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Large-Scale NaBr/Selectfluor Mediated Alcohol Oxidation: Conversion of (-)-Borneol into (-)-Camphor. 大规模NaBr/选择性氟介导的醇氧化：(-)-冰片转化为(-)-樟脑。
IF 0.7
Organic Syntheses Pub Date : 2025-01-01 Epub Date: 2025-02-28 DOI: 10.15227/orgsyn.102.0100
Shyam Sathyamoorthi
{"title":"Large-Scale NaBr/Selectfluor Mediated Alcohol Oxidation: Conversion of (-)-Borneol into (-)-Camphor.","authors":"Shyam Sathyamoorthi","doi":"10.15227/orgsyn.102.0100","DOIUrl":"10.15227/orgsyn.102.0100","url":null,"abstract":"<p><p>Checked by Sergio Armentia Matheu, Saad Shaaban, and Nuno Maulide.</p>","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"102 ","pages":"100-113"},"PeriodicalIF":0.7,"publicationDate":"2025-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11934096/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143710013","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis of Serine Derived Oxazolines Using a Molybdenum Dioxide Catalyst. 二氧化钼催化合成丝氨酸衍生恶唑啉。
IF 0.7
Organic Syntheses Pub Date : 2025-01-01 Epub Date: 2025-03-31 DOI: 10.15227/orgsyn.102.0156
Wyatt C Powell, Garrett E Evenson, Maciej A Walczak
{"title":"Synthesis of Serine Derived Oxazolines Using a Molybdenum Dioxide Catalyst.","authors":"Wyatt C Powell, Garrett E Evenson, Maciej A Walczak","doi":"10.15227/orgsyn.102.0156","DOIUrl":"10.15227/orgsyn.102.0156","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"102 ","pages":"156-184"},"PeriodicalIF":0.7,"publicationDate":"2025-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC12207748/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144529121","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Introducing Volume 100 of Organic Syntheses 介绍《有机合成》第100卷
Organic Syntheses Pub Date : 2024-08-01 DOI: 10.1002/0471264229.os100.01
Rick L. Danheiser
{"title":"Introducing Volume 100 of <i>Organic Syntheses</i>","authors":"Rick L. Danheiser","doi":"10.1002/0471264229.os100.01","DOIUrl":"https://doi.org/10.1002/0471264229.os100.01","url":null,"abstract":"Abstract For over one hundred years Organic Syntheses (OS) has provided the chemistry community with reliable procedures for the synthesis of organic compounds. Procedures for synthesizing specific compounds of interest comprised the subject of nearly all of the articles published in Organic Syntheses for many years. More recently, however, the majority of articles in Organic Syntheses showcase reactions serving to demonstrate a representative protocol for a generally useful synthetic method. “OS Perspectives” provide authors with an opportunity to provide personal perspectives on topics associated with the field of organic synthesis. Appropriate subjects for OS Perspectives include, but are not limited to, discussions of the following: Trends and developments in the strategies, methods, and the applications of organic synthetic chemistry; Trends and developments with regard to the community of researchers in the field; Reflections on how research in the field is carried out and published.","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"1 1","pages":"1-3"},"PeriodicalIF":0.0,"publicationDate":"2024-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"147911976","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Preparation of Radical Clocks Bearing Carbonyl Groups: Synthesis of N-Methoxy-N-methylspiro[cyclopropane-1,9'-fluorene]-2-carboxamide. 含羰基的辐射钟的制备：合成 N-甲氧基-N-甲基螺[环丙烷-1,9'-芴]-2-甲酰胺。
IF 0.7
Organic Syntheses Pub Date : 2024-01-01 Epub Date: 2024-03-23 DOI: 10.15227/orgsyn.101.0061
Nicole D Bartolo, Ryan N Robson, Collin H Witt, K A Woerpel
{"title":"Preparation of Radical Clocks Bearing Carbonyl Groups: Synthesis of <i>N</i>-Methoxy-<i>N</i>-methylspiro[cyclopropane-1,9'-fluorene]-2-carboxamide.","authors":"Nicole D Bartolo, Ryan N Robson, Collin H Witt, K A Woerpel","doi":"10.15227/orgsyn.101.0061","DOIUrl":"10.15227/orgsyn.101.0061","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"101 ","pages":"61-80"},"PeriodicalIF":0.7,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11326668/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142000480","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Platinum-Catalyzed Enantioselective Diboration of Monosubstituted Alkenes. 铂催化单取代烯烃的对映选择性二硼化反应。
IF 0.8
Organic Syntheses Pub Date : 2024-01-01 Epub Date: 2024-06-28 DOI: 10.15227/orgsyn.101.0229
Chenpeng Gao, Paul S Lee, James P Morken
{"title":"Platinum-Catalyzed Enantioselective Diboration of Monosubstituted Alkenes.","authors":"Chenpeng Gao, Paul S Lee, James P Morken","doi":"10.15227/orgsyn.101.0229","DOIUrl":"10.15227/orgsyn.101.0229","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"101 ","pages":"229-241"},"PeriodicalIF":0.8,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11851291/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143502452","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis of Benzyl-δ-Truxinate via Enantioselective [2+2] Photocycloaddition. 通过对映体选择性 [2+2] 光环加成法合成苄基-δ-三嗪酸。
IF 0.8
Organic Syntheses Pub Date : 2024-01-01
Rodrigo Villanueva, Ellie F Plachinski, Tehshik P Yoon
{"title":"Synthesis of Benzyl-δ-Truxinate via Enantioselective [2+2] Photocycloaddition.","authors":"Rodrigo Villanueva, Ellie F Plachinski, Tehshik P Yoon","doi":"","DOIUrl":"","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"101 ","pages":"309-326"},"PeriodicalIF":0.8,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11584058/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142710885","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Hydrodealkenylative Cleavage of C(sp3)-C(sp2) Bonds: Preparation of (1S, 3R)-3-Methylcyclohexan-1-ol. C(sp3)-C（sp2）键的氢脱烷基裂解：制备(1S, 3R)-3-甲基环己烷-1-醇。
IF 0.8
Organic Syntheses Pub Date : 2024-01-01 Epub Date: 2024-12-04 DOI: 10.15227/orgsyn.101.0488
Brady W Dehnert, Ohyun Kwon
{"title":"Hydrodealkenylative Cleavage of C(sp<sup>3</sup>)-C(sp<sup>2</sup>) Bonds: Preparation of (1<i>S</i>, 3<i>R</i>)-3-Methylcyclohexan-1-ol.","authors":"Brady W Dehnert, Ohyun Kwon","doi":"10.15227/orgsyn.101.0488","DOIUrl":"10.15227/orgsyn.101.0488","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"101 ","pages":"488-507"},"PeriodicalIF":0.8,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC12088641/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144101118","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Intramolecular Coupling for General Synthesis of Backbone Substituted Bicyclo[1.1.1]pentyl Boronates. 骨架取代双环[1.1.1]戊基硼酸盐合成的分子内偶联。
IF 0.7
Organic Syntheses Pub Date : 2024-01-01 Epub Date: 2024-05-16 DOI: 10.15227/orgsyn.101.0181
Jet Tsien, Yangyang Yang, René García-Del Valle, Jonathan M E Hughes, Byron K Peters, Rohan R Merchant, Qin Tian
{"title":"Intramolecular Coupling for General Synthesis of Backbone Substituted Bicyclo[1.1.1]pentyl Boronates.","authors":"Jet Tsien, Yangyang Yang, René García-Del Valle, Jonathan M E Hughes, Byron K Peters, Rohan R Merchant, Qin Tian","doi":"10.15227/orgsyn.101.0181","DOIUrl":"10.15227/orgsyn.101.0181","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"101 ","pages":"181-206"},"PeriodicalIF":0.7,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11824253/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143414155","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis of 4-(2,2-Difluorovinyl)benzonitrile through a Wittig-type Olefination of 4-Formylbenzonitrile. 4-甲酰基苯腈wittig型烯烃合成4-（2,2-二氟乙烯基）苯腈。
IF 0.7
Organic Syntheses Pub Date : 2024-01-01 DOI: 10.15227/orgsyn.101.0542
Andrew J Intelli, Jacob P Sorrentino, Ryan A Altman
{"title":"Synthesis of 4-(2,2-Difluorovinyl)benzonitrile through a Wittig-type Olefination of 4-Formylbenzonitrile.","authors":"Andrew J Intelli, Jacob P Sorrentino, Ryan A Altman","doi":"10.15227/orgsyn.101.0542","DOIUrl":"10.15227/orgsyn.101.0542","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"101 ","pages":"542-563"},"PeriodicalIF":0.7,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11756535/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143028958","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis of Enantioenriched NH-Sulfoximines by NH Transfer to Sulfoxides Using Ammonium Carbamate and (Diacetoxyiodo)benzene 氨基甲酸铵和(二乙酰氧基)苯催化氨转移合成对映体富集的NH-亚砜胺
IF 0.7
Organic Syntheses Pub Date : 2023-01-01 DOI: 10.15227/orgsyn.0100.0186
{"title":"Synthesis of Enantioenriched NH-Sulfoximines by NH Transfer to Sulfoxides Using Ammonium Carbamate and (Diacetoxyiodo)benzene","authors":"","doi":"10.15227/orgsyn.0100.0186","DOIUrl":"https://doi.org/10.15227/orgsyn.0100.0186","url":null,"abstract":"","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"1 1","pages":""},"PeriodicalIF":0.7,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"67334268","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
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