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Organic Syntheses最新文献

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Preparation of N-Boc-3-methylpyrrole via Anionic Rearrangement 阴离子重排法制备n - boc -3-甲基吡咯
IF 0.7
Organic Syntheses Pub Date : 2023-01-01 DOI: 10.15227/orgsyn.0100.0061
Daniel P. Graeff
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引用次数: 0
α-Oxamination of Amides via Electrophilic Activation 亲电活化法α-酰胺化研究
IF 0.7
Organic Syntheses Pub Date : 2023-01-01 DOI: 10.15227/orgsyn.100.0136
Miran Lemmerer
{"title":"α-Oxamination of Amides via Electrophilic Activation","authors":"Miran Lemmerer","doi":"10.15227/orgsyn.100.0136","DOIUrl":"https://doi.org/10.15227/orgsyn.100.0136","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67342526","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis of a Furoindoline Scaffold via an Interrupted Fischer Indolization 间断菲舍尔注射法合成呋喃吲哚啉支架
Organic Syntheses Pub Date : 2023-01-01 DOI: 10.15227/orgsyn.100.0304
Georgia M. Scherer
{"title":"Synthesis of a Furoindoline Scaffold via an Interrupted Fischer Indolization","authors":"Georgia M. Scherer","doi":"10.15227/orgsyn.100.0304","DOIUrl":"https://doi.org/10.15227/orgsyn.100.0304","url":null,"abstract":"A. 3-Methyltetrahydrofuran-2-ol (2). A single-necked (24/40 joint) 1000-mL round-bottomed flask, charged with a Teflon-coated magnetic stir bar (5 x 1 cm, football-shaped), and a 125 mL pressure-equalizing addition funnel (24/40 joint) are dried in an oven overnight (160 °C). The glassware is assembled while hot, and the addition funnel is sealed with a 24/40 rubber septum with an argon inlet and an outlet connected to a bubbler. The apparatus is allowed to cool to 23 °C under a stream of dry argon. The joint between the addition funnel and round-bottomed flask is wrapped tightly with Teflon tape and clamped with a Keck clip (24/40) (Note 2). 3-Methyldihydrofuran-2(3H)-one (1) (3.3 mL, 3.52 g, 35.2 mmol, 1.0 equiv) (Note 3) is added to the addition funnel through the septum using a plastic i-Bu2AlH CH2Cl2, –78 °C","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136004008","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Potassium 5-Bromopentyltrifluoroborate 5-溴代三氟硼酸钾
IF 0.7
Organic Syntheses Pub Date : 2023-01-01 DOI: 10.15227/orgsyn.100.0218
Sarah J. Burke
{"title":"Potassium 5-Bromopentyltrifluoroborate","authors":"Sarah J. Burke","doi":"10.15227/orgsyn.100.0218","DOIUrl":"https://doi.org/10.15227/orgsyn.100.0218","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67343095","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Large Scale Epoxide Opening by a Pendant Silanol. 利用硅烷偶联醇打开大规模环氧化物。
IF 0.7
Organic Syntheses Pub Date : 2023-01-01 DOI: 10.15227/orgsyn.100.0446
Annu Anna Thomas, Someshwar Nagamalla, Shyam Sathyamoorthi
{"title":"Large Scale Epoxide Opening by a Pendant Silanol.","authors":"Annu Anna Thomas, Someshwar Nagamalla, Shyam Sathyamoorthi","doi":"10.15227/orgsyn.100.0446","DOIUrl":"10.15227/orgsyn.100.0446","url":null,"abstract":"<p><p></p>","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10809772/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139564547","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Introducing Volume 100 of Organic Syntheses 介绍《有机合成》第100卷
IF 0.7
Organic Syntheses Pub Date : 2023-01-01 DOI: 10.15227/orgsyn.100.0001
R. Danheiser
{"title":"Introducing Volume 100 of Organic Syntheses","authors":"R. Danheiser","doi":"10.15227/orgsyn.100.0001","DOIUrl":"https://doi.org/10.15227/orgsyn.100.0001","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67342302","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Ethoxypillar[6]arene 乙氧基柱[6]芳烃
IF 0.7
Organic Syntheses Pub Date : 2022-01-01 DOI: 10.15227/orgsyn.099.0125
Chelsea R. Wilson
{"title":"Ethoxypillar[6]arene","authors":"Chelsea R. Wilson","doi":"10.15227/orgsyn.099.0125","DOIUrl":"https://doi.org/10.15227/orgsyn.099.0125","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67341493","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Large Scale Oxidative Cyclization of (E)-hex-3-en-1-yl (4-methoxyphenyl)sulfamate (E)-己-3-烯-1-基(4-甲氧基苯基)氨基甲酸酯的大规模氧化环化
IF 0.7
Organic Syntheses Pub Date : 2022-01-01 DOI: 10.15227/orgsyn.099.0286
Anand H Shinde
{"title":"Large Scale Oxidative Cyclization of (E)-hex-3-en-1-yl (4-methoxyphenyl)sulfamate","authors":"Anand H Shinde","doi":"10.15227/orgsyn.099.0286","DOIUrl":"https://doi.org/10.15227/orgsyn.099.0286","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67342187","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Synthesis of (((1R,3S,3'S)-3,3'-Diethyl-3H,3'H-1,1'-spirobi[isobenzofuran]-7,7'-diyl)bis(oxy))bis(diphenylphosphane) ((1R,3S,3' s)-3,3'-二乙基- 3h,3'- 1,1'-spirobi[异苯并呋喃]-7,7'-二基)双(氧)双(二苯基膦)的合成
IF 0.7
Organic Syntheses Pub Date : 2022-01-01 DOI: 10.15227/orgsyn.099.0190
Siyuan Sun
{"title":"Synthesis of (((1R,3S,3'S)-3,3'-Diethyl-3H,3'H-1,1'-spirobi[isobenzofuran]-7,7'-diyl)bis(oxy))bis(diphenylphosphane)","authors":"Siyuan Sun","doi":"10.15227/orgsyn.099.0190","DOIUrl":"https://doi.org/10.15227/orgsyn.099.0190","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67341507","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis of [(R)-DTBM-SEGPHOS]NiCl2 for the Enantioselective Acetal Formation from N-Propanoyl-1,3-Thiazinane-2-thione and Trimethyl Orthoformate n -丙酰基-1,3-噻嗪-2-硫酮和原甲酸三甲酯对映选择性缩醛合成[(R)-DTBM-SEGPHOS]NiCl2
IF 0.7
Organic Syntheses Pub Date : 2022-01-01 DOI: 10.15227/orgsyn.099.0001
Stuart C. D. Kennington
{"title":"Synthesis of [(R)-DTBM-SEGPHOS]NiCl2 for the Enantioselective Acetal Formation from N-Propanoyl-1,3-Thiazinane-2-thione and Trimethyl Orthoformate","authors":"Stuart C. D. Kennington","doi":"10.15227/orgsyn.099.0001","DOIUrl":"https://doi.org/10.15227/orgsyn.099.0001","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67340965","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
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