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Catalytic Hydrogenation of Carbon Dioxide as a Method to Produce Valuable Chemicals 将二氧化碳催化氢化作为生产有价值化学品的一种方法
IF 0.7
Catalysis in Industry Pub Date : 2024-05-13 DOI: 10.1134/S2070050424010045
I. A. Makaryan, I. V. Sedov, V. I. Savchenko
{"title":"Catalytic Hydrogenation of Carbon Dioxide as a Method to Produce Valuable Chemicals","authors":"I. A. Makaryan,&nbsp;I. V. Sedov,&nbsp;V. I. Savchenko","doi":"10.1134/S2070050424010045","DOIUrl":"10.1134/S2070050424010045","url":null,"abstract":"<p>The aim of this review is to summarize and comparatively analyze recent reports on studying carbon dioxide conversion to methanol, dimethyl ether, and C<sub>2+</sub> hydrocarbons, in particular, olefins, by catalytic hydrogenation. It is shown that the main approaches to providing high activity and selectivity of these processes are the targeted design of catalysts and the selection of conditions for hydrogenation processes, in particular, the use of supercritical CO<sub>2</sub> and procedures that are alternative to conventional physicochemical methods for CO<sub>2</sub> activation (electrocatalysis, photocatalysis).</p>","PeriodicalId":507,"journal":{"name":"Catalysis in Industry","volume":"16 1","pages":"14 - 38"},"PeriodicalIF":0.7,"publicationDate":"2024-05-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140939636","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Preparing Zeolite-Containing Adsorbents with Different Kaolins for the Efficient Drying and Purification of Natural Gas 用不同的高岭土制备含沸石的吸附剂以高效干燥和净化天然气
IF 0.7
Catalysis in Industry Pub Date : 2024-05-13 DOI: 10.1134/S2070050424010021
I. Kh. Allaguzin, O. S. Travkina, B. I. Kutepov, D. Sh. Sabirov
{"title":"Preparing Zeolite-Containing Adsorbents with Different Kaolins for the Efficient Drying and Purification of Natural Gas","authors":"I. Kh. Allaguzin,&nbsp;O. S. Travkina,&nbsp;B. I. Kutepov,&nbsp;D. Sh. Sabirov","doi":"10.1134/S2070050424010021","DOIUrl":"10.1134/S2070050424010021","url":null,"abstract":"<p>An adsorbent consisting of a granular NаX zeolite with a hierarchical porous structure and a high degree of crystallinity and phase purity is used for the efficient drying and purification of natural and associated gases from H<sub>2</sub>S. The possibility of using KZhV, MP KAKh, KCh-2, and KR-2 kaolins produced in Russia as temporary binder materials during its production is studied. It is found that KZhV and MP KAKh kaolins do not require additional treatment to prepare such an adsorbent. KCh-2 and KR-2 kaolins require additional dispersion.</p>","PeriodicalId":507,"journal":{"name":"Catalysis in Industry","volume":"16 1","pages":"1 - 6"},"PeriodicalIF":0.7,"publicationDate":"2024-05-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140939738","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Bifunctional Cobalt Catalysts for the Fischer–Tropsch Synthesis of Low-Pour-Point Diesel Fuel: From Development to Implementation: 2. Optimization of the Catalyst Component Composition 用于费托合成低倾点柴油的双功能钴催化剂：从开发到实施：2. 催化剂组分的优化
IF 0.7
Catalysis in Industry Pub Date : 2023-12-26 DOI: 10.1134/S2070050423040128
R. E. Yakovenko, V. G. Bakun, I. N. Zubkov, O. P. Papeta, A. N. Saliev, A. P. Savost’yanov
{"title":"Bifunctional Cobalt Catalysts for the Fischer–Tropsch Synthesis of Low-Pour-Point Diesel Fuel: From Development to Implementation: 2. Optimization of the Catalyst Component Composition","authors":"R. E. Yakovenko,&nbsp;V. G. Bakun,&nbsp;I. N. Zubkov,&nbsp;O. P. Papeta,&nbsp;A. N. Saliev,&nbsp;A. P. Savost’yanov","doi":"10.1134/S2070050423040128","DOIUrl":"10.1134/S2070050423040128","url":null,"abstract":"<p>The effect of the content of metallic (Co–Al<sub>2</sub>O<sub>3</sub>/SiO<sub>2</sub> catalyst) and acidic components (ZSM-5 zeolite in H-form) on the properties of a bifunctional catalyst for the integrated synthesis of low-pour-point diesel fuel by the Fischer–Tropsch method has been studied. The catalysts in the form of a composite mixture with a binder (boehmite) have been characterized by XRD, BET, and TPR methods. The tests are conducted in a fixed-bed flow reactor at a pressure of 2.0 MPa, a temperature of 240°C, and a gas space velocity of 1000 h<sup>–1</sup>. The activity and selectivity of catalysts and the fractional and hydrocarbon compositions of products as a function of the ratio of components have been compared. It has been found that the synthesis productivity with respect to С<sub>5+</sub> hydrocarbons and selectivity to products of the С<sub>11</sub>–C<sub>18</sub> diesel fraction with a high content of isomeric products correlate with the ratio of metallic and acidic components in the catalyst composition. The catalyst recommended for use in diesel fuel production has a composition with a ratio of metallic and acidic components of 1.17.</p>","PeriodicalId":507,"journal":{"name":"Catalysis in Industry","volume":"15 4","pages":"357 - 366"},"PeriodicalIF":0.7,"publicationDate":"2023-12-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139053601","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Selective Catalytic Hydrodebromination of 2,3,4,5-Tetrabromothiophene with Hydrogen on a Palladium Catalyst 钯催化剂上 2,3,4,5-四溴噻吩与氢的选择性催化加氢脱溴反应
IF 0.7
Catalysis in Industry Pub Date : 2023-12-26 DOI: 10.1134/S2070050423040025
N. A. Alekseeva, V. V. Eremina, S. V. Sysolyatin, I. A. Shchurova
{"title":"Selective Catalytic Hydrodebromination of 2,3,4,5-Tetrabromothiophene with Hydrogen on a Palladium Catalyst","authors":"N. A. Alekseeva,&nbsp;V. V. Eremina,&nbsp;S. V. Sysolyatin,&nbsp;I. A. Shchurova","doi":"10.1134/S2070050423040025","DOIUrl":"10.1134/S2070050423040025","url":null,"abstract":"<p>A way of hydrodebrominating 2,3,4,5-tetrabromothiophene (<b>1</b>) to 3,4-dibromothiophene (<b>2</b>) on a 5% Pd/Sibunit catalyst is proposed. The effect of solvent, alkaline agent, temperature, and concentration of <b>1</b> on the yield of <b>2</b> is studied. The optimum conditions are catalyst : substrate mass ratio, 1:10; temperature, 80°С; H<sub>2</sub> pressure, 0.7 MPa; solvent, dimethylformamide; alkaline agent, triethylamine in amounts of 2.2 mol per 1 mol of substrate <b>1</b>. The yield of <b>2</b> is 97.5% in this case. The catalyst can be reused in at least 15 cycles with high yields of <b>2</b>. The new approach appears to be highly productive with little waste, compared to the conventional chemical reduction of <b>1</b> with zinc in CH<sub>3</sub>COOH.</p>","PeriodicalId":507,"journal":{"name":"Catalysis in Industry","volume":"15 4","pages":"404 - 409"},"PeriodicalIF":0.7,"publicationDate":"2023-12-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139053780","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of Water-Soluble Polymers on the Dynamics of Carbon Dioxide Sorption by Lime-Based Sorbents 水溶性聚合物对石灰基吸附剂吸附二氧化碳动力学的影响
IF 0.7
Catalysis in Industry Pub Date : 2023-12-26 DOI: 10.1134/S2070050423040062
V. S. Derevshchikov, O. Yu. Selyutina
{"title":"Effect of Water-Soluble Polymers on the Dynamics of Carbon Dioxide Sorption by Lime-Based Sorbents","authors":"V. S. Derevshchikov,&nbsp;O. Yu. Selyutina","doi":"10.1134/S2070050423040062","DOIUrl":"10.1134/S2070050423040062","url":null,"abstract":"<p>This study concerns the effect of water-soluble polymers with different structures on the sorption properties of unregenerable lime-based sorbents of carbon dioxide. It is shown that introducing water-soluble polymers into the composition of sorbents can either prolong or shorten the periods of their protective effect. To explain these findings, the porous structure of sorbents is studied, the transport of carbon dioxide is modeled using molecular dynamics, and coefficients of the diffusion of СО<sub>2</sub> in water–polymer solutions are calculated. Modelling results correlate with data from sorption experiments: a stronger dynamic sorption capacity is obtained for a sorbent when a water–polymer medium with a greater coefficient of СО<sub>2</sub> diffusion is added. These results can be used to optimize systems for separating carbon dioxide from gaseous mixtures and intensify mass transfer in systems for the photo- and electrocatalytic conversion of СО<sub>2</sub> into useful products.</p>","PeriodicalId":507,"journal":{"name":"Catalysis in Industry","volume":"15 4","pages":"325 - 332"},"PeriodicalIF":0.7,"publicationDate":"2023-12-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139053867","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Catalysis in the Automotive Industry: Mutual Development and State-of-the-Art 汽车工业中的催化作用：共同发展与技术现状
IF 0.7
Catalysis in Industry Pub Date : 2023-12-26 DOI: 10.1134/S2070050423040050
S. P. Denisov, E. A. Alikin, E. O. Baksheev, V. N. Rychkov
{"title":"Catalysis in the Automotive Industry: Mutual Development and State-of-the-Art","authors":"S. P. Denisov,&nbsp;E. A. Alikin,&nbsp;E. O. Baksheev,&nbsp;V. N. Rychkov","doi":"10.1134/S2070050423040050","DOIUrl":"10.1134/S2070050423040050","url":null,"abstract":"<p>In this paper, the development of catalytic technologies used aboard a vehicle for purifying exhaust gases is estimated and forecasted. According to forecasts, in the next decade, the total production of vehicles will exceed 1 billion units and 75% of them will be equipped with internal combustion engines, which should necessarily be accompanied by an exhaust gas purification system. The development of catalytic technologies for purifying vehicle exhaust gases is mutually stimulated by the tightening of environmental standards and improving the internal combustion engines. For example, to date, the European standards have gone from Euro 1 to Euro 6d. The introduction of Euro 7 standards in Europe and the introduction of their counterparts in a number of countries by 2025 is planned. In addition, this paper discusses the concepts of systems that purify the exhaust gases of gasoline and diesel engines to meet the Euro 7 standards.</p>","PeriodicalId":507,"journal":{"name":"Catalysis in Industry","volume":"15 4","pages":"443 - 449"},"PeriodicalIF":0.7,"publicationDate":"2023-12-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139053511","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Transformation of Amorphous Aluminum Oxide in the Catalytic Dehydration of Aromatic Alcohol 无定形氧化铝在芳香族酒精催化脱水过程中的转变
IF 0.7
Catalysis in Industry Pub Date : 2023-12-26 DOI: 10.1134/S2070050423040049
A. V. Boretskaya, M. I. Farid, S. R. Egorova, A. A. Lamberov
{"title":"Transformation of Amorphous Aluminum Oxide in the Catalytic Dehydration of Aromatic Alcohol","authors":"A. V. Boretskaya,&nbsp;M. I. Farid,&nbsp;S. R. Egorova,&nbsp;A. A. Lamberov","doi":"10.1134/S2070050423040049","DOIUrl":"10.1134/S2070050423040049","url":null,"abstract":"<p>The widespread use of aluminum oxides to synthesize heterogeneous catalysts in petroleum chemistry and oil refining makes it necessary to determine the factors that influence the efficiency of catalytic systems. However, there have been no studies on the effect of amorphous aluminum oxide in aluminum oxide catalysts on the characteristics of a catalytic reaction. The amount of amorphous aluminum hydroxides and oxides is generally not certified, but they can considerably worsen the performance of a catalyst. Amorphous aluminum oxide samples obtained from two different precursors are studied in this work via X-ray phase analysis, low-temperature nitrogen adsorption, electron microscopy, and thermally programmed desorption of ammonia. The catalytic properties of the samples are studied in the vapor phase dehydration of 1-phenylethanol to styrene. It is shown for the first time that the transformation of amorphous aluminum oxide during the catalytic reaction lowers the conversion of alcohol from 84 (for a fresh catalyst) to 64% (for a regenerated sample). The crystallization of amorphous aluminum oxide through high temperature treatment contributes to an increase in catalytic indicators. However, they do not reach the required values because of a strong drop in the textural characteristics and acidic properties of an aluminum oxide surface.</p>","PeriodicalId":507,"journal":{"name":"Catalysis in Industry","volume":"15 4","pages":"387 - 396"},"PeriodicalIF":0.7,"publicationDate":"2023-12-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139053505","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of the Structure and Acidity of Zeolites on the Synthesis of Solketal from Glycerol and Acetone 沸石的结构和酸度对甘油和丙酮合成 Solketal 的影响
IF 0.7
Catalysis in Industry Pub Date : 2023-12-26 DOI: 10.1134/S207005042304013X
O. N. Kovalenko, I. I. Simentsova, V. N. Panchenko, M. N. Timofeeva
{"title":"Effect of the Structure and Acidity of Zeolites on the Synthesis of Solketal from Glycerol and Acetone","authors":"O. N. Kovalenko,&nbsp;I. I. Simentsova,&nbsp;V. N. Panchenko,&nbsp;M. N. Timofeeva","doi":"10.1134/S207005042304013X","DOIUrl":"10.1134/S207005042304013X","url":null,"abstract":"<p>A study is performed to establish the main factors that allow regulation of the activity and selectivity of the synthesis of solketal from glycerol and acetone, and the acidic and catalytic properties of mordenite zeolites (MOR, SiO<sub>2</sub> : Al<sub>2</sub>O<sub>3</sub> = 29.2) and faujasite (FAU, SiO<sub>2</sub> : Al<sub>2</sub>O<sub>3</sub> = 14.9; 97 and 810). The reaction is studied in a methanol solution at an acetone : glycerol molar ratio of 2.5 and a temperature of 25–50°C. Using zeolites, the main product is solketal with a selectivity of 88.1–94.7%. It is shown that the main factors determining the conversion of glycerol and the yield of solketal are the accessibility of the reagents to active sites, the number and strength of acid sites, and their resistance to the toxic action of water molecules that form during the reaction.</p>","PeriodicalId":507,"journal":{"name":"Catalysis in Industry","volume":"15 4","pages":"410 - 419"},"PeriodicalIF":0.7,"publicationDate":"2023-12-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139053565","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of the Nature of Supports and the Degree of Palladium Dispersion on the Catalyst Activity and Selectivity in the Sunflower Oil Hydrogenation Reaction 载体性质和钯分散程度对葵花籽油加氢反应中催化剂活性和选择性的影响
IF 0.7
Catalysis in Industry Pub Date : 2023-12-26 DOI: 10.1134/S2070050423040098
A. V. Romanenko, P. A. Simonov, M. A. Kulagina, S. I. Udalova, I. N. Voropaev, G. A. Bukhtiyarova
{"title":"Effect of the Nature of Supports and the Degree of Palladium Dispersion on the Catalyst Activity and Selectivity in the Sunflower Oil Hydrogenation Reaction","authors":"A. V. Romanenko,&nbsp;P. A. Simonov,&nbsp;M. A. Kulagina,&nbsp;S. I. Udalova,&nbsp;I. N. Voropaev,&nbsp;G. A. Bukhtiyarova","doi":"10.1134/S2070050423040098","DOIUrl":"10.1134/S2070050423040098","url":null,"abstract":"<p>Results of studying the Pd/C and Pd/O powder catalysts synthesized by the deposition of 0.5 and 1.0 wt % Pd on carbon materials (Sibunit 159k, thermal carbon black T-900, Vulcan XC<b>-</b>72R) and oxide supports (Ox: γ-Al<sub>2</sub>O<sub>3</sub>, Cr<sub>2</sub>O<sub>3</sub>, Ga<sub>2</sub>O<sub>3</sub>, TiO<sub>2</sub>, Ta<sub>2</sub>O<sub>5</sub>, and V<sub>2</sub>O<sub>5</sub>, diatomaceous earth FW-70) and their catalytic properties in the partial hydrogenation of sunflower oil were described. Using a Parr fixed-bed reactor, comparative tests of the catalysts in the kinetic mode conducted to determine their activity (SCA, <i>V</i><sub>0</sub>) and <i>trans</i>-isomerization selectivity parameters (<i>S</i><sub>tr</sub>). The effect of the average particle size of supported palladium (<i>d</i><sub>CO</sub>) on these parameters in a wide range of <i>d</i><sub>CO</sub> values was discussed.</p>","PeriodicalId":507,"journal":{"name":"Catalysis in Industry","volume":"15 4","pages":"374 - 386"},"PeriodicalIF":0.7,"publicationDate":"2023-12-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139053782","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Silica- and Alumina-Supported Sulfated Zirconia Catalysts for Hexane Isomerization: Effect of the Support Nature 用于己烷异构化的二氧化硅和氧化铝支撑硫酸化氧化锆催化剂：支撑性质的影响
IF 0.7
Catalysis in Industry Pub Date : 2023-12-26 DOI: 10.1134/S2070050423040116
M. D. Smolikov, L. I. Bikmetova, K. V. Kazantsev, V. A. Skurenok, S. S. Yablokova, A. V. Lavrenov
{"title":"Silica- and Alumina-Supported Sulfated Zirconia Catalysts for Hexane Isomerization: Effect of the Support Nature","authors":"M. D. Smolikov,&nbsp;L. I. Bikmetova,&nbsp;K. V. Kazantsev,&nbsp;V. A. Skurenok,&nbsp;S. S. Yablokova,&nbsp;A. V. Lavrenov","doi":"10.1134/S2070050423040116","DOIUrl":"10.1134/S2070050423040116","url":null,"abstract":"<p>The effect of the support nature on the hexane isomerization reaction parameters for SiO<sub>2</sub>- and Al<sub>2</sub>O<sub>3</sub>-supported sulfated zirconia catalysts with different textural characteristics has been studied. It has been shown that a higher hexane conversion is achieved in the presence of sulfated zirconia catalysts supported on aluminas. Using IR spectroscopy of adsorbed CO, it has been found that, in the Al<sub>2</sub>O<sub>3</sub>-supported catalysts, the concentration of Brønsted acid sites (BAS) characterized by adsorbed CO with an absorption band at 2170 cm<sup>–1</sup> and strong Lewis acid sites (LAS) characterized by adsorbed CO with absorption bands at 2210 and 2224 cm<sup>–1</sup> is higher than that in the SiO<sub>2</sub>-supported catalysts. In the Al<sub>2</sub>O<sub>3</sub>-supported catalysts with different textural characteristics, an increase in the contribution of LAS to the total acidity leads to a significant increase in the high-octane 2,2-dimethylbutane yield and the hexane isomerization depth.</p>","PeriodicalId":507,"journal":{"name":"Catalysis in Industry","volume":"15 4","pages":"350 - 356"},"PeriodicalIF":0.7,"publicationDate":"2023-12-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139053781","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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