Journal of Analytical Chemistry最新文献_第4页

Using a Humate-Based Magnetic Sorbent and GC–MS for the Determination of Phenolic Xenoestrogens in Bottom Sediments 使用腐殖酸基磁性吸附剂和气相色谱-质谱法测定底层沉积物中的酚类异雌激素

IF 1 4区化学

Journal of Analytical Chemistry Pub Date : 2024-10-22 DOI: 10.1134/S1061934824700862

A. S. Gubin, P. T. Sukhanov, A. A. Kushnir, Kh. S. Shikhaliev, M. A. Potapov

{"title":"Using a Humate-Based Magnetic Sorbent and GC–MS for the Determination of Phenolic Xenoestrogens in Bottom Sediments","authors":"A. S. Gubin, P. T. Sukhanov, A. A. Kushnir, Kh. S. Shikhaliev, M. A. Potapov","doi":"10.1134/S1061934824700862","DOIUrl":"10.1134/S1061934824700862","url":null,"abstract":"A sorbent with magnetic properties, functionalized with humates, in combination with gas chromatography–mass spectrometry is proposed for the determination of phenolic xenoestrogens (ED) in bottom sediments. The octylphenol (OP), nonylphenol (NP), and bisphenol A (BPA) ED are chosen as test samples. Along with ED, the distribution of the naturally occurring estrogen, 17β-estradiol (ES), is studied. Sorption preconcentration is carried out under dynamic conditions: a sorbent weighing 0.5 g is placed in a borosilicate glass column, on both sides of which magnets are placed to immobilize the sorbent. The analytical characteristics of the determination method are established using model samples of bottom sediments selected in a background area with a minimal anthropogenic impact. The limit of quantification for ED is 30–60 ng/kg (dry weight). In analyzing real samples, the sensitivity of the method is reduced by 3–4 times due to matrix effects of the presence of petroleum products in waters. The ED content of bottom sediments at the site of wastewater discharge into the river Don near the city of Voronezh, as well as on the Black Sea coast of the Caucasus (area of the city of Tuapse and the village of Olginka) was monitored. The maximum concentrations of OP, NP, BPA, and ES in bottom sediments were found in the area of the port of Tuapse, where they were 5.7, 8.1, 6.2 and 0.9 µg/kg, respectively.","PeriodicalId":606,"journal":{"name":"Journal of Analytical Chemistry","volume":null,"pages":null},"PeriodicalIF":1.0,"publicationDate":"2024-10-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142518433","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

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Thermodynamic Modeling of the Composition of the Main Background Ions and Determination of Gas-Kinetic Temperature in the Normal (“Hot”) Inductively Coupled Plasma 正常（"热"）电感耦合等离子体中主要背景离子成分的热力学建模和气体动力学温度的测定

IF 1 4区化学

Journal of Analytical Chemistry Pub Date : 2024-10-22 DOI: 10.1134/S1061934824700825

A. A. Pupyshev, P. V. Kel’, M. Yu. Burylin, A. G. Abakumov, P. G. Abakumov

{"title":"Thermodynamic Modeling of the Composition of the Main Background Ions and Determination of Gas-Kinetic Temperature in the Normal (“Hot”) Inductively Coupled Plasma","authors":"A. A. Pupyshev, P. V. Kel’, M. Yu. Burylin, A. G. Abakumov, P. G. Abakumov","doi":"10.1134/S1061934824700825","DOIUrl":"10.1134/S1061934824700825","url":null,"abstract":"A possibility of studying effects of the main background ions formed by the main elements of inductively coupled plasma (H, N, O, and Ar) at the working parameters of the normal (“hot”) plasma mode by thermodynamic modeling is assessed. Such ions, responsible for the strongest spectral interferences in the mass spectra are always observed upon the injection of aqueous (“wet”) sample solutions into inductively coupled plasma mass spectrometers (ICP MS). The quantitative composition of the main background ions in an ICP MS is calculated as a function of plasma temperature in the temperature range from 3000 to 8000 K using thermodynamic modeling. The results of modeling were compared with the experimental data on the measured mass spectra of the main background ions and a high degree of correlation between the theoretical and experimental results was shown. The agreement between the results of calculations the experimental data validates the thermodynamic model of thermochemical processes in an ICP MS used and its applicability to subsequent calculations in fulfilling analytical tasks. A possibility of the unambiguous assessment of gas-kinetic plasma temperature is confirmed by comparing the theoretical and experimental mass spectra of the main ICP background ions in a normal mode. It was found that the calculated and experimental data on the concentration of only NO+ ions do not agree with the regularities noticed for the other background ions in the normal ICP mode.","PeriodicalId":606,"journal":{"name":"Journal of Analytical Chemistry","volume":null,"pages":null},"PeriodicalIF":1.0,"publicationDate":"2024-10-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142518393","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Application of Zeolites in High-Performance Liquid Chromatography 沸石在高效液相色谱中的应用

IF 1 4区化学

Journal of Analytical Chemistry Pub Date : 2024-10-22 DOI: 10.1134/S1061934824700722

V. D. Luzanova, N. B. Rozhmanova, S. N. Lanin, P. N. Nesterenko

{"title":"Application of Zeolites in High-Performance Liquid Chromatography","authors":"V. D. Luzanova, N. B. Rozhmanova, S. N. Lanin, P. N. Nesterenko","doi":"10.1134/S1061934824700722","DOIUrl":"10.1134/S1061934824700722","url":null,"abstract":"Inorganic zeolites, or microporous crystalline aluminosilicates, possess high porosity, well-developed specific surface area, uniform pores, and ion-exchange properties, which determine their molecular sieve and adsorption properties. The use of zeolites as catalysts, desiccants for solvents and gases, and selective adsorbents for the separation of low-molecular-weight compounds is widely known. Zeolites also serve extensively as packing materials for chromatographic columns in gas-adsorption chromatography. However, their application to high-performance liquid chromatography (HPLC) is less recognized. In HPLC, the retention of adsorbates depends not only on adsorption interactions but also on the molecular sieve effect in the micropores and kinetically selective effects. Additional interactions with the mobile phase components alter the thermodynamic parameters of the adsorbates interaction with the zeolite, decrease effective pore size, and hinder the diffusion of the separated compounds into the adsorbent’s pores. Despite these challenges, zeolites remain promising adsorbents due to their strictly determined pore size (dpore) and geometry, as well as their customizable polarities, which ensure high selectivity for the separation of low-molecular-weight compounds. The most promising zeolites for HPLC are wide-pore zeolites (dpore 0.6–0.8 nm) with 8, 10, 12, and 14-member ring channels. This review offers a concise overview of the classification, composition, and structure of zeolites and their impact on the adsorption properties of these adsorbents. Data on the use of zeolites in HPLC are also systematized.","PeriodicalId":606,"journal":{"name":"Journal of Analytical Chemistry","volume":null,"pages":null},"PeriodicalIF":1.0,"publicationDate":"2024-10-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142518398","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Online Preconcentration of Bisphenol A on a Magnetic Molecularly Imprinted Sorbent and its Determination in Natural Media 磁性分子印迹吸附剂在线预富集双酚 A 及其在天然介质中的测定

IF 1 4区化学

Journal of Analytical Chemistry Pub Date : 2024-10-22 DOI: 10.1134/S1061934824700850

A. S. Gubin, A. A. Kushnir, P. T. Sukhanov

{"title":"Online Preconcentration of Bisphenol A on a Magnetic Molecularly Imprinted Sorbent and its Determination in Natural Media","authors":"A. S. Gubin, A. A. Kushnir, P. T. Sukhanov","doi":"10.1134/S1061934824700850","DOIUrl":"10.1134/S1061934824700850","url":null,"abstract":"An original bench-scale installation based on the principles of online magnetic solid-phase extraction is developed. The setup includes a borosilicate glass column packed with Fe3O4@MIP-BPA, which is fixed with two neodymium magnets. Compared to using one magnet, a design with two magnets ensures the uniform distribution of the sorbent over the entire cross-section of the column. The highest concentration factors (EF = 3216) and the degree of desorption of bisphenol A (BPA) are achieved, respectively, at a volumetric solution flow rate (W) of 2.0 mL/min and with eluting BPA with methanol (W = 0.4 mL/min). The determination of BPA in concentrates from model media by GC−MS provides high sensitivity of the developed method for determining BPA. In analyzing model solutions prepared in distilled water, the limit of detection (LOD) is 0.3 ng/L. In analyzing river water, the LOD increases by approximately 2 times. In analyzing soils, LOD = 2.2 ng/kg dry weight. Soils, compared to water bodies, contain a larger number of interfering components; the sensitivity of the method is reduced by 7–8 times. Bottom sediments are even more contaminated; the LOD more than doubles compared to the determination of BPA in soils.","PeriodicalId":606,"journal":{"name":"Journal of Analytical Chemistry","volume":null,"pages":null},"PeriodicalIF":1.0,"publicationDate":"2024-10-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142518435","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

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Silagerm 8040-Based Planar Microfluidic Chips for Sampling and Sample Preparation in the Analysis of Gas Media 基于 Silagerm 8040 的平面微流控芯片，用于气体介质分析中的取样和样品制备

IF 1 4区化学

Journal of Analytical Chemistry Pub Date : 2024-10-22 DOI: 10.1134/S1061934824700758

A. E. Margaryan, I. A. Platonov, I. N. Kolesnichenko, E. A. Novikova, A. S. Karsunkina

引用次数: 0

Micellar Microextraction with Alkyl Polyglucosides for the Preconcentration and Spectrophotometric Determination of Phosphate Ions in Aqueous Media 用烷基多糖苷进行微孔微萃取以预浓缩和分光光度法测定水介质中的磷酸盐离子

IF 1 4区化学

Journal of Analytical Chemistry Pub Date : 2024-10-22 DOI: 10.1134/S1061934824700771

I. I. Timofeeva, M. A. Kochetkova, D. D. Dvoinykh, Ya. V. Safinskaya, E. A. Zubakina, A. V. Bulatov

{"title":"Micellar Microextraction with Alkyl Polyglucosides for the Preconcentration and Spectrophotometric Determination of Phosphate Ions in Aqueous Media","authors":"I. I. Timofeeva, M. A. Kochetkova, D. D. Dvoinykh, Ya. V. Safinskaya, E. A. Zubakina, A. V. Bulatov","doi":"10.1134/S1061934824700771","DOIUrl":"10.1134/S1061934824700771","url":null,"abstract":"A micellar microextraction technique has been developed for the preconcentration and spectrophotometric determination of phosphate ions in aqueous media. This method is based on the formation of a reduced form of molybdophosphoric heteropolyacid and its extraction from the aqueous phase into a supramolecular solvent. The supramolecular solvent phase is formed in situ by introducing an amphiphile and a coacervation agent into the acidic aqueous phase. The feasibility of using biodegradable alkyl polyglucoside (C8–C10) as an amphiphile and carboxylic acids as coacervation agents has been investigated. In the acidic medium required for the formation of the reduced form of molybdophosphoric heteropolyacid, the phase of the supramolecular solvent is separated. The maximum absorbance of the extract is achieved using pivalic acid as the coacervation agent. The procedure is characterized by the limit of detection (3σ) for phosphate ions 5 µg/L. The technique is environmentally friendly and does not require the use of expensive equipment.","PeriodicalId":606,"journal":{"name":"Journal of Analytical Chemistry","volume":null,"pages":null},"PeriodicalIF":1.0,"publicationDate":"2024-10-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142518359","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Voltammetric Determination of Hydroquinone in Water Samples Using Platinum Electrode Modified with Poly(Alizarin Red S) 使用聚茜素红 S 修饰的铂电极以伏安法测定水样中的对苯二酚

IF 1 4区化学

Journal of Analytical Chemistry Pub Date : 2024-10-22 DOI: 10.1134/S1061934824700898

M. Amayreh, M. Esaifan, M. K. Hourani

{"title":"Voltammetric Determination of Hydroquinone in Water Samples Using Platinum Electrode Modified with Poly(Alizarin Red S)","authors":"M. Amayreh, M. Esaifan, M. K. Hourani","doi":"10.1134/S1061934824700898","DOIUrl":"10.1134/S1061934824700898","url":null,"abstract":"The presented work focused on the preparation of a voltammetric sensor for hydroquinone (HQ) determination using a polycrystalline platinum electrode modified with Alizarin Red S (ARS). The electrode was prepared by electropolymerization of ARS on a platinum electrode through the application of 100 cyclic voltammetric segments between –0.4 and 1.2 V against Ag/AgCl (quasi-reference electrode). The modified poly (ARS)-Pt electrode was characterized in terms of stability and cyclic voltammetric behavior as a sensor for HQ in aqueous media. The modified electrode showed excellent stability and higher current than the unmodified electrode for the electrooxidation of HQ. Thus, the oxidation of HQ at poly (ARS)-Pt electrode exhibits notable electrocatalytic performance. The limit of detection is 0.16 µM, and the standard curve exhibits a linear relationship over the range from 0.25 to 15 µM (R2 = 0.999). Investigation of the response to some potential interferences indicated that the electrode is unresponsive to Na+, K+, Mg2+, Ca2+, Zn2+, Mn2+, Mo2+, Co2+, Bi2+, Cd2+, Ni2+, Al3+, ({text{NO}}_{3}^{ - }), ({text{SO}}_{4}^{{2 - }}), Cl–, phenol and resorcinol, but shows marginal change towards Hg2+ and Cu2+. Recovery tests indicated recovery values between 97.0% and 100.81% when analyzing real samples at the modified electrode.","PeriodicalId":606,"journal":{"name":"Journal of Analytical Chemistry","volume":null,"pages":null},"PeriodicalIF":1.0,"publicationDate":"2024-10-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142518437","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Interaction of Vanadium(V) with 4-(2',3',4'-Trihydroxyphenyl)-3-Nitro-5-Sulfoazobenzene in the Presence of Cationic Surfactants 阳离子表面活性剂存在时钒（V）与 4-(2',3',4'-三羟基苯基)-3-硝基-5-磺偶氮苯的相互作用

IF 1 4区化学

Journal of Analytical Chemistry Pub Date : 2024-10-22 DOI: 10.1134/S1061934824700801

V. I. Mardanova, Kh. D. Nagiev, F. M. Chyragov

{"title":"Interaction of Vanadium(V) with 4-(2',3',4'-Trihydroxyphenyl)-3-Nitro-5-Sulfoazobenzene in the Presence of Cationic Surfactants","authors":"V. I. Mardanova, Kh. D. Nagiev, F. M. Chyragov","doi":"10.1134/S1061934824700801","DOIUrl":"10.1134/S1061934824700801","url":null,"abstract":"Complex formation of vanadium(V) with 4-(2',3',4'-trihydroxyphenyl)-3-nitro-5-sulfoazobenzene (R) in the presence of cationic surfactants (CS), cetylpyridinium chloride (CPCl), cetylpyridinium bromide (CPBr), and cetyltrimethylammonium bromide (CTMABr), is studied. Vanadium(V) and R form a colored complex at a component ratio of 1 : 2 and pH of 5.0–5.5. The absorbance maximum of the complex is at 449 nm, while the reagent under these conditions absorbs light at 395 nm. In the presence of cationic surfactants, mixed-ligand complexes with a component ratio of V(V) : R : CS = 1 : 2 : 2 are formed, which results in a bathochromic shift of the absorbance maximum. Additionally, the pH value for the maximum complex formation shifts to a more acidic medium compared to the homoligand V(V)–R complex. The absorbance of the V(V) : R : CPCl, V(V): R : CPBr, and V(V) : R : CTMABr complexes is maximal at 457, 461, and 466 nm, respectively. The yield of these complexes is the highest at pH of 3.5–4.0 for VV(V) : R : CPCl and V(V): R : CPBr, and at a pH of 2.5–3.0 for V(V) : R : CTMABr. The formation of both homoligand and mixed-ligand vanadium(V) complexes depends on the reaction time, temperature, and concentrations of the reacting components. The determined stability constants indicate the high stability of the resulting mixed-ligand complexes. The specific conductivity of the complexes under the optimal conditions of complex formation was determined using conductometric titration. Calibration curves for the determination of vanadium(V) as homoligand and mixed-ligand complexes are linear. The effect of foreign ions and masking agents on the determination of V(V) as homoligand and mixed-ligand complexes was analyzed; it was shown that the presence of cationic surfactants significantly increases the selectivity of the reaction. An analysis of water samples from Lake Khanbulan, Lankaran District, Azerbaijan Republic using the developed procedure showed the presence of small amounts of vanadium(V).","PeriodicalId":606,"journal":{"name":"Journal of Analytical Chemistry","volume":null,"pages":null},"PeriodicalIF":1.0,"publicationDate":"2024-10-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142518363","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0

Magnetic Solid-Phase Extraction with Dispersion of Magnetic Hypercrosslinked Polystyrene by Carbon Dioxide for the Extraction of Amphenicols from Honey and Milk in Their Determination by HPLC–MS/MS 用二氧化碳分散磁性超交联聚苯乙烯的磁性固相萃取技术萃取蜂蜜和牛奶中的安非他明醇，并用 HPLC-MS/MS 进行测定

IF 1 4区化学

Journal of Analytical Chemistry Pub Date : 2024-09-03 DOI: 10.1134/S1061934824700655

N. O. Goncharov, V. V. Tolmacheva, T. V. Lazarevich, A. O. Melekhin, I. D. Puryskin, V. V. Apyari, S. G. Dmitrienko

{"title":"Magnetic Solid-Phase Extraction with Dispersion of Magnetic Hypercrosslinked Polystyrene by Carbon Dioxide for the Extraction of Amphenicols from Honey and Milk in Their Determination by HPLC–MS/MS","authors":"N. O. Goncharov, V. V. Tolmacheva, T. V. Lazarevich, A. O. Melekhin, I. D. Puryskin, V. V. Apyari, S. G. Dmitrienko","doi":"10.1134/S1061934824700655","DOIUrl":"10.1134/S1061934824700655","url":null,"abstract":"A magnetic solid-phase extraction method with the dispersion of magnetic hypercrosslinked polystyrene (MHCPS) by carbon dioxide is proposed for the extraction and preconcentration of amphenicols (chloramphenicol, florfenicol, and thiamphenicol) from honey and milk before their determination by HPLC–MS/MS. Effervescent tablets, consisting of sodium bicarbonate, citric acid, and MHCPS in the case of honey and sodium bicarbonate and MHCPS in the case of milk, were used. The conditions for obtaining tablets were selected (the amount and ratio of the acid, base, and MHCPS in the composition of a tablet and its mass), ensuring the quantitative release of amphenicols. Procedures for the determination of amphenicols in honey and milk with the dispersion of the sorbent by carbon dioxide and the subsequent determination of the compounds by HPLC–MS/MS are developed. The limits of detection are 0.3–1 and 0.02–0.05 μg/kg for honey and milk, respectively.","PeriodicalId":606,"journal":{"name":"Journal of Analytical Chemistry","volume":null,"pages":null},"PeriodicalIF":1.0,"publicationDate":"2024-09-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142177614","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

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Azolotriazine-Based Fluorescent Test Systems for the Field Diagnosis of Endometritis in Cows 基于偶氮三嗪的荧光检测系统用于奶牛子宫内膜炎的现场诊断

IF 1 4区化学

Journal of Analytical Chemistry Pub Date : 2024-09-03 DOI: 10.1134/S1061934824700588

T. A. Kuchmenko, D. Yu. Vandyshev, V. N. Skorikov, R. U. Umarkhanov, Kh. S. Shikhaliev, P. V. Seredin, V. V. Yagov, V. I. Mikhalev

{"title":"Azolotriazine-Based Fluorescent Test Systems for the Field Diagnosis of Endometritis in Cows","authors":"T. A. Kuchmenko, D. Yu. Vandyshev, V. N. Skorikov, R. U. Umarkhanov, Kh. S. Shikhaliev, P. V. Seredin, V. V. Yagov, V. I. Mikhalev","doi":"10.1134/S1061934824700588","DOIUrl":"10.1134/S1061934824700588","url":null,"abstract":"The results of an experiment assessing the applicability of solutions of 6-oxo-2-phenylimidazo[1,2-b]pyrido[4,3-e][1,2,4]triazine-7(6H)-yl)acetic acid on plates and cellulose substrates for detecting excessive levels of volatile organic compounds associated with endometritis inflammation relative to biologically normal levels are considered. The fluorescent properties of the dye are studied using gynecological mucus from cows collected in various periods (pre- and post-partum) and nasal mucus from newborn calves. The test system responses were compared with clinically established diagnoses and the results of a microbiological study. An evaluation of the test systems revealed a false positive rate of no more than 11% and a false negative rate of 2%. Other characteristics, such as specificity, accuracy, and precision of the test systems based on 6-oxo-2-phenylimidazo[1,2-b]pyrido[4,3-e][1,2,4]triazine-7(6H)-yl)acetic acid were also assessed. The potential application of this fluorophore to the rapid on-site diagnosis of endometritis inflammation in cows is considered promising based on these findings.","PeriodicalId":606,"journal":{"name":"Journal of Analytical Chemistry","volume":null,"pages":null},"PeriodicalIF":1.0,"publicationDate":"2024-09-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142177605","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

引用次数: 0