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Catalytic Enantioselective Addition of an In‐Situ Prepared Aryltitanium Reagent to p ‐Chloroacetophenone: ( R )‐(+)‐1‐(4‐Chlorophenyl)‐1‐ m ‐Tolylethanol 原位制备芳基钛试剂对对氯苯乙酮的催化对映选择性加成:(R)‐(+)‐1‐(4‐氯苯基)‐1‐m‐甲苯乙醇
IF 0.7
Organic Syntheses Pub Date : 2020-04-29 DOI: 10.1002/0471264229.OS096.21
Yusuke Kobayashi, A. Matsuda, Tomoya Ushimaru, T. Harada, J. Hughes, K. Campos
{"title":"Catalytic Enantioselective Addition of an In‐Situ Prepared Aryltitanium Reagent to\u0000 p\u0000 ‐Chloroacetophenone: (\u0000 R\u0000 )‐(+)‐1‐(4‐Chlorophenyl)‐1‐\u0000 m\u0000 ‐Tolylethanol","authors":"Yusuke Kobayashi, A. Matsuda, Tomoya Ushimaru, T. Harada, J. Hughes, K. Campos","doi":"10.1002/0471264229.OS096.21","DOIUrl":"https://doi.org/10.1002/0471264229.OS096.21","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"127 1","pages":""},"PeriodicalIF":0.7,"publicationDate":"2020-04-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"50943877","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Discussion Addendum for: Synthesis of Ynamides by Copper-Mediated Coupling of 1,1-Dibromo-1-Alkenes with Nitrogen Nucleophiles. Preparation of 4-Methyl-N-(2-Phenylethynyl)-N-(Phenylmethyl)Benzenesulfonamide 讨论附录:铜介导1,1-二溴-1-烯烃与氮亲核试剂偶联合成酰胺。4-甲基- n -(2-苯基乙基)- n -(苯基甲基)苯磺酰胺的制备
IF 0.7
Organic Syntheses Pub Date : 2020-04-29 DOI: 10.1002/0471264229.os096.13
Cédric Theunissen, Pierre Thilmany, Mounsef Lahboubi, N. Blanchard, G. Evano
{"title":"Discussion Addendum for: Synthesis of Ynamides by Copper-Mediated Coupling of 1,1-Dibromo-1-Alkenes with Nitrogen Nucleophiles. Preparation of 4-Methyl-N\u0000-(2-Phenylethynyl)-N\u0000-(Phenylmethyl)Benzenesulfonamide","authors":"Cédric Theunissen, Pierre Thilmany, Mounsef Lahboubi, N. Blanchard, G. Evano","doi":"10.1002/0471264229.os096.13","DOIUrl":"https://doi.org/10.1002/0471264229.os096.13","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":" ","pages":""},"PeriodicalIF":0.7,"publicationDate":"2020-04-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"44936590","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
( R )‐ N,N '‐Dimethyl‐1,1'‐Binaphthyldiamine (R)‐N, N 110毫克‐‐”‐Binaphthyldiamine
IF 0.7
Organic Syntheses Pub Date : 2020-04-29 DOI: 10.1002/0471264229.os096.24
S. Denmark, P. Ryabchuk, Eric R. Welin, B. Stoltz
{"title":"(\u0000 R\u0000 )‐\u0000 N,N\u0000 '‐Dimethyl‐1,1'‐Binaphthyldiamine","authors":"S. Denmark, P. Ryabchuk, Eric R. Welin, B. Stoltz","doi":"10.1002/0471264229.os096.24","DOIUrl":"https://doi.org/10.1002/0471264229.os096.24","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"7 ","pages":""},"PeriodicalIF":0.7,"publicationDate":"2020-04-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"50944039","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis of 3,6-Bis(dimethylamino)-9H-xanthen-9-one by Stepwise Chemical Redox Cycling 逐步化学氧化还原循环合成3,6-二(二甲氨基)- 9h -杂原-9- 1
IF 0.7
Organic Syntheses Pub Date : 2020-01-01 DOI: 10.15227/orgsyn.097.0021
J. Bachman
{"title":"Synthesis of 3,6-Bis(dimethylamino)-9H-xanthen-9-one by Stepwise Chemical Redox Cycling","authors":"J. Bachman","doi":"10.15227/orgsyn.097.0021","DOIUrl":"https://doi.org/10.15227/orgsyn.097.0021","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"1 1","pages":""},"PeriodicalIF":0.7,"publicationDate":"2020-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67338969","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Discussion Addendum for: (S)-(-)-2-Allylcyclohexanone (2-Allylcyclohexan-1-one] (S)-(-)-2-烯丙基环己酮(2-烯丙基环己酮-1- 1)的讨论附录
IF 0.7
Organic Syntheses Pub Date : 2020-01-01 DOI: 10.15227/orgsyn.097.0079
M. Braun
{"title":"Discussion Addendum for: (S)-(-)-2-Allylcyclohexanone (2-Allylcyclohexan-1-one]","authors":"M. Braun","doi":"10.15227/orgsyn.097.0079","DOIUrl":"https://doi.org/10.15227/orgsyn.097.0079","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"115 1","pages":"79-95"},"PeriodicalIF":0.7,"publicationDate":"2020-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67339290","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Preparation of Asymmetric Phase-transfer Catalyst, 1,4-Bis((4S,5S)-1,3-bis(3,5-di-tert-butylbenzyl)-4,5-diphenylimidazolidin-2-ylidene)piperazine-1,4-diium chloride 不对称相转移催化剂1,4-二((4S,5S)-1,3-二(3,5-二叔丁基苄基)-4,5-二苯基咪唑烷-2-酰基)哌嗪-1,4-氯化二铵的制备
IF 0.7
Organic Syntheses Pub Date : 2020-01-01 DOI: 10.15227/orgsyn.097.0274
Esther Cai Xia Ang
{"title":"Preparation of Asymmetric Phase-transfer Catalyst, 1,4-Bis((4S,5S)-1,3-bis(3,5-di-tert-butylbenzyl)-4,5-diphenylimidazolidin-2-ylidene)piperazine-1,4-diium chloride","authors":"Esther Cai Xia Ang","doi":"10.15227/orgsyn.097.0274","DOIUrl":"https://doi.org/10.15227/orgsyn.097.0274","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"1 1","pages":""},"PeriodicalIF":0.7,"publicationDate":"2020-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67339796","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Preparation of O-Pivaloyl Hydroxylamine Triflic Acid o -戊酰羟胺三酸的制备
IF 0.7
Organic Syntheses Pub Date : 2020-01-01 DOI: 10.15227/orgsyn.097.0207
S. Makai, Eric Falk, B. Morandi
{"title":"Preparation of O-Pivaloyl Hydroxylamine Triflic Acid","authors":"S. Makai, Eric Falk, B. Morandi","doi":"10.15227/orgsyn.097.0207","DOIUrl":"https://doi.org/10.15227/orgsyn.097.0207","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"97 1","pages":"207-216"},"PeriodicalIF":0.7,"publicationDate":"2020-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67339649","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 6
Discussion Addendum for: Synthesis of Arylboronic Pinacol Esters from Corresponding Arylamines 讨论附录:由相应芳胺合成芳基硼醇酯
IF 0.7
Organic Syntheses Pub Date : 2020-01-01 DOI: 10.15227/orgsyn.097.0001
F. Mo
{"title":"Discussion Addendum for: Synthesis of Arylboronic Pinacol Esters from Corresponding Arylamines","authors":"F. Mo","doi":"10.15227/orgsyn.097.0001","DOIUrl":"https://doi.org/10.15227/orgsyn.097.0001","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"97 1","pages":"1-11"},"PeriodicalIF":0.7,"publicationDate":"2020-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67338888","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Synthesis of α-Bromoacetyl MIDA Boronate α-溴乙酰基MIDA硼酸盐的合成
IF 0.7
Organic Syntheses Pub Date : 2020-01-01 DOI: 10.15227/orgsyn.097.0157
C. Lee
{"title":"Synthesis of α-Bromoacetyl MIDA Boronate","authors":"C. Lee","doi":"10.15227/orgsyn.097.0157","DOIUrl":"https://doi.org/10.15227/orgsyn.097.0157","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"97 1","pages":"157-171"},"PeriodicalIF":0.7,"publicationDate":"2020-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67339432","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Asymmetric Michael Addition of Dimethyl Malonate to 2-Cyclopenten-1-one Catalyzed by a Heterobimetallic Complex. 异双金属配合物催化丙二酸二甲酯与2-环戊烯-1- 1的不对称Michael加成反应。
IF 0.7
Organic Syntheses Pub Date : 2020-01-01 DOI: 10.15227/orgsyn.097.0327
Nicholas J Fastuca, Alice R Wong, Victor W Mak, Sarah E Reisman
{"title":"Asymmetric Michael Addition of Dimethyl Malonate to 2-Cyclopenten-1-one Catalyzed by a Heterobimetallic Complex.","authors":"Nicholas J Fastuca, Alice R Wong, Victor W Mak, Sarah E Reisman","doi":"10.15227/orgsyn.097.0327","DOIUrl":"https://doi.org/10.15227/orgsyn.097.0327","url":null,"abstract":"A flame-dried 1L, three-necked round-bottomed flask with 24/40 joints and a 1.5” Teflon coated egg-shaped magnetic stir bar is brought into a nitrogen filled glovebox (Note 2). The flask is charged with gallium (III) chloride (5.0 g, 28.4 mmol, 1.0 equiv) (Notes 3 and 4). The flask is sealed with three rubber septa (one of which is fitted with an internal temperature probe) brought out of the glovebox, and put under positive pressure of nitrogen via a needle attached to a nitrogen line. Another flame-dried 1L, three-necked round-bottomed flask with 24/40 joints and a 1.5” Teflon coated egg-shaped magnetic stir bar is charged with (S)-(–)-1,1’-bi(2-naphthol) ((S)-BINOL, (S)-1) (16.26 g, 56.8 mmol, 2.0 equiv) (Note 5). The flask is sealed with three rubber septa (one of which is fitted with a thermometer) and evacuated and backfilled with nitrogen three times (5 minutes under vacuum per cycle). A flame-dried 500 mL round-bottomed flask with a 24/40 joint and a 1” Teflon coated egg-shaped magnetic stir bar is charged with sodium tert-butoxide (10.92 g,","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"97 ","pages":"327-338"},"PeriodicalIF":0.7,"publicationDate":"2020-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9128456/pdf/nihms-1808558.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10254905","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
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