Composites Part A: Applied Science and Manufacturing最新文献

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Accelerated fatigue characterization of additively manufactured continuous carbon fiber reinforced thermoplastic: A thermodynamic approach
IF 8.1 2区 材料科学
Composites Part A: Applied Science and Manufacturing Pub Date : 2025-02-13 DOI: 10.1016/j.compositesa.2025.108805
Mohammad Rouhi Moghanlou, Elaheh Azizian-Farsani, Ali Mahmoudi, Michael M Khonsari
{"title":"Accelerated fatigue characterization of additively manufactured continuous carbon fiber reinforced thermoplastic: A thermodynamic approach","authors":"Mohammad Rouhi Moghanlou,&nbsp;Elaheh Azizian-Farsani,&nbsp;Ali Mahmoudi,&nbsp;Michael M Khonsari","doi":"10.1016/j.compositesa.2025.108805","DOIUrl":"10.1016/j.compositesa.2025.108805","url":null,"abstract":"<div><div>A thermodynamic approach for accelerated fatigue characterization of additively manufactured continuous carbon fiber (CCF)-reinforced thermoplastics produced via fused filament fabrication (FFF) is presented. Specifically, we applied the concept of fracture fatigue entropy (FFE) to run-stop-cooldown (RSC) cyclic tests to efficiently predict fatigue life across both low- and high-cycle regions (10<sup>4</sup> – 10<sup>7</sup> cycles) while minimizing experimental workload. Results are presented for two fiber orientations: unidirectional (0°) and [0°/90°/±45°]<sub>s</sub> specimens. Elastic properties are established via tensile tests, and RSC tests are performed to assess the cyclic plastic strain energy and its associated temperature variations via thermographic measurements, leading to fatigue limit prediction. Through extensive tension–tension fatigue test accounting for internal friction, the study revealed average FFE values of 3.10 MJ/m<sup>3</sup>K and 3.67 MJ/m<sup>3</sup>K for 0° and [0°/90°/±45°]<sub>s</sub> specimens, respectively. These values are valid for low- and high-cycle fatigue regimes. A comparison between the experimental results and analytical predictions confirmed FFE’s capability for S-N curve prediction while highlighting the significant role of fiber orientation in cyclic response. Additionally, the steady-state temperature rise (Δ<em>T<sub>ss</sub></em>) was found to be significantly affected by fiber orientation, ranging from 0.3 °C in unidirectional to 14.6 °C in multidirectional specimens under the same applied load.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"192 ","pages":"Article 108805"},"PeriodicalIF":8.1,"publicationDate":"2025-02-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143428138","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of manufacturing conditions on morphology development in rapid stamp formed polyamide/glass fibre composite laminate components
IF 8.1 2区 材料科学
Composites Part A: Applied Science and Manufacturing Pub Date : 2025-02-13 DOI: 10.1016/j.compositesa.2025.108804
Ellen L. Heeley , Neil Reynolds , William Hamby , Catherine A. Kelly , Michael J. Jenkins , Darren J. Hughes
{"title":"Effect of manufacturing conditions on morphology development in rapid stamp formed polyamide/glass fibre composite laminate components","authors":"Ellen L. Heeley ,&nbsp;Neil Reynolds ,&nbsp;William Hamby ,&nbsp;Catherine A. Kelly ,&nbsp;Michael J. Jenkins ,&nbsp;Darren J. Hughes","doi":"10.1016/j.compositesa.2025.108804","DOIUrl":"10.1016/j.compositesa.2025.108804","url":null,"abstract":"<div><div>The effect of manufacturing conditions on the morphology of an industrially-processed 11-ply polyamide/glass fibre (PA66-GF60) laminate was investigated. Through-thickness temperature variation during the manufacturing process (pre-heating, stamp forming, demoulding) was revealed via eight inter-ply thermocouples. Thermal and X-ray analysis provided insights into process-induced polymer crystallinity and morphology through the laminate thickness. Cooling rates up to ∼ 2100 °C/min were observed in outer plies, compared to ∼ 420 °C/min for inner plies. A self-heating exothermal phenomenon was observed during crystallisation of the inner layers, leading to increased core crystallinity. X-ray diffraction revealed differences in preferred polymer orientation between the plies. For the inner plies, additional mobility from slower cooling leads to partially oriented crystallites along the glass fibre axis and a well-developed lamellar macromorphology. The rapidly cooled outer plies showed unoriented morphology, without long-range ordering. The work provides detailed understanding of polymer morphology for an industrially-relevant high-volume manufacturing process for thermoplastic matrix components.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"192 ","pages":"Article 108804"},"PeriodicalIF":8.1,"publicationDate":"2025-02-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143428136","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
High-efficiency ultrasonic welding of CF/epoxy joints with enhanced strength upon tailoring the energy director structure
IF 8.1 2区 材料科学
Composites Part A: Applied Science and Manufacturing Pub Date : 2025-02-12 DOI: 10.1016/j.compositesa.2025.108799
Jiaming Liu , Dong Quan , Jiaying Pan , Xuemin Wang , Xi Yang , Guoqun Zhao
{"title":"High-efficiency ultrasonic welding of CF/epoxy joints with enhanced strength upon tailoring the energy director structure","authors":"Jiaming Liu ,&nbsp;Dong Quan ,&nbsp;Jiaying Pan ,&nbsp;Xuemin Wang ,&nbsp;Xi Yang ,&nbsp;Guoqun Zhao","doi":"10.1016/j.compositesa.2025.108799","DOIUrl":"10.1016/j.compositesa.2025.108799","url":null,"abstract":"<div><div>Encouraging advancement in the ultrasonic welding of thermoset composites (TSCs) was recently achieved by co-curing weldable thermoplastic coupling layers (CLs) onto their surfaces. However, obvious temperature inhomogeneity at the welding interface easily leads to thermally decomposition of epoxy matrix and irreparable defects in the welds. This study proposed a strategy for producing high-quality ultrasonically-welded TSC joints by utilizing novel-structured thermoplastic meshes as energy directors (EDs). Compared to prevalent film EDs, the usage of mesh EDs significantly promoted the heat generation efficiency and temperature distribution uniformity at welding interfaces. The maximum temperature of TSCs reached during welding processes decreased from 373.7 °C to 216.7 °C with reduced welding time by 32.4 %. These phenomena effectively prevented thermally decomposed epoxy matrix, and resulted in high-quality welding lines with remarkable lap-shear strength, i.e. reaching a maximum value of 31.1 MPa. Overall, this study presents a promising strategy for developing robust TSC joints by tailoring ED structures.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"192 ","pages":"Article 108799"},"PeriodicalIF":8.1,"publicationDate":"2025-02-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143421131","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Enhancing the thermal conductivity and dielectric properties of polymer composite film through segregated boron nitride nanosheets
IF 8.1 2区 材料科学
Composites Part A: Applied Science and Manufacturing Pub Date : 2025-02-12 DOI: 10.1016/j.compositesa.2025.108802
Miracle Hope Adegun , Kit-Ying Chan , Heng Zhang , Yunfei Yang , Xiaomeng Zhao , Xuili Dong , Xi Shen , Jinglei Yang , Jang-Kyo Kim
{"title":"Enhancing the thermal conductivity and dielectric properties of polymer composite film through segregated boron nitride nanosheets","authors":"Miracle Hope Adegun ,&nbsp;Kit-Ying Chan ,&nbsp;Heng Zhang ,&nbsp;Yunfei Yang ,&nbsp;Xiaomeng Zhao ,&nbsp;Xuili Dong ,&nbsp;Xi Shen ,&nbsp;Jinglei Yang ,&nbsp;Jang-Kyo Kim","doi":"10.1016/j.compositesa.2025.108802","DOIUrl":"10.1016/j.compositesa.2025.108802","url":null,"abstract":"<div><div>High interfacial thermal resistance (ITR) between thermally conductive nanofillers and polymer matrix, and lack of good orientation of nanofillers are primary limiting factors in harnessing their inherent thermal conductivity in polymer nanocomposites. Thus, exploiting ultrahigh thermal conductivities of nanofillers involves developing methods or mechanisms that can minimize the ITR. In this work, boron nitride nanosheets (BNNS)/polyvinyl alcohol (PVA) nanocomposite films with segregation-induced interconnection among BNNS are fabricated by a sequential unidirection freeze-casting (UFC) technique. A PVA aerogel is first made by UFC followed by infiltrating functionalized BNNS into its pores and microchannels which is subjected to a second UFC process. The composite aerogel is subsequently hot pressed to compact the available pore channels for reduced ITR arising from better contact between the segregated BNNS cell walls. The resulting segregated BNNS/PVA (SBP) nanocomposite film with 40 wt% BNNS exhibits high thermal conductivity of 5.2 W/mK, which is about 267 % higher than the nanocomposite film containing dispersed BNNS made by conventional UFC. The SBP film also possessed high electrical insulation characteristics and a very low dielectric loss of <span><math><mrow><msup><mrow><mn>10</mn></mrow><mrow><mo>-</mo><mn>2</mn></mrow></msup></mrow></math></span> at a frequency of 1 kHz, properties arising directly from the segregated BNNS. The sequential UFC provides an effective method to incorporate aligned and interconnected BNNS through segregation for enhanced thermal conductivity and electrical resistivity for thermal management in microelectronics and integrated circuits.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"192 ","pages":"Article 108802"},"PeriodicalIF":8.1,"publicationDate":"2025-02-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143421050","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Two-step phase-separated ANF/polyimide aerogel fibers with tunable in situ core-sheath structure for wearable heat-insulated fabrics 用于可穿戴隔热织物的具有可调原位芯鞘结构的两步相分离 ANF/聚酰亚胺气凝胶纤维
IF 8.1 2区 材料科学
Composites Part A: Applied Science and Manufacturing Pub Date : 2025-02-12 DOI: 10.1016/j.compositesa.2025.108801
Zhilin Chen , Xianbo Hou , Jia Chen , Shuyan Nie , Shaowei Zhu , Tao Liu , Liming Chen
{"title":"Two-step phase-separated ANF/polyimide aerogel fibers with tunable in situ core-sheath structure for wearable heat-insulated fabrics","authors":"Zhilin Chen ,&nbsp;Xianbo Hou ,&nbsp;Jia Chen ,&nbsp;Shuyan Nie ,&nbsp;Shaowei Zhu ,&nbsp;Tao Liu ,&nbsp;Liming Chen","doi":"10.1016/j.compositesa.2025.108801","DOIUrl":"10.1016/j.compositesa.2025.108801","url":null,"abstract":"<div><div>Aerogel fibers have exhibited crucial application prospects in wearable heat-insulated fabrics. However, developing aerogel fibers with robust mechanical performance and high flexibility remains challenging due to their inherent fragility caused by high porosity. Herein, aramid nanofibers (ANF) reinforced polyimide (PI) aerogel fibers (ANF/PIAFs) are presented with tunable in situ core-sheath structure for super-flexible and super-toughness wearable heat-insulated fabrics by a novel two-step (2Step) phase separation strategy. The results demonstrate that the formation of sheath thickness and pore morphology of aerogel fibers can be tuned by the phase separation steps. Attributed to the core-sheath structure and the entanglement of chains with the introduction of ANF nanofibers, the tough and flexible ANF/PIAFs demonstrate improved tensile modulus (748.53 MPa), tensile strength (51.94 MPa) and fracture energy (18.28 MJ/m<sup>3</sup>) by 2.5 times, 11.5 times, and 288.2 times compared with the unprocessed PI aerogel fibers. Moreover, the addition of ANF effectively inhibits the shrinkage of aerogel fibers, which maintains the high thermal insulation ability (0.034 W/(m·K)). The strategy outlined in this study introduces a novel and universal method for fabricating aerogel fibers with a core-sheath structure using the improved phase separation technique, demonstrating the promising potential for applications in flexible thermal-insulated fabrics.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"192 ","pages":"Article 108801"},"PeriodicalIF":8.1,"publicationDate":"2025-02-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143421049","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Nonlinear rheological and thermo-oxidative aging behaviors of carbon black filled natural rubber nanocomposites mediated by a deep eutectic solvent based on 4-methyl-5,7-dihydroxycoumarin and tetrabutylammonium bromide
IF 8.1 2区 材料科学
Composites Part A: Applied Science and Manufacturing Pub Date : 2025-02-11 DOI: 10.1016/j.compositesa.2025.108798
Benteng Liu , Yihu Song , Miao Du , Qiang Zheng
{"title":"Nonlinear rheological and thermo-oxidative aging behaviors of carbon black filled natural rubber nanocomposites mediated by a deep eutectic solvent based on 4-methyl-5,7-dihydroxycoumarin and tetrabutylammonium bromide","authors":"Benteng Liu ,&nbsp;Yihu Song ,&nbsp;Miao Du ,&nbsp;Qiang Zheng","doi":"10.1016/j.compositesa.2025.108798","DOIUrl":"10.1016/j.compositesa.2025.108798","url":null,"abstract":"<div><div>Deep eutectic solvents (DESs) are able to promote vulcanization and improve mechanical properties of rubber nanocomposites. Investigated are rheological and thermo-oxidative aging behaviors of carbon black (CB) filled natural rubber (NR) nanocomposites mediated by a developed DES, revealing that the presence of DES could significantly promote vulcanization of NR and dispersibility of CB, the latter being related to polar interactions between DES and CB. DES interferes with the Payne effect by improving the onset strain amplitude and weakening the storage modulus decay and the loss modulus overshoot in the nonlinear viscoelasticity region without influencing mechanisms of Mullins effect during cyclic uniaxial tension at large strains. During long-term thermo-oxidative aging, DES influences the evolutions of mechanical properties and Mullins effect depending on the composition. This work is helpful for mediating the CB dispersity, NR crosslinking, strain softening and thermal-oxidative aging behavior of NR nanocomposites for design and manufacture of high-performance products.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"192 ","pages":"Article 108798"},"PeriodicalIF":8.1,"publicationDate":"2025-02-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143421132","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
A wide range of strain rate sensitivity and impact-induced behavior of Al/PTFE reactive materials: Experimental and numerical investigation
IF 8.1 2区 材料科学
Composites Part A: Applied Science and Manufacturing Pub Date : 2025-02-11 DOI: 10.1016/j.compositesa.2025.108797
Xinxin Ren , Jinchun Liu , Jiaxiang Wu , Yuchun Li , Yan Tu , Zhengwei Meng
{"title":"A wide range of strain rate sensitivity and impact-induced behavior of Al/PTFE reactive materials: Experimental and numerical investigation","authors":"Xinxin Ren ,&nbsp;Jinchun Liu ,&nbsp;Jiaxiang Wu ,&nbsp;Yuchun Li ,&nbsp;Yan Tu ,&nbsp;Zhengwei Meng","doi":"10.1016/j.compositesa.2025.108797","DOIUrl":"10.1016/j.compositesa.2025.108797","url":null,"abstract":"<div><div>Under impact loading, Al/PTFE reactive materials demonstrate notable strain rate sensitivity and impact-induced ignition. To investigate the influence of impact velocity, Al/PTFE composites (26.5 %/73.5 %) with 35 μm Al particles were synthesized and subjected to quasi-static and dynamic compression experiments. Results revealed a bilinear logarithmic relationship between stress and strain rate. A two-stage simplified Johnson-Cook (JC) model was calibrated to determine its mechanical properties and the parameters were validated by numerical simulations matching the experimental results. Extended simulations analyzed a wide range of strain rate sensitivities and established a dynamic increase factor (DIF) formulation that accurately describes the dynamic mechanical response of the material. These findings provide a robust basis for material selection and performance prediction, supported by comparisons with existing literature.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"192 ","pages":"Article 108797"},"PeriodicalIF":8.1,"publicationDate":"2025-02-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143402935","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Self-assembling biomimetic coating composed of 1D/2D CNT/polydopamine modified GO hybrid for solving conflict between carbon fiber-epoxy adhesion strength and fracture toughness
IF 8.1 2区 材料科学
Composites Part A: Applied Science and Manufacturing Pub Date : 2025-02-11 DOI: 10.1016/j.compositesa.2025.108800
Yating Li , Qing Wu , Ziyi Ye , Renjie Yao , Dan Jin , Min Zhao , Jianfeng Zhu
{"title":"Self-assembling biomimetic coating composed of 1D/2D CNT/polydopamine modified GO hybrid for solving conflict between carbon fiber-epoxy adhesion strength and fracture toughness","authors":"Yating Li ,&nbsp;Qing Wu ,&nbsp;Ziyi Ye ,&nbsp;Renjie Yao ,&nbsp;Dan Jin ,&nbsp;Min Zhao ,&nbsp;Jianfeng Zhu","doi":"10.1016/j.compositesa.2025.108800","DOIUrl":"10.1016/j.compositesa.2025.108800","url":null,"abstract":"<div><div>Tackling the intractable contradiction of interfacial strength-toughness is critical. Herein, shell nacre-mimetic coating composed of carbon nanotube (CNT) reinforced polyether amine (PEA)-polydopamine (PDA) and PDA functionalized graphene oxide (GO@PDA) was self-assembled around carbon fiber via a facile, green, low-cost but effective technique of vacuum filtration to fulfill the amplification of synergy effects of GO and CNTs under the constraint of delicate layered architecture. Contents of CNTs and GO@PDA were compared to optimize the performances. When 0.2 g GO@PDA and 5 ml CNTs were added, amazing growths in interfacial shear strength and fracture toughness of 114.2 % and 348.7 % were achieved, relative to untreated fiber composites. Increase in interfacial adhesion is associated with synergistic interactions of covalent and hydrogen bonds, π-π stacking along with mechanical pinning at interphase, while advance in interfacial toughness assigns with crack propagation, stretching deformation, and breakage of hydrogen bridge and π-π interaction that dissipate energy.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"192 ","pages":"Article 108800"},"PeriodicalIF":8.1,"publicationDate":"2025-02-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143421136","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Structural and hetero-interfacial engineering of magnetic bimetallic composites based polyurethane microwave absorbing coating for marine environment
IF 8.1 2区 材料科学
Composites Part A: Applied Science and Manufacturing Pub Date : 2025-02-08 DOI: 10.1016/j.compositesa.2025.108770
Qiaoqiao Han , Junhuai Xu , Jianyang Shi , Mi Zhou , Haibo Wang , Liang Geng , Junjie Xiong , Zongliang Du
{"title":"Structural and hetero-interfacial engineering of magnetic bimetallic composites based polyurethane microwave absorbing coating for marine environment","authors":"Qiaoqiao Han ,&nbsp;Junhuai Xu ,&nbsp;Jianyang Shi ,&nbsp;Mi Zhou ,&nbsp;Haibo Wang ,&nbsp;Liang Geng ,&nbsp;Junjie Xiong ,&nbsp;Zongliang Du","doi":"10.1016/j.compositesa.2025.108770","DOIUrl":"10.1016/j.compositesa.2025.108770","url":null,"abstract":"<div><div>Construction of microwave-absorbing materials adapted to marine application scenarios remain a challenge. Herein, environmentally stable Co<sub>x</sub>Ni<sub>y</sub>@C absorbers are fabricated. The CoNi-C heterogeneous interface in these absorbers induces a more inhomogeneous space charge distribution than Co-C and Ni-C interfaces, contributing to strong hetero-interfacial polarization and thereby improving microwave absorption performance. The C2 absorber demonstrated an EAB of 5.68 GHz, covering the entire Ku-band at a thickness of 1.98 mm. Additionally, simulations revealed an excellent radar stealth effect in unmanned aerial vehicle (UAV) mode. The 3D graphite skeleton of the absorber can extend the diffusion path of corrosive media and facilitate bacterial deposition, producing synergistic anti-corrosion and antibacterial effects. After immersion in a 3.5 % NaCl solution for 47 days, the |Z|<sub>0.01Hz</sub> value of polyurethane (PU)/C2 coating remained at 6.32 × 10<sup>8</sup> Ω cm<sup>2</sup>, indicating superior anticorrosion characteristics. The antibacterial rates of C2 reached 99.77 % against <em>Escherichia coli</em> and 99.11 % against <em>Staphylococcus aureus</em>. This work offers fresh concepts for the development of next-generation multifunctional microwave absorbents.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"192 ","pages":"Article 108770"},"PeriodicalIF":8.1,"publicationDate":"2025-02-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143376946","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
On the ply-wise investigation of the crystalline morphology distribution of in-situ consolidated CF/PEEK composite using Wide-Angle X-ray scattering (WAXS)
IF 8.1 2区 材料科学
Composites Part A: Applied Science and Manufacturing Pub Date : 2025-02-07 DOI: 10.1016/j.compositesa.2025.108792
Shafaq Shafaq , Matthew J. Donough , Ashleigh L. Farnsworth , Andrew W. Phillips , Gleny Chirima , Nigel A. St John , B. Ben Arber , Kilahney Murphy , Gangadhara Prusty
{"title":"On the ply-wise investigation of the crystalline morphology distribution of in-situ consolidated CF/PEEK composite using Wide-Angle X-ray scattering (WAXS)","authors":"Shafaq Shafaq ,&nbsp;Matthew J. Donough ,&nbsp;Ashleigh L. Farnsworth ,&nbsp;Andrew W. Phillips ,&nbsp;Gleny Chirima ,&nbsp;Nigel A. St John ,&nbsp;B. Ben Arber ,&nbsp;Kilahney Murphy ,&nbsp;Gangadhara Prusty","doi":"10.1016/j.compositesa.2025.108792","DOIUrl":"10.1016/j.compositesa.2025.108792","url":null,"abstract":"<div><div><em>In-situ</em> consolidated thermoplastic composites using automated fibre placement (AFP) experience highly localised and transient heating and cooling cycles during the process. Hence, the <em>in-situ</em> consolidation process can lead to significant fluctuations in polymer properties across the full part volume. The fluctuation in properties is primarily due to variations in cooling rates during the melting process and the number of high-temperature cycles experienced at each point. This paper presents the first study investigating the localised ply-wise crystalline properties of a Polyether-ether-ketone (PEEK) polymer matrix in a hot gas torch assisted <em>in-situ</em> consolidated carbon fibre PEEK composite with varying processing parameters using wide-angle X-ray scattering (WAXS) conducted on SAXS/WAXS beamline. The results demonstrate that crystallinity, and crystal orientation fraction exhibit ply-wise. However, maximum tool surface heating achieves a more uniform morphology. By integrating both orientation and crystallinity, a comprehensive strategy for optimising the mechanical performance of polymer materials can be developed.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"192 ","pages":"Article 108792"},"PeriodicalIF":8.1,"publicationDate":"2025-02-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143421133","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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