Halil Burak Kaybal , Hayrettin Duzcukoglu , Ramazan Asmatulu
{"title":"Integration of polysiloxane-modified halloysite nanoclay nanocomposite coatings on fiber-reinforced polymeric composites structures: Part II—Icing/deicing, self-cleaning, sandpaper abrasion, and water immersion performances","authors":"Halil Burak Kaybal , Hayrettin Duzcukoglu , Ramazan Asmatulu","doi":"10.1016/j.compositesa.2025.108879","DOIUrl":"10.1016/j.compositesa.2025.108879","url":null,"abstract":"<div><div>Cold weather conditions such as frost, snow, and freezing rain can limit the performance of fiber-reinforced composites, commonly used in aviation, defense, automotive, and other industries, potentially causing damage. Ice accumulation on surfaces can disrupt systems and damage components. Superhydrophobic (SH) surfaces offer a solution to prevent ice formation. This study explores the development of SH nanocomposite coatings based on polysiloxane-modified halloysite nanoclay (HNC) for glass, carbon, and Kevlar composites. The coatings’ effectiveness in preventing and removing ice was evaluated through various tests, including ice adhesion and air-blowing tests. The results showed that the SH coatings enhanced ice dissipation, particularly for carbon fiber composites. Despite slight changes in water contact angle after repeated tests, the coatings retained SH properties. Self-cleaning and wear tests demonstrated that the coatings successfully repelled dust and pollutants, while maintaining mechanical durability. This work offers a promising approach to improve ice-prevention performance in critical industrial applications.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"193 ","pages":"Article 108879"},"PeriodicalIF":8.1,"publicationDate":"2025-03-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143681007","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Feng Liang , Xin Cheng , Yuling Tang , Shuangyang Li , Jianfei Zhou , Bi Shi
{"title":"Robust and durable collagen-based fibers through dual cross-linking for eco-friendly slow fashion","authors":"Feng Liang , Xin Cheng , Yuling Tang , Shuangyang Li , Jianfei Zhou , Bi Shi","doi":"10.1016/j.compositesa.2025.108871","DOIUrl":"10.1016/j.compositesa.2025.108871","url":null,"abstract":"<div><div>Slow fashion, as a strategic alternative aimed at mitigating resource waste and environmental degradation in fast fashion, necessitates the development of robust and durable fibers. Collagen-based fibers have emerged as a promising option due to their moisture properties, biodegradability, and biocompatibility for durable textiles. However, these fibers encounter significant challenges in terms of mechanical strength, durability, and viability for sustainable production. In this study, robust and durable collagen-based fibers were designed using a dual cross-linking strategy and continuously prepared in situ via a low-temperature aqueous coagulation device. During wet spinning, polyvinyl alcohol (PVA) and aluminum chloride (AlCl<sub>3</sub>) act as the continuant and cross-linker, respectively. AlCl<sub>3</sub> effectively chelates the carboxyl groups on the collagen molecular chains and the reactive hydroxyl groups on the PVA chains, forming a stable coordination-hydrogen bond dual cross-linking network. Optimization of the spinning parameters resulted in fibers exhibiting superior mechanical properties, with a tensile strength of 339 MPa, Young’s modulus of 12.9 GPa, and toughness of 93 MJ/m<sup>3</sup>. Additionally, these fibers demonstrate a 10.8 % moisture regain and a dyeing grade of 4, highlighting their enhanced durability and breathability. This research provides robust solutions for enduring fibers and sustainable manufacturing processes in the slow fashion sector, facilitating new opportunities for the sustainable utilization of collagen waste.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"193 ","pages":"Article 108871"},"PeriodicalIF":8.1,"publicationDate":"2025-03-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143704250","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Hongtao Wang , Jikang Zhao , Jingxuan Dong , Ke Xu , Hongbo Geng , Xiaopeng Chen , Tianming Li , Guipin Yao , Xiaolong Jia , Lei Ge , Xiaoping Yang
{"title":"Efficient analysis of characteristic responses to curing behavior using FBG sensors for residual strain controlling in CFRP laminates","authors":"Hongtao Wang , Jikang Zhao , Jingxuan Dong , Ke Xu , Hongbo Geng , Xiaopeng Chen , Tianming Li , Guipin Yao , Xiaolong Jia , Lei Ge , Xiaoping Yang","doi":"10.1016/j.compositesa.2025.108869","DOIUrl":"10.1016/j.compositesa.2025.108869","url":null,"abstract":"<div><div>Fiber Bragg Grating (FBG) in-situ monitoring systems have become an effective tool for assisting with the high-precision molding and process optimization of carbon fiber-reinforced polymers (CFRP). This study aims to explore the underlying mechanisms by which FBG sensing signals characterize the curing behavior of CFRP. Initially, based on in-situ/non in-situ testing methods, the characteristic responsiveness of FBG sensing signals to the curing behavior of CFRP was explored. Furthermore, the feature response amplitude was used to evaluate the feature responsiveness of embedding setups (packaging structure and embedding techniques) to phase transitions. It was found that non-uniform adhesion and consolidation affected the sensor’s representation of curing shrinkage. Finally, using high characteristic response FBG sensors, the process optimal strategy for CFRP was explored. The proposed method for analyzing the characteristic response of FBG sensing signals establishes and validates the relationship between CFRP curing behaviors and signal points, as well as stage-specific amplitude changes. This research serves as a fundamental basis for accurately characterizing CFRP curing behaviors and enhancing high-precision forming process design.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"194 ","pages":"Article 108869"},"PeriodicalIF":8.1,"publicationDate":"2025-03-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143725613","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
J. Lee , M. Duhovic , D. May , T. Allen , P. Kelly
{"title":"Physics-informed neural networks for real-time simulation of transverse Liquid Composite Moulding processes and permeability measurements","authors":"J. Lee , M. Duhovic , D. May , T. Allen , P. Kelly","doi":"10.1016/j.compositesa.2025.108857","DOIUrl":"10.1016/j.compositesa.2025.108857","url":null,"abstract":"<div><div>Physics-Informed Neural Networks (PINNs) offer advantages over conventional data-driven machine learning approaches as they are data-free and can make better predictions on unseen data by incorporating physical information in the form of the governing equations. The governing equation for the coupled flow and deformation behaviour in transverse Liquid Composite Moulding processes is used to demonstrate the capabilities of PINNs for process simulation. Parametric solutions of the deformation of a saturated fabric stack under varying applied loading are obtained using the PINN model, showing close agreement with finite element simulations but with significantly shorter computation times. A novel PINN architecture is developed to replace empirical equations for the permeability and compressibility constitutive relations with neural networks trained to fit experimental data. Finally, PINNs are used to analyse transverse permeability measurements, allowing for real-time monitoring of the permeability variation through the thickness, as opposed to the apparent permeability of a hydrodynamically-deformed sample.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"193 ","pages":"Article 108857"},"PeriodicalIF":8.1,"publicationDate":"2025-03-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143681003","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Siyuan Chen , Adam Thompson , Tim Dodwell , Stephen Hallett , Jonathan Belnoue
{"title":"A comparison between robust design and digital twin approaches for Non-Crimp fabric (NCF) forming","authors":"Siyuan Chen , Adam Thompson , Tim Dodwell , Stephen Hallett , Jonathan Belnoue","doi":"10.1016/j.compositesa.2025.108864","DOIUrl":"10.1016/j.compositesa.2025.108864","url":null,"abstract":"<div><div>There is growing interest in adopting digital twin systems within the field of composites manufacturing. However, given the current limitations in measuring variability and accurately simulating complex defects, it remains questionable as to whether the high costs of building a digital twin are justified. In this paper, a case study is conducted on simulation-driven optimisation of the forming of non-crimp fabric (NCF). A robust design strategy (a one-time optimisation that is robust to variabilities of the material and process) is compared with a digital twin approach (active control is conducted based on real-time optimisation, accounting for in-situ measurements of variabilities). An optimisation method based on a Gaussian process (GP) surrogate model, active learning, dimension reduction and gradient boosting is developed. This method enables the optimisation of complex forming processes with a very small dataset, built from large simulation models. Both strategies significantly reduce the wrinkling level and improve process robustness.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"193 ","pages":"Article 108864"},"PeriodicalIF":8.1,"publicationDate":"2025-03-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143704028","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Advancements and innovations in textile engineering: An In-Depth analysis of SWCNTs and PANI integration in smart textile technologies","authors":"Fahad Alhashmi Alamer, Alhanouf Alzahrani","doi":"10.1016/j.compositesa.2025.108872","DOIUrl":"10.1016/j.compositesa.2025.108872","url":null,"abstract":"<div><div>This review explores advancements in smart textiles, emphasizing the integration of single-walled carbon nanotubes (SWCNTs) and polyaniline (PANI). Combining these materials enhances the physical properties and functionalities of textiles, particularly in wearable electronics. SWCNTs improve the mechanical strength, thermal stability, and electrical properties of PANI-coated textiles. We discuss key fabrication techniques like solution blending and electrospinning and address the challenges of SWCNT integration such as dispersion and potential toxicity. Additionally, the review covers the broader application potential of SWCNTs in multifunctional smart textiles, including self-healing materials and sensors. This analysis aims to inform researchers and industry professionals about the current capabilities and future possibilities of SWCNTs and PANI in textile engineering.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"193 ","pages":"Article 108872"},"PeriodicalIF":8.1,"publicationDate":"2025-03-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143681001","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Maximilian Pitto , Holger Fiedler , Tom Allen , Casparus Johannes Reinhard Verbeek , Simon Bickerton
{"title":"High-power air plasma diagnostics by optical emission spectroscopy for subsecond continuous carbon fibre surface modification","authors":"Maximilian Pitto , Holger Fiedler , Tom Allen , Casparus Johannes Reinhard Verbeek , Simon Bickerton","doi":"10.1016/j.compositesa.2025.108855","DOIUrl":"10.1016/j.compositesa.2025.108855","url":null,"abstract":"<div><div>This paper aims to elucidate the interplay between surface heating, plasma emission, and treatment time in a subsecond continuous unsized CF plasma surface oxidation process. Optical emission spectroscopy, high-speed imaging, infrared thermography, scanning electron microscopy, and X-ray photoelectron spectroscopy were utilised to characterise the plasma species, discharge mode, CF surface temperature, morphology, and functionality, respectively. It was shown that plasma transition from diffuse to filamentary discharge for a nozzle in close proximity to CF changes the surface modification trend. Specifically, increased treatment time was needed for O/C composition enhancement in the filamentary discharge, potentially resulting from elevated treatment heterogeneity. The diffuse discharge achieved a maximum O/C for the minimum residence time of <span><math><mrow><mn>0</mn><mo>.</mo><mn>41</mn><mspace></mspace></mrow></math></span>s. The transitional discharge mode with the maximum O emission intensity produced the overall maximum O/C enhancement of 57% in <span><math><mrow><mn>0</mn><mo>.</mo><mn>61</mn><mspace></mspace></mrow></math></span>s with a non-monotonic temporal trend. It was revealed that for diffuse and transitional plasma, <figure><img></figure> , <figure><img></figure> surface content is explained well by the maximum <figure><img></figure> luminescence emission intensity divided by treatment time, enabling the use of <figure><img></figure> emission as an indicator for atmospheric pressure air plasma reactivity. While high temperatures, exceeding 650 °C for filamentary plasma, can influence the oxidation rate, only energetic and highly concentrated oxidative plasma species such as O, O<sub>3</sub>, <figure><img></figure> can realise the subsecond functionalisation. Overall, this work shows that characterising the discharge mode and measuring the plasma species using readily available tools provides valuable information to commission plasma sources for fibre functionalisation.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"193 ","pages":"Article 108855"},"PeriodicalIF":8.1,"publicationDate":"2025-03-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143681006","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Longxu Yao , Zhanqiang Liu , Qinghua Song , Bing Wang , Yukui Cai , Qiang Luan , Hongxin Wang
{"title":"Machining quality improvement through ice densification pretreatment during rotary ultrasonic face grinding SiO2f/SiO2 composite","authors":"Longxu Yao , Zhanqiang Liu , Qinghua Song , Bing Wang , Yukui Cai , Qiang Luan , Hongxin Wang","doi":"10.1016/j.compositesa.2025.108878","DOIUrl":"10.1016/j.compositesa.2025.108878","url":null,"abstract":"<div><div>From the perspective of weakening the inherent preparation defects of the SiO<sub>2f</sub>/SiO<sub>2</sub> composite, a novel hybrid machining process combining ice densification pretreatment with rotary ultrasonic face grinding (IDP-RUFG) was firstly proposed in this study to reduce the contradiction between grinding surface quality and grinding efficiency. The improvement mechanism of IDP-RUFG process on the machinability of SiO<sub>2f</sub>/SiO<sub>2</sub> composite was analyzed from material strengthening and grinding mechanics. The grinding experiments were carried out to confirm the surface integrity improvement in the IDP-RUFG process. By comparing with the conventional RUFG surface, the maximum peak height Sp on the IDP-RUFG surface was reduced by 16.6 %∼31.4 % with the 9.1 %∼27.9 % reduction in the debonding fiber damage ratio <em>β</em>. The subsurface damage patterns both in IDP-RUFG process and RUFG process were characterized by fiber–matrix interface debonding, subsurface cracks, and matrix fracture. However, the subsurface damage depth during the IDP-RUFG process could be reduced by more than 40 %.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"193 ","pages":"Article 108878"},"PeriodicalIF":8.1,"publicationDate":"2025-03-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143681002","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
E. Polyzos , I.A. Rodrigues Lopes , P.P. Camanho , D. Van Hemelrijck , L. Pyl
{"title":"Continuum damage modeling of unidirectional 3D-printed composites under longitudinal tension","authors":"E. Polyzos , I.A. Rodrigues Lopes , P.P. Camanho , D. Van Hemelrijck , L. Pyl","doi":"10.1016/j.compositesa.2025.108850","DOIUrl":"10.1016/j.compositesa.2025.108850","url":null,"abstract":"<div><div>This work presents a two-scale modeling approach for simulating the progressive damage behavior of unidirectional 3D-printed composites reinforced with continuous fibers. The approach utilizes a semi-analytical method, combining analytical homogenization at the micro-scale and finite element modeling at the macro-scale. At the micro-scale, the analytical model incorporates weakest link theory and Weibull statistics to account for fiber damage. At the macro-scale, a novel method based on continuum damage mechanics (CDM) is developed to consider damage evolution. The two-scale modeling approach is compared to experimental results of tensile and open-hole tests of 3D-printed composites reinforced with continuous carbon fibers. The comparison demonstrates that the two-scale modeling approach captures well the complex mechanical behavior of unidirectional 3D-printed composites.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"193 ","pages":"Article 108850"},"PeriodicalIF":8.1,"publicationDate":"2025-03-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143680998","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Dynamic analysis of composite laminated sandwich plates with graphene-reinforced magnetorheological elastomer: Numerical and experimental study","authors":"Purushothaman Selvaraj, Ramesh Babu Vemuluri","doi":"10.1016/j.compositesa.2025.108874","DOIUrl":"10.1016/j.compositesa.2025.108874","url":null,"abstract":"<div><div>This study investigates the dynamic characteristics of composite laminated magnetorheological elastomer (MRE) sandwich plates, both with and without graphene in the<!--> <!-->MRE core. First, the composite laminated face sheets, MRE core, and graphene-reinforced MRE (GMRE) core are prepared. Then laminated composite MRE sandwich plates (MRESP) and graphene-reinforced MRE sandwich plates (GMRESP) are fabricated, and the natural frequencies of the sandwich plates are determined experimentally with various magnetic fields under clamped-free (CF) boundary conditions. The governing differential equations for the composite laminated MRESP and GMRESP are derived using classical laminated plate theory (CLPT) and solved using Lagrange formulation. Numerical simulation has been conducted using MATLAB, results are validated with experimental results and available literature. Further, the influence of various parameters on MRESP and GMRESP dynamic behaviour was investigated.<!--> <!-->The GMRESP and MRESP natural frequencies exhibit an increase of 30.29 % and 26.51 %, respectively, as the magnetic field increased from 0 G to 300 G.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"193 ","pages":"Article 108874"},"PeriodicalIF":8.1,"publicationDate":"2025-03-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143681000","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}