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Discussion Addendum for: Nickel-Catalyzed Cross-Coupling of Aryl Halides with Alkyl Halides: Ethyl 4-(4-(4-methylphenylsulfonamido)-phenyl)butanoate 镍催化芳基卤化物与卤代烷的交叉偶联:4-(4-(4-甲基苯基磺胺)-苯基)丁酸乙酯
IF 0.7
Organic Syntheses Pub Date : 2022-01-01 DOI: 10.15227/orgsyn.099.0215
Daniel C. Salgueiro
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引用次数: 0
Discussion Addendum for: Synthesis of N-Boc-N-Hydroxymethyl-L-phenylalaninal and Methyl trans-Oxazolidine-5-carboxylate, Chiral Synthons for threo-β-Amino-α-hydroxy Acids 讨论附录:n - boc - n -羟甲基- l-苯丙氨酸和甲基反式恶唑烷-5-羧酸酯的合成，3 -β-氨基-α-羟基酸的手性合成物
IF 0.7
Organic Syntheses Pub Date : 2022-01-01 DOI: 10.15227/orgsyn.099.0274
Youngran Seo
{"title":"Discussion Addendum for: Synthesis of N-Boc-N-Hydroxymethyl-L-phenylalaninal and Methyl trans-Oxazolidine-5-carboxylate, Chiral Synthons for threo-β-Amino-α-hydroxy Acids","authors":"Youngran Seo","doi":"10.15227/orgsyn.099.0274","DOIUrl":"https://doi.org/10.15227/orgsyn.099.0274","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67341722","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis of Phenanthridinones via the Palladium-Catalyzed Annulation of Benzyne 钯催化苯环化法合成菲苯二酮
IF 0.7
Organic Syntheses Pub Date : 2022-01-01 DOI: 10.15227/orgsyn.099.0159
Dominick C. Witkowski
{"title":"Synthesis of Phenanthridinones via the Palladium-Catalyzed Annulation of Benzyne","authors":"Dominick C. Witkowski","doi":"10.15227/orgsyn.099.0159","DOIUrl":"https://doi.org/10.15227/orgsyn.099.0159","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67341788","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis of Carboxylic Acids from Benzamide Precursors Using Nickel Catalysis 用镍催化苯甲酰胺前体合成羧酸
IF 0.7
Organic Syntheses Pub Date : 2022-01-01 DOI: 10.15227/orgsyn.099.0305
Ana S Bulger
{"title":"Synthesis of Carboxylic Acids from Benzamide Precursors Using Nickel Catalysis","authors":"Ana S Bulger","doi":"10.15227/orgsyn.099.0305","DOIUrl":"https://doi.org/10.15227/orgsyn.099.0305","url":null,"abstract":"A. N-Methyl-N-phenyl benzamide (3). A single-necked (24/40 joint) 500 mL round-bottomed flask is equipped with a Teflon-coated magnetic stir bar (3 cm, oval-shaped). The flask is dried in an oven (105 °C) for 16 h. The flask is brought out of the oven, sealed immediately with a rubber septum, and allowed to cool to room temperature (23 °C) in a desiccator (Note 2). The flask is purged with argon by connecting to an argon manifold using a needle (18G), and via another needle (18G) to a gas outlet terminating in an oil bubbler. The atmosphere is maintained under a slight positive pressure of argon for the duration of the reaction (Note 3). The flask is then charged with triethylamine (6.5 mL, 47 mmol, 1.3 equiv) (Note 4) using a plastic syringe Et3N CH2Cl2, 0 °C to 23 °C 1","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67341869","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Transition-Metal-Free Synthesis of an Aryl Boronate Ester through Base-Mediated Boryl Substitution of an Aryl Halide with a Silylborane 用硅硼烷取代芳基卤化物以无过渡金属合成芳基硼酸酯
IF 0.7
Organic Syntheses Pub Date : 2022-01-01 DOI: 10.15227/orgsyn.099.0039
R. Shishido
{"title":"Transition-Metal-Free Synthesis of an Aryl Boronate Ester through Base-Mediated Boryl Substitution of an Aryl Halide with a Silylborane","authors":"R. Shishido","doi":"10.15227/orgsyn.099.0039","DOIUrl":"https://doi.org/10.15227/orgsyn.099.0039","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67340937","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis of Alkylboronic Esters from Alkyl Iodides 由烷基碘化物合成烷基硼酯
IF 0.7
Organic Syntheses Pub Date : 2022-01-01 DOI: 10.15227/orgsyn.099.0015
Qianyi Liu
{"title":"Synthesis of Alkylboronic Esters from Alkyl Iodides","authors":"Qianyi Liu","doi":"10.15227/orgsyn.099.0015","DOIUrl":"https://doi.org/10.15227/orgsyn.099.0015","url":null,"abstract":"¶College of Chemistry and Molecular Engineering, Peking University, Beijing 100871, China; ‡WuXi AppTec (Tianjin) Co., Ltd., Tianjin 300457, China; ∥Tianjin Key Laboratory of Structure and Performance for Functional Molecules, College of Chemistry, Tianjin Normal University, Tianjin 300387, China; †Department of Chemistry and Biochemistry, University of California Santa Barbara, California 93106, USA; §School of Materials Science and Engineering, Peking University, Beijing 100871, China aThese authors contributed equally.","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67341095","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Preparation of 1,2:5,6-Di-O-cyclohexylidene-D-mannitol and 2,3-Cyclohexylidene-D-glyceraldehyde 1,2:5,6-二- o -环己基- d -甘露醇和2,3-环己基- d -甘油醛的制备
IF 0.7
Organic Syntheses Pub Date : 2022-01-01 DOI: 10.15227/orgsyn.099.0363
N. R. Dhatrak
{"title":"Preparation of 1,2:5,6-Di-O-cyclohexylidene-D-mannitol and 2,3-Cyclohexylidene-D-glyceraldehyde","authors":"N. R. Dhatrak","doi":"10.15227/orgsyn.099.0363","DOIUrl":"https://doi.org/10.15227/orgsyn.099.0363","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67341909","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Stereoselective Synthesis of Dimethyl 4(S)-Allyl-N-Boc-L-glutamate and Related Congeners 4(S)-烯丙基- n - boc - l-谷氨酸二甲基及其同源物的立体选择性合成
IF 0.7
Organic Syntheses Pub Date : 2022-01-01 DOI: 10.15227/orgsyn.099.0326
Akash Mishra
{"title":"Stereoselective Synthesis of Dimethyl 4(S)-Allyl-N-Boc-L-glutamate and Related Congeners","authors":"Akash Mishra","doi":"10.15227/orgsyn.099.0326","DOIUrl":"https://doi.org/10.15227/orgsyn.099.0326","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67341927","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Preparation of a donor-acceptor Stenhouse Adduct (DASA): 5-((2Z,4E)-5-(diethylamino)-2-hydroxypenta-2,4-dien-1-ylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione. 施-受体Stenhouse加合物(DASA)的制备:5-((2Z,4E)-5-(二乙胺)-2-羟基戊基-2,4-二烯-1-乙基)-2,2-二甲基-1,3-二恶烷-4,6-二酮。
IF 0.7
Organic Syntheses Pub Date : 2022-01-01 DOI: 10.15227/orgsyn.099.0079
Friedrich Stricker
{"title":"Preparation of a donor-acceptor Stenhouse Adduct (DASA): 5-((2Z,4E)-5-(diethylamino)-2-hydroxypenta-2,4-dien-1-ylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione.","authors":"Friedrich Stricker","doi":"10.15227/orgsyn.099.0079","DOIUrl":"https://doi.org/10.15227/orgsyn.099.0079","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67341385","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Discussion Addendum for: Preparation of Diisopropylammonium Bis(catecholato)cyclohexylsilicate 讨论附录:制备双(儿茶酚酸)环己基硅酸二异丙铵
IF 0.7
Organic Syntheses Pub Date : 2022-01-01 DOI: 10.15227/orgsyn.099.0342
Christopher B. Kelly
{"title":"Discussion Addendum for: Preparation of Diisopropylammonium Bis(catecholato)cyclohexylsilicate","authors":"Christopher B. Kelly","doi":"10.15227/orgsyn.099.0342","DOIUrl":"https://doi.org/10.15227/orgsyn.099.0342","url":null,"abstract":"† Chemical Process R&D, Discovery Process Research, Janssen Research & Development LLC, 1400 McKean Rd., Spring House, PA 19477, USA ‡ Department of Biological and Chemical Sciences, College of Life Sciences, Thomas Jefferson University, 4201 Henry Ave., Philadelphia, PA 19144, USA § Chemical Process R&D, Discovery Process Research, Janssen Pharmaceutica N.V., Turnhoutseweg 30, B-2340 Beerse, Belgium","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67342337","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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