J. Praena, B. Fernández, M. Macías, I. Porras, María Pedrosa-Rivera, Hanna Koivunoro, M. Sabaté-Gilarte, F. Arias de Saavedra
{"title":"Measurement of the 33S(n,α)30Si Thermal Cross-Section with Slow Neutrons at ILL","authors":"J. Praena, B. Fernández, M. Macías, I. Porras, María Pedrosa-Rivera, Hanna Koivunoro, M. Sabaté-Gilarte, F. Arias de Saavedra","doi":"10.3390/qubs9030027","DOIUrl":"https://doi.org/10.3390/qubs9030027","url":null,"abstract":"This work is focused on an accurate experimental determination of the thermal 33S(n,α)30Si cross-section. This cross-section is a critical parameter for the potential use of 33S as a cooperative target in boron neutron capture therapy or to understand its role in the stellar nucleosynthesis of 36S. At present, there are large discrepancies in this experimental value; therefore, in this work we measured it relative to the 10B(n,α)7Li standard cross-section at the high flux reactor of the Institut Laue-Langevin. The experimental setup was based on a double-sided silicon strip detector. Two 33S samples were used. One 10B sample was used as reference. Particular attention was taken to the characterization of the mass thickness of the samples before and after the experiment because of the high volatility of 33S. Such work was already published in a dedicated paper. A cross-check of the 10B sample was carried out with the neutron flux monitor at the n_TOF-CERN facility. The obtained cross-section of (280 ± 33) mb is significantly higher than the existing data.","PeriodicalId":31879,"journal":{"name":"Quantum Beam Science","volume":"9 3","pages":"27-27"},"PeriodicalIF":0.0,"publicationDate":"2025-09-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.mdpi.com/2412-382X/9/3/27/pdf?version=1758507290","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"147330949","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
May Sweet, K. Mishima, Masafumi Harada, Keisuke Kurita, Hiroshi Iikura, S. Tasaki, Norio Kikuchi
{"title":"Simulation Study on Dose and LET of Neutron Irradiation for Biological Experiments Using Spallation, Reactor, and Compact Neutron Sources","authors":"May Sweet, K. Mishima, Masafumi Harada, Keisuke Kurita, Hiroshi Iikura, S. Tasaki, Norio Kikuchi","doi":"10.3390/qubs9020011","DOIUrl":"https://doi.org/10.3390/qubs9020011","url":null,"abstract":"Neutron beams, being electrically neutral and highly penetrating, offer unique advantages for the irradiation of biological species such as plants, seeds, and microorganisms. We comprehensively investigated the potential of neutron irradiation for inducing genetic mutations by using simulations of spallation, reactor, and compact neutron sources based on J-PARC BL10, the JRR-3 TNRF, and KUANS. We analyzed neutron flux, energy deposition rates, and Linear Energy Transfer (LET) distributions. The KUANS simulation demonstrated the highest dose rate of 17 Gy/h, significantly surpassing that obtained at BL10, due to the large solid angle achieved with optimal sample placement. The findings highlight KUANS’s suitability for efficiently inducing specific genetic mutations and neutron breeding, particularly for inducing targeted mutations in biological samples, also on account of its LET range of 20–70 keV/μm. Our results emphasize the importance of choosing neutron sources based on LET requirements to maximize mutation induction efficiency. This research study shows the potential of compact neutron sources such as KUANS for effective biological irradiation and neutron breeding, offering a viable alternative to larger facilities. The neutron filters used at BL10 and the TNRF effectively exclude low-energy neutrons while keeping the high-LET component. The neutron capture reaction, 14N(n,p)14C, was found to be the main dose contributor under thermal neutron-dominated conditions.","PeriodicalId":31879,"journal":{"name":"Quantum Beam Science","volume":"9 2","pages":"11-11"},"PeriodicalIF":0.0,"publicationDate":"2025-04-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.mdpi.com/2412-382X/9/2/11/pdf?version=1744119255","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"147330908","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
L. Giuffrida, V. Istokskaia, A. Picciotto, V. Kantarelou, M. Barozzi, R. Dell`Anna, M. Divoký, O. Denk, D. Giubertoni, F. Grepl, A. Hadjikyriacou, M. Hanus, J. Krása, M. Kucharik, T. Levato, P. Navratil, J. Pilar, F. Schillaci, S. Stanček, M. Tosca, M. Tryus, A. Velyhan, A. Lucianetti, T. Mocek, D. Margarone
{"title":"A Platform for Laser-Driven Ion Sources Generated with Nanosecond Laser Pulses in the Intensity Range of 1013–1015 W/cm2","authors":"L. Giuffrida, V. Istokskaia, A. Picciotto, V. Kantarelou, M. Barozzi, R. Dell`Anna, M. Divoký, O. Denk, D. Giubertoni, F. Grepl, A. Hadjikyriacou, M. Hanus, J. Krása, M. Kucharik, T. Levato, P. Navratil, J. Pilar, F. Schillaci, S. Stanček, M. Tosca, M. Tryus, A. Velyhan, A. Lucianetti, T. Mocek, D. Margarone","doi":"10.3390/qubs8010005","DOIUrl":"https://doi.org/10.3390/qubs8010005","url":null,"abstract":"An experimental platform for laser-driven ion (sub-MeV) acceleration and potential applications was commissioned at the HiLASE laser facility. The auxiliary beam of the Bivoj laser system operating at a GW level peak power (~10 J in 5–10 ns) and 1–10 Hz repetition rate enabled a stable production of high-current ion beams of multiple species (Al, Ti, Fe, Si, Cu, and Sn). The produced laser–plasma ion sources were fully characterized against the laser intensity on the target (1013–1015 W/cm2) by varying the laser energy, focal spot size, and pulse duration. The versatility and tuneability of such high-repetition-rate laser–plasma ion sources are of potential interest for user applications. Such a statistically accurate study was facilitated by the large amount of data acquired at the high repetition rate (1–10 Hz) provided by the Bivoj laser system.","PeriodicalId":31879,"journal":{"name":"Quantum Beam Science","volume":"53 1","pages":""},"PeriodicalIF":1.4,"publicationDate":"2024-01-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139441204","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Double-Relief Silver Coins Minted in the Greek Colonies (444–390/340–280/270 BC) of Southern Italy Analysed by XRF","authors":"J. Brocchieri, R. Vitale, Carlo Sabbarese","doi":"10.3390/qubs8010002","DOIUrl":"https://doi.org/10.3390/qubs8010002","url":null,"abstract":"A sample of 18 double-relief coins from different poleis of Magna Graecia and ancient Italy has been analysed using a handheld XRF spectrometer directly inside the Museo Provinciale Campano (Capua, Italy). The data analysis shows that (i) the main elements are Ag and Cu, indicating that the coins are of high fineness (average Ag 95.7%), (ii) trace elements can help to characterise the coins, (iii) a superficial chemically altered layer (corrosion) is absent, (iv) the values of ratio Ag Kα/Lα evidence the presence of an enrichment layer on the surface of silver or subaerata in some coins. Multivariate statistical analysis and graph analysis allowed the coins to be assigned to different groups with the highest possible accuracy on the basis of the chemical data obtained and models to be constructed to classify the coins according to their historical periods.","PeriodicalId":31879,"journal":{"name":"Quantum Beam Science","volume":"32 4","pages":""},"PeriodicalIF":1.4,"publicationDate":"2023-12-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139157947","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Stress Measurement of Stainless Steel Piping Welds by Complementary Use of High-Energy Synchrotron X-rays and Neutrons","authors":"Yasufumi Miura, Kenji Suzuki, Satoshi Morooka, Takahisa Shobu","doi":"10.3390/qubs8010001","DOIUrl":"https://doi.org/10.3390/qubs8010001","url":null,"abstract":"Probabilistic fracture mechanics (PFM) is increasingly recognized as a viable approach for evaluating the structural integrity of nuclear components, such as piping, primarily affected by stress corrosion cracking (SCC). PFM analysis requires several input parameters, among which welding residual stress is critically important due to its significant influence on SCC initiation and propagation. Recently, a novel technique involving a double-exposure method (DEM) utilizing synchrotron X-rays was introduced as an effective means for measuring welding residual stress with high spatial resolution. In this paper, we applied DEM to assess the residual stress of a plate specimen, which was extracted from a welded pipe through electrical discharge machining. Consequently, detailed stress maps under a plane stress state were generated. Additionally, the residual stress distributions in the welded pipe under a triaxial stress state were evaluated using neutron diffraction. Based on these findings, we proposed a methodology to acquire detailed stress maps of welded pipes by combining high-energy synchrotron X-rays and neutron diffraction.","PeriodicalId":31879,"journal":{"name":"Quantum Beam Science","volume":"44 4","pages":""},"PeriodicalIF":1.4,"publicationDate":"2023-12-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139164409","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Cable Robots as Conventional Linear Stage Alternatives for the Investigation of Complex-Shaped Objects via Macroscopic X-ray Fluorescence Imaging","authors":"Matthias Alfeld, Philipp Tempel, V. van der Wijk","doi":"10.3390/qubs7040037","DOIUrl":"https://doi.org/10.3390/qubs7040037","url":null,"abstract":"The acquisition of elemental and chemical distribution images on the surface of cultural heritage objects has provided us new insights into our past. The techniques commonly employed, such as macroscopic X-ray fluorescence imaging (MA-XRF), in general require pointwise or whisk-broom scanning of an object under constant measurement geometry for optimal results. Most scanners in this field use stacked linear motorized stages, which are a proven solution for 2D sample positioning. Instead of these serial systems, we propose the use of a parallel cable robot to position the measurement head relative to the object investigated. In this article, we illustrate the significance of the issue and present our own cable robot prototype and test its capabilities, but also discuss the current shortcomings of the concept. With this, we demonstrate the potential of cable robots as platforms for MA-XRF and similar imaging techniques.","PeriodicalId":31879,"journal":{"name":"Quantum Beam Science","volume":"73 3","pages":""},"PeriodicalIF":1.4,"publicationDate":"2023-11-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139253713","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Almaz Nazarov, Alexey Maslov, Elena A. Korznikova, Kamil Ramazanov
{"title":"Chromium–Aluminum Coatings for Oxidation Protection of Titanium–Aluminum Intermetallic Alloys","authors":"Almaz Nazarov, Alexey Maslov, Elena A. Korznikova, Kamil Ramazanov","doi":"10.3390/qubs7040036","DOIUrl":"https://doi.org/10.3390/qubs7040036","url":null,"abstract":"This article explores the utilization of cathodic-arc deposition Cr-Al overlay coatings as oxidation protection for Ti-Al-Nb intermetallic alloys. The primary objective is to investigate PVD Al-Cr coatings deposited via cathodic-arc deposition without subsequent vacuum annealing. The microstructure, phase, and chemical composition of the coatings were characterized using scanning electron microscopy, energy-dispersive X-ray spectroscopy, and X-ray diffraction analysis. Isothermal exposure of samples in a laboratory air furnace was conducted, revealing the efficacy of Cr-Al coatings in protecting the Ti49-11Al-40Nb-1.5Zr-0.75V-0.75Mo-0.2Si (mass%) intermetallic alloy VTI-4 against oxidation. The findings highlight that the as-deposited coatings possess a layered structure and contain Al-Cr intermetallics. Post-exposure to the furnace without prior vacuum annealing results in coatings exhibiting a porous microstructure, raising concerns regarding oxidation protection. This investigation of Cr-Al coatings on a VTI-4 alloy substrate yields valuable insights into their nanolaminate structure and challenges associated with aluminum droplet fractions. The proposed additional vacuum heat treatment at 650 °C for 500 h effectively homogenizes the coating, leading to predominant Cr2Al and Ti-Al phases. Additionally, the formation of diffusion layers at the “coating–substrate” interface and the presence of oxide barriers contribute to the coatings’ heat resistance. Our research introduces possibilities for tailoring coating properties for specific high-temperature applications in aerospace, energy, or industrial contexts. Further refinement of the heat treatment process offers the potential for developing advanced coatings with enhanced performance characteristics.","PeriodicalId":31879,"journal":{"name":"Quantum Beam Science","volume":"16 3","pages":""},"PeriodicalIF":1.4,"publicationDate":"2023-11-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139257887","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Andrew G. Manning, Shinichiro Yano, Sojeong Kim, Won Bo Lee, Soo-Hyung Choi, Nicolas R. de Souza
{"title":"Identifying the Spin-Incoherent Contribution to Quasielastic Neutron Scattering with a Cold Triple-Axis Spectrometer","authors":"Andrew G. Manning, Shinichiro Yano, Sojeong Kim, Won Bo Lee, Soo-Hyung Choi, Nicolas R. de Souza","doi":"10.3390/qubs7040035","DOIUrl":"https://doi.org/10.3390/qubs7040035","url":null,"abstract":"Polarisation analysis for neutron scattering experiments is a powerful tool suitable for a wide variety of studies, including soft-matter samples which have no bulk magnetic behaviour and/or a significant hydrogen content. Here, we describe a method to leverage the versatility and spin-polarisation capabilities of a cold triple-axis spectrometer to perform a measurement to separate coherent and incoherent neutron scattering for a non-magnetic sample in the quasielastic neutron scattering (QENS) regime. Such measurements are complementary to unpolarised QENS measurements, which may typically be performed on a backscattering or time-of-flight spectrometer instrument where polarisation analysis can be significantly more difficult to achieve, and utilise the strengths of each type of instrument.","PeriodicalId":31879,"journal":{"name":"Quantum Beam Science","volume":"65 2","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-11-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136283477","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Measurement of Mechanical Behavior of 11B-Enriched MgB2 Wire Using a Pulsed Neutron Source","authors":"Shutaro Machiya, Kozo Osamura, Yoshimitsu Hishinuma, Hiroyasu Taniguchi, Stefanus Harjo, Takuro Kawasaki","doi":"10.3390/qubs7040034","DOIUrl":"https://doi.org/10.3390/qubs7040034","url":null,"abstract":"MgB2 represents a hexagonal superconductive material renowned for its straightforward composition, which has facilitated the development of cost-effective practical wires. Its capacity to function at temperatures as low as liquid hydrogen (LH2) has made it a prominent candidate as wire material for the coils of next-generation fusion reactors. Much like other superconducting wires, a prevalent issue arises when these wires are employed in coils, wherein electromagnetic forces induce tensile stress and strain within the wire. This, in turn, diminishes the critical current, which is the maximum current capable of flowing within the generated magnetic field and strain. The techniques and methods for accurately measuring the actual strain on the filaments are of paramount importance. While strain measurements have been conducted with synchrotron radiation and neutrons for other practical wires in the past, no such measurements have been undertaken for MgB2. Presumably, this lack of measurement is attributed to its relatively greater thickness, making it less suitable for synchrotron radiation measurements. Additionally, the high absorption cross-section of the included boron-10 poses challenges in obtaining elastic scattering data for neutron measurements. In response, we fabricated a wire enriched with boron-11, an isotope with a smaller neutron absorption cross-section. We then embarked on the endeavor to measure its strain under tensile loading using pulsed neutrons. Consequently, we succeeded in obtaining changes in the lattice constant under tensile loading through Rietveld analysis. This marks the inaugural instance of strain measurement on an MgB2 filament, signifying a significant milestone in superconductivity research.","PeriodicalId":31879,"journal":{"name":"Quantum Beam Science","volume":"97 ","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135872626","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Collective Acceleration of Helium Ions from Its Residual Atmosphere in a Luce Diode","authors":"Vladislav Ryzhkov, Mikhail Zhuravlev, Gennady Remnev","doi":"10.3390/qubs7040033","DOIUrl":"https://doi.org/10.3390/qubs7040033","url":null,"abstract":"The collective acceleration of helium ions from its residual atmosphere in the Luce diode was studied at helium pressures from 0.13 to 0.23 Pa. The energy of accelerated ions was determined from the drift velocity of the virtual cathode accelerating the ions. The number of 4He was determined by radioactivities of 13N and 30P induced in h-BN and Al targets via the nuclear reactions 10B(α,n)13N and 27Al(α,n)30P. The efficiency of capturing 4He ions in collective acceleration from the residual helium atmosphere was estimated as 0.25%. With increasing helium pressure above 0.15 Pa, the energy of the main ion group noticeably decreased to 0.46 MeV/amu compared to the acceleration from a usual residual atmosphere (~0.6 MeV/amu); however, the probability of ion acceleration to a specific energy of up to 1.57 MeV/amu increased significantly. Such increases in the ion energy were accompanied by the appearance of the signal of the second virtual cathode 7–9 ns after the appearance of the first virtual cathode.","PeriodicalId":31879,"journal":{"name":"Quantum Beam Science","volume":"26 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135266047","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}