenge, where both nanoindentation and chemical analyses do not achieve an adequate phase classification due to the similar mechanical and chemical properties of both constituents. Here, the kernel average misorientation from electron backscatter diffraction (EBSD) was implemented into a Matlab code to differentiate and quantify the microstructural constituents. Correlative electron channeling contrast imaging (ECCI) validated the automated phase classification results and was further employed to investigate the effect of the grain tolerance angle on classification. Moreover, ECCI investigations highlighted that the grain structure of HSLA steels can be subdivided into four grain categories. Each category contained a different nanohardness or substructure size that precluded a nanoindentation-based phase classification. Consequently, the automated EBSD classification approach based on local misorientation achieved a reliable result using a grain tolerance angle of 5°.","PeriodicalId":14079,"journal":{"name":"International Journal of Materials Research","volume":"25 1","pages":"4177 - 4191"},"PeriodicalIF":0.8,"publicationDate":"2023-08-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"75839699","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 3
Correction: Effects of annealing on bonding strengthening mechanism of Ti/Al composite sheets by twin‑roll casting with roller vibration 修正:退火对双辊振动铸造Ti/Al复合薄板结合强化机制的影响
IF 0.8 4区 材料科学
International Journal of Materials Research Pub Date : 2023-08-22 DOI: 10.1557/s43578-023-01051-4
Li Li, Fengshan Du
{"title":"Correction: Effects of annealing on bonding strengthening mechanism of Ti/Al composite sheets by twin‑roll casting with roller vibration","authors":"Li Li, Fengshan Du","doi":"10.1557/s43578-023-01051-4","DOIUrl":"https://doi.org/10.1557/s43578-023-01051-4","url":null,"abstract":"Correction: Effects of annealing on bonding strengthening mechanism of Ti/Al composite sheets by twin‐roll casting with roller vibration Li Li1,2, Fengshan Du1,2,a) 1 National Engineering Research Center for Equipment and Technology of Cold Strip Rolling, Yanshan University, Qinhuangdao 066004, Hebei, People’s Republic of China 2 College of Mechanical Engineering, Yanshan University, Qinhuangdao 066004, Hebei, People’s Republic of China a) Address all correspondence to this author. e-mail: fsdu@ysu.edu.cn","PeriodicalId":14079,"journal":{"name":"International Journal of Materials Research","volume":"2 1","pages":"4175 - 4175"},"PeriodicalIF":0.8,"publicationDate":"2023-08-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"77603066","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Ultraviolet-B radiation from Gd (III) doped hardystonite Gd (III)掺杂硬石的紫外- b辐射
IF 0.8 4区 材料科学
International Journal of Materials Research Pub Date : 2023-08-18 DOI: 10.1515/ijmr-2022-0289
Vijay P. Singh, Ch.B. Annapurna Devi, A. Rao, J. Joo
{"title":"Ultraviolet-B radiation from Gd (III) doped hardystonite","authors":"Vijay P. Singh, Ch.B. Annapurna Devi, A. Rao, J. Joo","doi":"10.1515/ijmr-2022-0289","DOIUrl":"https://doi.org/10.1515/ijmr-2022-0289","url":null,"abstract":"Abstract Trivalent gadolinium (Gd3+)-doped calcium zinc silicate (Ca2ZnSi2O7/hardystonite) with a molar composition of Ca2−x ZnSi2O7:xGd3+ (x = 0.09 mol) was produced using a sol–gel system. The hardystonite was characterized using X-ray diffraction and Fourier transform infrared spectroscopy. The X-ray diffraction study revealed that the prepared sample contained a tetragonal phase of Ca2ZnSi2O7. The vibrational structures of the sample were studied using Fourier transform infrared spectroscopy measurements. The photoluminescence emission spectrum of the Ca1.91ZnSi2O7:0.09Gd3+ phosphor narrow band was optimized at 312 nm in the Ultraviolet-B region under excitation at 273 nm wavelength. Electron paramagnetic resonance study authenticates the presence of gadolinium (Gd) ions within the trivalent state in the Ca1.91ZnSi2O7:0.09Gd3+ host.","PeriodicalId":14079,"journal":{"name":"International Journal of Materials Research","volume":"41 1","pages":""},"PeriodicalIF":0.8,"publicationDate":"2023-08-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"90883708","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Bacterial cellulose: A smart biomaterial for biomedical applications 细菌纤维素:用于生物医学应用的智能生物材料
IF 0.8 4区 材料科学
International Journal of Materials Research Pub Date : 2023-08-17 DOI: 10.1557/s43578-023-01116-4
Ashutosh Pandey, M. Singh, Annika Singh
{"title":"Bacterial cellulose: A smart biomaterial for biomedical applications","authors":"Ashutosh Pandey, M. Singh, Annika Singh","doi":"10.1557/s43578-023-01116-4","DOIUrl":"https://doi.org/10.1557/s43578-023-01116-4","url":null,"abstract":"The escalating curiosity in bacterial cellulose (BC) due to exceptional attributes such as purity, biodegradability, non-toxicity, porous fibrillar structure, and high water retention potential expand its applications to tissue engineering, controlled drug delivery, and cosmetics. BC has proved highly prospective to be used to manufacture innovative wound care solutions, drug carriers and delivering complexes. The drug-carrying BC found enormous applications in dental therapies, wound care, and scare-free wound management. Various degradation techniques of BC under antibiotic environments and physiological conditions offer different advantages in drug design. The drug loading capacity of BC can be increased by in situ modifications of its fibrillar network. The BC-based scaffolds compounded with other materials such as nanopolymers have explored new frontiers for BC applications in auspicious biomedicinal product developments. BC can accommodate different nanoparticles, biomaterials, synthetic materials, carbon materials, and plant extracts, which allows using BC in various biomedical and cosmetic products.\u0000 Graphical abstract","PeriodicalId":14079,"journal":{"name":"International Journal of Materials Research","volume":"67 1","pages":""},"PeriodicalIF":0.8,"publicationDate":"2023-08-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"89618386","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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