{"title":"A new process route for the additive manufacturing of a high nitrogen containing martensitic stainless steel - A feasibility study","authors":"L. Becker, P. König, J. Lentz, S. Weber","doi":"10.1016/j.addlet.2024.100257","DOIUrl":"10.1016/j.addlet.2024.100257","url":null,"abstract":"<div><div>High-nitrogen martensitic stainless steels, such as X30CrMoN15 (0.3 to 0.5 mass% nitrogen), exhibit an excellent combination of strength and corrosion resistance, making them well-suited for applications in the medical technology and aerospace industry. The qualification of these steels for additive manufacturing (AM) could generate new application areas where AM, due to its process-specific advantages, could offer added value compared to conventional manufacturing methods. However, the laser powder bed fusion (PBF-LB/M) of high-nitrogen alloyed steels is challenging due to the high tendency for gas pore formation, resulting from the limited nitrogen solubility in the steel melt. In this work, a new process route for AM of a high nitrogen containing X50CrMoV15 martensitic stainless steel is presented, which consists of a process combination of powder nitriding, PBF-LB/M and subsequent hot isostatic pressing (HIP) with integrated quenching. Gas nitriding is used to achieve a nitrogen content in the starting powder that exceeds the maximum solubility in the melt. Although the nitrogen content decreases during the PBF-LB/M process, the high solidification and cooling rates prevent the melt from reaching equilibrium nitrogen levels, resulting in a nitrogen content above the solubility limit in the final PBF-LB/M state. The pores formed during the process are closed through HIP, which also allows hardening via integrated gas quenching. With an additional cryogenic treatment, the process produces a fully dense steel with 75% martensitic structure and 0.246 mass% nitrogen. Further optimization opportunities have been identified and are discussed.</div></div>","PeriodicalId":72068,"journal":{"name":"Additive manufacturing letters","volume":"11 ","pages":"Article 100257"},"PeriodicalIF":4.2,"publicationDate":"2024-11-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142702849","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Additive manufacturing simulations: An approach based on space partitioning and dynamic 3D mesh adaptation","authors":"Panagis Foteinopoulos, Alexios Papacharalampopoulos, Panagiotis Stavropoulos","doi":"10.1016/j.addlet.2024.100256","DOIUrl":"10.1016/j.addlet.2024.100256","url":null,"abstract":"<div><div>Simulation is one of the most widely used methods for process optimization towards improved part quality in Additive Manufacturing (AM), particularly for metal parts. However, due to the nature of the AM processes and the complex phenomena that occur, simulations that are capable of providing a detailed overview of the physical mechanisms demand considerable computational resources and time. In this study, a numerical approach is presented, which can be applied to any implicit numerical thermal simulation for AM, allowing for a significant decrease in computational time (higher than 70%) with minimal impact on accuracy. This is achieved by combining space partitioning, enabled by a boundary condition that was developed, with dynamic mesh adaptation in the <em>x</em>-, <em>y</em>-, and <em>z</em>-axis. The methodology is described in detail and both the decrease in computational time and the accuracy of the developed approach are validated in a computational case study, as well as using experimental results.</div></div>","PeriodicalId":72068,"journal":{"name":"Additive manufacturing letters","volume":"11 ","pages":"Article 100256"},"PeriodicalIF":4.2,"publicationDate":"2024-11-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142702850","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Nicolas Nothomb , Ignacio Rodriguez-Barber , María Teresa Pérez-Prado , Norberto Jimenez Mena , Grzegorz Pyka , Aude Simar
{"title":"Understanding the effect of pre-sintering scanning strategy on the relative density of Zr-modified Al7075 processed by laser powder bed fusion","authors":"Nicolas Nothomb , Ignacio Rodriguez-Barber , María Teresa Pérez-Prado , Norberto Jimenez Mena , Grzegorz Pyka , Aude Simar","doi":"10.1016/j.addlet.2024.100253","DOIUrl":"10.1016/j.addlet.2024.100253","url":null,"abstract":"<div><div>Only a limited aluminium material palette is currently available for L-PBF processing, especially for high strength aluminium alloy. Unmodified Al7075 suffers from hot cracking making it nearly impossible to process by L-PBF. Adding some grain refiner to Al7075 solves this issue of hot cracking. However, this alloy still presents difficulties to be processed with densities above 99.5%. In this study, the unconventional pre-sintering scanning strategy is applied to process 99.9% density Al7075+1.8%Zr. For this scanning strategy, each layer is scanned twice with different power, i.e. it is first scanned with half the power selected for the second scan. This specific strategy remelts potential defect generated by the first scan and reduces lack of fusion pores. These two phenomena lead to high density L-PBF Al7075+1.8%Zr and pave the way to higher densities for high strength aluminium alloys.</div></div>","PeriodicalId":72068,"journal":{"name":"Additive manufacturing letters","volume":"11 ","pages":"Article 100253"},"PeriodicalIF":4.2,"publicationDate":"2024-11-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142702920","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Mohammad Salman Yasin , Kevin Stonaker , Shuai Shao , Nima Shamsaei
{"title":"Mechanical performance of laser powder bed fused Ti-6Al-4V: The influence of filter condition and part location","authors":"Mohammad Salman Yasin , Kevin Stonaker , Shuai Shao , Nima Shamsaei","doi":"10.1016/j.addlet.2024.100255","DOIUrl":"10.1016/j.addlet.2024.100255","url":null,"abstract":"<div><div>Deteriorated filter condition in laser powder bed fusion (L-PBF) systems may negatively impact shield gas flow, causing inadequate spatter particle/plume removal, leading to laser beam attenuation and reduction in melt pool depth, and potentially causing more frequent formation of volumetric defects. This work investigated the effects of filter condition and part location on the micro-/defect-structure and mechanical behavior, including tensile and fatigue, of Ti-6Al-4V parts fabricated by L-PBF. Interestingly, within the manufacturer recommended service intervals, no specific effect of filter condition could be observed on the micro-/defect-structure or the mechanical behavior of the fabricated parts. However, the parts’ defect-structures were affected by their location, with ones located near the center of the build plate having less porosity than the ones located away. Although these defects did not affect the tensile properties, they frequently observed to initiate fatigue cracks (the critical defects sizes were often in the range of a few tens of micrometers). Therefore, their sensitivity to location resulted in the location dependence of the fatigue behavior.</div></div>","PeriodicalId":72068,"journal":{"name":"Additive manufacturing letters","volume":"11 ","pages":"Article 100255"},"PeriodicalIF":4.2,"publicationDate":"2024-11-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142656286","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Scott C. Bozeman, O. Burkan Isgor, Julie D. Tucker
{"title":"Area-based composition predictions of materials fabricated using simultaneous wire-powder-directed energy deposition","authors":"Scott C. Bozeman, O. Burkan Isgor, Julie D. Tucker","doi":"10.1016/j.addlet.2024.100254","DOIUrl":"10.1016/j.addlet.2024.100254","url":null,"abstract":"<div><div>Functionally graded materials are an emergent method for designing components with programmable site-specific material properties. These materials are typically fabricated using metal additive manufacturing tools by simultaneously feeding multiple wire and/or powder feedstocks at various rates to achieve spatial composition change. The wire-powder-directed energy deposition (WP-DED) technique is of particular interest for many functionally graded material applications by balancing the low raw materials cost of wire with the high resolution of powder. However, feeding wire and powder are inherently different processes since all extruded wire enters the melt pool, while much of the blown powder is scattered, which makes determining the composition of the build challenging. In this study, we devise a simple area-based measurement method for estimating the composition of WP-DED structures. WP-DED single beads are printed using 309L stainless steel wire and commercially pure Fe powder at five wire feed rates (0.5, 0.75, 1.00, 1.25, 1.50 mm/mm) and five powder feed rates (2, 4, 6, 8, 10 rpm). Characteristic defects including interface gaps and macrosegregation (lack of mixing) tendencies are examined. High powder feed rates (8, 10 rpm) result in interface gaps at all wire feed rates, but smooth deposition and complete mixing is achieved at low powder feed rates, particularly with lower wire feed rates as well. The area-based composition measurement method is within ±20% of energy dispersive x-ray spectroscopy measurements for all samples, showing its effectiveness as a rapid composition estimate for WP-DED materials development.</div></div>","PeriodicalId":72068,"journal":{"name":"Additive manufacturing letters","volume":"11 ","pages":"Article 100254"},"PeriodicalIF":4.2,"publicationDate":"2024-11-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142656285","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Luke N. Carter , Victor M. Villapún , James Andrews , Thomas R.B. Grandjean , John Dardis , Sophie C. Cox
{"title":"Modelling process monitoring data in laser powder bed fusion: A pragmatic route to additive manufacturing quality assurance","authors":"Luke N. Carter , Victor M. Villapún , James Andrews , Thomas R.B. Grandjean , John Dardis , Sophie C. Cox","doi":"10.1016/j.addlet.2024.100252","DOIUrl":"10.1016/j.addlet.2024.100252","url":null,"abstract":"<div><div>Quality assurance remains a significant challenge for laser powder bed fusion and metal additive manufacturing. Despite system manufacturers offering process monitoring as a possible solution, datasets are large and cumbersome with practical use limited without direct comparative data. Model datasets would enable individual build validation, highlight deviations, and facilitate intelligent build planning whereby challenging features or build strategies could be pre-emptively assessed.</div><div>Herein a pragmatic approach has been developed to model process monitoring data from a commercial system using a relatively simple algorithm. Using a heuristic method, the algorithm response has been fitted to an experimental dataset to derive governing constants and their relationship to key process parameters. Predictability of constants and model fit has been shown to improve with increasing line energy up to a maximum R<sup>2</sup>=0.8. Algorithm variable trends, supported by corresponding sensitivity analysis, identified two different behavioural regimes. Under low linear energy density (<0.2J/mm) the cumulative spacetime proximity time-weight variable shows a low sensitivity index, characterised by a flat model response reflected in the experimental data. At higher energies (≥0.2J/mm) algorithm variables become more predictable, reflected in stabilising sensitivity indices, as measurements adopt a form characteristic of the cumulative spacetime proximity function.</div><div>Effectiveness has been demonstrated through presentation of experimental and model data. Refining the methodology to accommodate noise, geometry, and systematic behaviours are identified as key steps to future development. This feasibility study has laid the groundwork for a generalised predictive tool, capable of realising the quality assurance ambitions promised by laser powder-bed fusion process monitoring.</div></div>","PeriodicalId":72068,"journal":{"name":"Additive manufacturing letters","volume":"11 ","pages":"Article 100252"},"PeriodicalIF":4.2,"publicationDate":"2024-10-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142572438","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Anil Bastola , Luke Parry , Robyn Worsley , Nisar Ahmed , Edward Lester , Richard Hague , Christopher Tuck
{"title":"Drop-on-demand 3D printing of programable magnetic composites for soft robotics","authors":"Anil Bastola , Luke Parry , Robyn Worsley , Nisar Ahmed , Edward Lester , Richard Hague , Christopher Tuck","doi":"10.1016/j.addlet.2024.100250","DOIUrl":"10.1016/j.addlet.2024.100250","url":null,"abstract":"<div><div>Soft robotics have become increasingly popular as a versatile alternative to traditional robotics. Magnetic composite materials, which respond to external magnetic fields, have attracted significant interest in this field due to their programmable two-way actuation and shape-morphing capabilities. Additive manufacturing (AM)/3D printing allows for the incorporation of different functional composite materials to create active components for soft robotics. However, current AM methods have limitations, especially when it comes to printing smart composite materials with high functional material content. This is a key requirement for enhancing responsiveness to external stimuli. Commonly used AM methods for smart magnetic composites, such as direct ink writing (DIW), confront challenges in achieving discontinuous printing, and enabling multi-material control at the voxel level, while some AM techniques are not suitable for producing composite materials. To address these limitations, we employed high-viscosity drop-on-demand (DoD) jetting and developed programmable magnetic composites filled with micron-sized hard magnetic particles. This method bridges the gap between conventional ink-jetting and DIW, which require printing inks with viscosities at opposite ends of the spectrum. This high-viscosity DoD jetting enables continuous, discontinuous, and non-contact printing, making it a versatile and effective method for 3D printing functional magnetic composites even with micron-sized fillers. Furthermore, we demonstrated stable magnetic domain programming and two-way shape-morphing actuations of printed structures for soft robotics. In summary, our work highlights high-viscosity DoD jetting as a promising method for printing functional magnetic composites and other similar materials for a wide range of applications.</div></div>","PeriodicalId":72068,"journal":{"name":"Additive manufacturing letters","volume":"11 ","pages":"Article 100250"},"PeriodicalIF":4.2,"publicationDate":"2024-10-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142560560","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Ji-Yun Wang , Verner Soh , Pei Wang , Tzu-Ching Tsao , Ming-Wen Chu , Ming-Hao Lee , Zhongji Sun , Shao-Pu Tsai
{"title":"In-situ heating TEM observation of solidification cell evolutions in an Al-Fe alloy built by laser-powder bed fusion","authors":"Ji-Yun Wang , Verner Soh , Pei Wang , Tzu-Ching Tsao , Ming-Wen Chu , Ming-Hao Lee , Zhongji Sun , Shao-Pu Tsai","doi":"10.1016/j.addlet.2024.100251","DOIUrl":"10.1016/j.addlet.2024.100251","url":null,"abstract":"<div><div>Cellular structures (i.e., solidification cells) are a unique feature within alloys fabricated through rapid solidification, such as laser-powder bed fusion (L-PBF). Ever since the report of these structures’ beneficial effects on the material's mechanical properties, numerous studies have been devoted to the understanding of their formation mechanisms. Yet, the integrity and stability of the cellular structures are often less investigated, despite their significance on property interpretation and evolution. In this work, a stepwise <em>in-situ</em> heating transmission electron microscopy (TEM) experiment was performed on the exemplary LPBF-fabricated AlFeSiMoZr alloy. A critical threshold of 325 °C was identified, beyond which the cellular structures start to decompose in conjunction with precipitate coarsening. Preferred precipitate nucleation sites and their subsequent coarsening kinetics were determined and presented. Nanometer-sized crystalline embryos (3.81 ± 0.66 nm) were discovered within the cellular structure boundaries in their as-built condition, offering new insights on the precipitate formation and evolution at elevated temperatures.</div></div>","PeriodicalId":72068,"journal":{"name":"Additive manufacturing letters","volume":"11 ","pages":"Article 100251"},"PeriodicalIF":4.2,"publicationDate":"2024-10-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142578222","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
R. Joey Griffiths , David Garcia , Greg D. Hahn , Jim Lua , Nam Phan , Hang Z. Yu
{"title":"A non-melting additive approach to structural repair of aluminum aircraft fastener holes","authors":"R. Joey Griffiths , David Garcia , Greg D. Hahn , Jim Lua , Nam Phan , Hang Z. Yu","doi":"10.1016/j.addlet.2024.100249","DOIUrl":"10.1016/j.addlet.2024.100249","url":null,"abstract":"<div><div>The damage to fastener holes in aerospace aluminum structures presents significant challenges for aircraft durability, and conventional bushing methods for repairing oversized holes often fall short due to the lack of metallurgical bonding and limited edge distance availability. This study investigates additive friction stir deposition, a non-melting additive process, as a viable alternative for the structural repair of aerospace fastener holes. The repair process, demonstrated on AA7050 (Al-Zn-Mg-Cu-Zr) hole structures, involves filling oversized holes with new material and machining to restore the original hole size. The repaired hole coupons are defect-free and exhibit good fatigue performance under fully reversed tension-compression loading (<em>R</em> = -1). At a nominal stress amplitude of 123.5 MPa, the average number of cycles to failure is 12,666 for unrepaired baseline coupons and 17,372 for effectively repaired coupons. Restoring complex geometries without compromising fatigue performance has been difficult in aerospace applications; this study marks the first demonstration of additive repair that consistently outperforms the unrepaired baseline coupons. Notably, the result is achieved through a low-energy, cost-effective solution without the need for post-repair heat treatment. Except for a few outliers, the post-repair fatigue performance generally remains inferior to that of undamaged, pristine coupons, likely due to precipitate evolution in AA7050 caused by the thermomechanical processing nature of additive friction stir deposition. This evolution weakens the repair region and the adjacent base material, leading to faster crack initiation and growth compared to the properly aged base material, AA7050-T7451.</div></div>","PeriodicalId":72068,"journal":{"name":"Additive manufacturing letters","volume":"11 ","pages":"Article 100249"},"PeriodicalIF":4.2,"publicationDate":"2024-10-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142554068","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Clemens Johannes Müller , Klaus Büßenschütt , Alexander Schwedt , Johannes Henrich Schleifenbaum , Markus Sudmanns
{"title":"Enabling tailored microstructures by hybrid directed energy deposition processing of a nickel-based superalloy","authors":"Clemens Johannes Müller , Klaus Büßenschütt , Alexander Schwedt , Johannes Henrich Schleifenbaum , Markus Sudmanns","doi":"10.1016/j.addlet.2024.100248","DOIUrl":"10.1016/j.addlet.2024.100248","url":null,"abstract":"<div><div>The technological advances in additive manufacturing, particularly laser based directed energy deposition (DED), revolutionized the production of complex metal components. Despite this progress, the oriented heat flux and several reheating thermal cycles can induce a strongly textured microstructure, which induces an anisotropic mechanical behavior. In addition, considerable residual stresses typically require additional post-processing. Therefore, hybrid process chains for additive manufacturing (AM) are being developed, which aim at integrating conventional post-processing into the AM process. However, a detailed investigation of thermal and mechanical effects of such hybrid processes on the mechanical properties and their interrelation is lacking. In an experimental study, we explore the integration of thermal and mechanical processing steps within the DED process chain to locally tailor microstructures and mechanical properties. Through electron backscatter diffraction measurements, we demonstrate significant microstructural changes of DED-manufactured nickel-based superalloy samples using deep rolling and laser heat treatment. A mechanical surface deformation induces microstructural misorientation leading to an increase in hardness down to substantial depth of several hundred micrometers. Additionally, the targeted management of heat input during laser heat treatment results in different grain morphologies and sizes, affecting average microhardness within a significant depth. The results demonstrate the potential for microstructural tailoring using hybrid AM process chains, while a substantial sensitivity of the microstructure to thermal and mechanical load emphasizes the importance of a precise process control. This work provides an understanding of the process-microstructure-property relationship required for developing new process pathways in hybrid AM that integrate thermal and mechanical processes into DED manufacturing.</div></div>","PeriodicalId":72068,"journal":{"name":"Additive manufacturing letters","volume":"11 ","pages":"Article 100248"},"PeriodicalIF":4.2,"publicationDate":"2024-10-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142445366","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}