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Preparation of Mg-Mn doped LiNiO2 via direct Indonesian Mixed Hydroxide Precipitate Lithiation 印尼混合氢氧沉淀直接锂化法制备Mg-Mn掺杂LiNiO2
Energy Storage Technology and Applications Pub Date : 2022-06-27 DOI: 10.20961/esta.v2i1.61257
M. Rahmawati, E. Apriliyani, T. Paramitha, H. S. A. Gustiana
{"title":"Preparation of Mg-Mn doped LiNiO2 via direct Indonesian Mixed Hydroxide Precipitate Lithiation","authors":"M. Rahmawati, E. Apriliyani, T. Paramitha, H. S. A. Gustiana","doi":"10.20961/esta.v2i1.61257","DOIUrl":"https://doi.org/10.20961/esta.v2i1.61257","url":null,"abstract":"Using local raw materials affects the development of the Li-ion batteries industry in Indonesia, which is highly important for the sustainability of electric vehicles. Cathode material affects around 40-50% of Li-ion batteries production costs. The utilization of cheap and local nickel sources for nickel rich-cathode material is a promising approach for reducing LIBs cell cost. Mixed Hydroxide Precipitate (MHP) which contain significantly high amount of nickel can serve as the nickel source for LiNiO2 cathode material This article proposes an effective and economical method to obtain nickel rich cathode material via direct high thermal lithiation of MHP. Non negligible amount of Mn and Mg in MHP can be directly used as a dopant. Based on XRD analysis, a mixture of NiO and LNO phase can be detected. The presence of Mg and Mn impurities is not observable. The SEM images confirms the irregular shape of the as-prepared LNO. The FTIR confirm the absence of residual Li. Based on the findings, a pretreatment technique is required to be explored in the future.","PeriodicalId":11676,"journal":{"name":"Energy Storage Technology and Applications","volume":"108 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2022-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"81211320","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Preliminary Study of LiCoPO4 cathode material synthesis for LiCoPO4/Graphite Cell LiCoPO4/石墨电池正极材料合成的初步研究
Energy Storage Technology and Applications Pub Date : 2022-06-27 DOI: 10.20961/esta.v2i1.61250
A. P. Hutama, C. Yudha, Y. R. Azinuddin
{"title":"Preliminary Study of LiCoPO4 cathode material synthesis for LiCoPO4/Graphite Cell","authors":"A. P. Hutama, C. Yudha, Y. R. Azinuddin","doi":"10.20961/esta.v2i1.61250","DOIUrl":"https://doi.org/10.20961/esta.v2i1.61250","url":null,"abstract":"Nowadays, the race towards a high-performance Li-ion batteries discovery for energy storage has become an interesting technological challenge. New or improved Li-ion battery cathodes have been developed relentlessly in this decade. LiCoPO4 (LCP) is a cathode material that allow a battery to operate at high voltage which resulted a high energy density battery. The presence of strong P-O bond adds a thermal stability feature to LIB cells. In this study, a LiCoPO4 material were prepared by precipitation of Co3(PO4)2 (CP) followed by high temperature Li insertion. H­3PO4 were used as the phosphate source. The crystallization or precipitation of CP can only be achieved under mild pH condition, which can be controlled using sodium hydroxide. XRD, SEM and FTIR analysis were used to characterize the final product. The as-obtained LCP were applied as cathode material while graphite was used as the counter anode. The cell can deliver a charge-discharge capacity at a voltage of 2.0-4.95 V. This preliminary can be a groundwork toward the commercialization of LCP based Li-ion batteries for high duty application.","PeriodicalId":11676,"journal":{"name":"Energy Storage Technology and Applications","volume":"35 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2022-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"84649295","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Comparative Study of Novelty Thin-films for Li-ion Batteries 新型锂离子电池薄膜的比较研究
Energy Storage Technology and Applications Pub Date : 2022-06-27 DOI: 10.20961/esta.v2i1.61268
M. Ikhsanudin
{"title":"Comparative Study of Novelty Thin-films for Li-ion Batteries","authors":"M. Ikhsanudin","doi":"10.20961/esta.v2i1.61268","DOIUrl":"https://doi.org/10.20961/esta.v2i1.61268","url":null,"abstract":"The development of Li-ion batteries leads to high-density Li-ion battery technology as a storage system. to realize a Li-ion battery with a high energy density is to modify its anode, called a thin-film anode. The anode used is coated with a material thickness of 10 mm, increasing the cathode material that can be accommodated in one cell. This study aimed to analyze the Cu-powder and LTO materials used in Thin-film Li-ion batteries as a substitute for graphite because they offer higher capacity, chemical stability, fast charging technology (LTO), cheap, and environmentally friendly (Cu-powder). Based on XRD and FTIR tests, the material has a good crystal structure, and not many impurities are still contained in it. The SEM results showed that both particles showed uniformity in the shape of a single particle and were strengthened by the SEM-EDX test to review the quantity of each element present in the two materials. The electrochemical test results showed that Cu-powder material was better, with a specific capacity of 144.82 mAh g-1, higher than LTO (81.04 mAh g-1).","PeriodicalId":11676,"journal":{"name":"Energy Storage Technology and Applications","volume":"62 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2022-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"77901972","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Increasing Electric Bicycle Performance using Lithium Ferro Phospate Batteries with a Battery Management System 利用磷酸铁锂电池和电池管理系统提高电动自行车性能
Energy Storage Technology and Applications Pub Date : 2022-06-27 DOI: 10.20961/esta.v2i1.61525
Windhu Griyasti Suci
{"title":"Increasing Electric Bicycle Performance using Lithium Ferro Phospate Batteries with a Battery Management System","authors":"Windhu Griyasti Suci","doi":"10.20961/esta.v2i1.61525","DOIUrl":"https://doi.org/10.20961/esta.v2i1.61525","url":null,"abstract":"The depletion of fossil fuel sources and the increasing environmental pollution caused by the burning of motor vehicle fuels are major problems worldwide that need to be solved. One of the promising solutions to overcome energy security and environmental pollution is the use of electric vehicles. E-bikes are one of the most popular electric vehicles because of their many benefits. A valve-regulated lead acid battery (VRLA) is now the most common energy source for electric vehicles. It is heavy and unsafe for the user due to its poor energy density. Lithium ion batteries may be a feasible solution. One type of Li-ion battery that is environmentally friendly is lithium ferro phosphate (LFP). The potential that exists encourages researchers to conduct research and compare the performance of VRLA batteries with LFP batteries. The data retrieval method is carried out using the Arduino data logger application and is equipped with a microcontroller to read current and voltage. The test results prove that the LFP battery has good voltage stability. The distance that can be traveled is quite long, which is up to 50.16 km, because it is supported by a large capacity. On the other hand, VRLA can only travel 37.83 kilometers. Furthermore, the energy density of LFP batteries is great. The VRLA battery has a low energy density of 38.7 Wh/kg, whereas the LFP battery has a higher energy density of 117 Wh/kg, making it lighter and safer for users.","PeriodicalId":11676,"journal":{"name":"Energy Storage Technology and Applications","volume":"26 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2022-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"81346560","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
A layered lithium nickel manganese oxide as environmentally friendly cathode material for secondary batteries 层状锂镍锰氧化物作为二次电池的环保正极材料
Energy Storage Technology and Applications Pub Date : 2022-06-27 DOI: 10.20961/esta.v2i1.61203
M. Arinawati, F. Nugroho, C. Yudha
{"title":"A layered lithium nickel manganese oxide as environmentally friendly cathode material for secondary batteries","authors":"M. Arinawati, F. Nugroho, C. Yudha","doi":"10.20961/esta.v2i1.61203","DOIUrl":"https://doi.org/10.20961/esta.v2i1.61203","url":null,"abstract":"Cobalt-free cathode material development is considered necessity to assure the sustainability of Li-ion batteries. Cobalt is always considered expensive and unsafe for both human and environment. LiNi0.5Mn0.5O2 (LNMO) is a layer structured cathode material that has similar feature to LiCoO2 (LCO). A simple and fast processing of LNMO is proposed. A precipitation of nickel manganese oxalate was obtained in a batch reactor under atmospheric condition. The as-obtained homogenous oxalate precursor was converted to LNMO via high temperature lithiation. Based on the XRD result, a crystalline product with layer structure is successfully obtained. The presence of impurities such as residual Li can be detected from the FTIR spectra. SEM Images confirmed quasi-spherical particles with grain size of less than 10 micrometer. The charge-discharge analysis of LNMO containing cell deliver a capacity of 42 mAh/g. In spite of its promising report, continuous improvement is necessary to obtain cell with better electrochemical performance.","PeriodicalId":11676,"journal":{"name":"Energy Storage Technology and Applications","volume":"11 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2022-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"88486051","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Kinetics Study of LiFePO4 Synthesis Reaction with Solid State Method 固相法合成LiFePO4反应动力学研究
Energy Storage Technology and Applications Pub Date : 2021-12-01 DOI: 10.20961/esta.v1i1.56797
E. Dyartanti, A. R. Nurohmah, I. P. Lestari, M. I. Putra, S. S. Nisa, Ulfa Pratiwi
{"title":"Kinetics Study of LiFePO4 Synthesis Reaction with Solid State Method","authors":"E. Dyartanti, A. R. Nurohmah, I. P. Lestari, M. I. Putra, S. S. Nisa, Ulfa Pratiwi","doi":"10.20961/esta.v1i1.56797","DOIUrl":"https://doi.org/10.20961/esta.v1i1.56797","url":null,"abstract":"Lithium Ferro Phosphate (LiFePO4) is a cathode that has the advantage of abundant raw material, inexpensive and easily upgraded compared to other cathode. The method commonly used for LiFePO4 synthesis is solid state. It is important to study kinetics in this process for product optimization. There are two methods in determining the kinetics of product formation including Thermogravimetric Differential Thermal Analysis (TG-DTA) and X-ray Diffraction (XRD). Meanwhile, Cyclic Voltammetry (CV) and Electrochemical Impedance Spectroscopy (EIS). Meanwhile, CV and EIS were used to determine electrochemical kinetics.","PeriodicalId":11676,"journal":{"name":"Energy Storage Technology and Applications","volume":"91 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2021-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"85658314","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis of FePO4 Precursor for LiFePO4 Battery Cathode from Used Nickel Plated A3 Steel Battery Shell by Hydrometallurgy Processing 湿法冶金法从镀镍的A3钢电池壳中合成LiFePO4电池正极前驱体
Energy Storage Technology and Applications Pub Date : 2021-12-01 DOI: 10.20961/esta.v1i1.56802
R. Aisyah, S. T. Samudera, A. Jumari, A. Nur
{"title":"Synthesis of FePO4 Precursor for LiFePO4 Battery Cathode from Used Nickel Plated A3 Steel Battery Shell by Hydrometallurgy Processing","authors":"R. Aisyah, S. T. Samudera, A. Jumari, A. Nur","doi":"10.20961/esta.v1i1.56802","DOIUrl":"https://doi.org/10.20961/esta.v1i1.56802","url":null,"abstract":"One of the most well-known material for lithium battery cathode synthesis of lithium ferro-phosphate type is iron phosphate precursor. The precursor is synthesized by the use of leaching method with tartaric acid solution with optimization at various leaching temperature and time. The temperature variables are at 30 ℃, 50 ℃, 70 ℃, and 90 oC. The time variables are at 3 hours, 6 hours, and 9 hours. The main material that is used is iron from used nickel plated A3 steel battery shell. The recovered iron concentration and quantity is calculated from absorbance by atomic absorption spectrophotometry (AAS). AAS analysis indicates the absorbed Fe is rated at 1,02 % (30 ℃, 2,76 % (50 ℃), 9,93 % (70 ℃), and 34,31 % (90 ℃) during 9 hours of leaching.The analysis indicates the recovered iron is rated the highest during 9 hours of leaching at the highest temperature. X-ray diffraction analysis at various leaching temperature variable indicates formation of iron phosphate crystal to be compared with iron phosphate commercial precursor, while scanning electron microscope analysis shows uniform iron phosphate particle morphology.","PeriodicalId":11676,"journal":{"name":"Energy Storage Technology and Applications","volume":"105 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2021-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"75166174","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
LiCoO2 Cathode Material Prepared through Two Step Sintering Process 两步烧结法制备LiCoO2正极材料
Energy Storage Technology and Applications Pub Date : 2021-12-01 DOI: 10.20961/esta.v1i1.56800
A. P. Hutama, M. Arinawati, E. Apriliyani, Y. R. Azinuddin, C. Yudha
{"title":"LiCoO2 Cathode Material Prepared through Two Step Sintering Process","authors":"A. P. Hutama, M. Arinawati, E. Apriliyani, Y. R. Azinuddin, C. Yudha","doi":"10.20961/esta.v1i1.56800","DOIUrl":"https://doi.org/10.20961/esta.v1i1.56800","url":null,"abstract":"LiCoO2 cathode material has been continuously applied in commercial LIBs cells. It has high gravimetric and volumetric density. In this research, an economical approach to obtain LiCoO2 is proposed. Pure cobalt oxide (Co3O4) precursor was obtained via atmospheric precipitation of cobalt sulfate and thermal decomposition of the as-obtained hydroxide precursor. The next heat treatment was performed to obtain LiCoO2 powder. To investigate the characteristic of the precursor and the final product, XRD, FTIR, and SEM analysis were conducted. The final product has hexagonal structure and quasi spherical morphology. The size of the particle is in micron. The charge-discharge analysis of LiCoO2 was conducted in LiCoO2/Graphite system where the initial capacity of LiCoO2 is 120 mAh/g at the current density of 0.1 C (20 mA/g). Overall, this method can be used for large scale LiCoO­2 cell production.","PeriodicalId":11676,"journal":{"name":"Energy Storage Technology and Applications","volume":"71 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2021-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76403338","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Zinc Oxalate as a Green Anode Material for Commercial Li-Ion Batteries: a Preliminary Study 草酸锌作为商用锂离子电池绿色负极材料的初步研究
Energy Storage Technology and Applications Pub Date : 2021-12-01 DOI: 10.20961/esta.v1i1.56799
M. Arinawati, A. P. Hutama, E. Apriliyani, M. Ikhsanudin, C. Yudha
{"title":"Zinc Oxalate as a Green Anode Material for Commercial Li-Ion Batteries: a Preliminary Study","authors":"M. Arinawati, A. P. Hutama, E. Apriliyani, M. Ikhsanudin, C. Yudha","doi":"10.20961/esta.v1i1.56799","DOIUrl":"https://doi.org/10.20961/esta.v1i1.56799","url":null,"abstract":"Li ion batteries is a crucial energy storage for new and renewable energy (NRE)-based power plant due to its high energy density. However, the anode materials of commercial Li-ion batteries such as graphite and Li4Ti5O12 are considered less eco-friendly due to it requirement of high temperature processing which is also uneconomical. In this research, for the first time ever, zinc oxalate was prepared via mild temperature precipitation process and applied as anode material in commercial Li-ion batteries. XRD, FTIR and SEM analysis were conducted to examine the physical and chemical properties of the as obtained zinc oxalate. The effect of precursor concentration was investigated. Charge-discharge analysis shows that zinc oxalate dihydrate as anode material delivered a discharge capacity of 25 mAh/g.","PeriodicalId":11676,"journal":{"name":"Energy Storage Technology and Applications","volume":"25 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2021-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83381091","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Li-ion Batteries Waste Processing and Utilization Progress: A Review 锂离子电池废弃物处理与利用研究进展
Energy Storage Technology and Applications Pub Date : 2021-12-01 DOI: 10.20961/esta.v1i1.56801
E. Apriliyani, M. Arinawati, S. S. Nisa, S. U. Muzayanha, T. Paramitha
{"title":"Li-ion Batteries Waste Processing and Utilization Progress: A Review","authors":"E. Apriliyani, M. Arinawati, S. S. Nisa, S. U. Muzayanha, T. Paramitha","doi":"10.20961/esta.v1i1.56801","DOIUrl":"https://doi.org/10.20961/esta.v1i1.56801","url":null,"abstract":"Li ion batteries (LIBs) are widely used as energy storage for electronic devices and electric vehicles. Due to its limited lifetime, its disposal can cause a serious environmental problem. Heavy metals are highly toxic and require serious handling. Moreover, the some of the heave metals are considered valuable to be directly discarded. In this review, LIBs waste processing techniques were discussed. The cathode material which contain high amount of heavy metals can be processed using metallurgical approach, such as: pyro-metallurgy, hydro-metallurgy and bio-metallurgy which have their own advances and disadvantages. The recovery of heavy metals can be performed by bottom-up process such as chemical precipitation, hydrothermal, and sol-gel process. In the end, the recovered valuable metals can be used as precursor to Li-ion batteries materials, thus reducing the exploitation of metals through mining process and reducing hazardous waste.","PeriodicalId":11676,"journal":{"name":"Energy Storage Technology and Applications","volume":"26 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2021-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"90910872","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
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