G. R. Reis, F. P. Silva, A. Oliveira-Ogliari, A. Faria-E-Silva, R. Moraes, V. R. Novais, M. Menezes
{"title":"An Experimental Thermally Deposited Coating for Improved Bonding to Glass-fiber Posts.","authors":"G. R. Reis, F. P. Silva, A. Oliveira-Ogliari, A. Faria-E-Silva, R. Moraes, V. R. Novais, M. Menezes","doi":"10.3290/j.jad.a37725","DOIUrl":"https://doi.org/10.3290/j.jad.a37725","url":null,"abstract":"PURPOSE To determine whether an experimental thermally deposited siloxane-methacrylate coating for use in industrial scale applications would improve the bond strength of resin-based materials to glass fiber posts (GFPs) without affecting their mechanical properties. MATERIALS AND METHODS An experimental 5% (w/v) solution of methacryloxypropyltrimethoxysilane was prepared. Two types of GFPs (Exacto, Angelus; White Post DC, FGM) were divided into the following groups: S: silane; SA: silane and adhesive; HS: 35% H₂O₂ and silane; HSA: 35% H₂O₂, silane and adhesive; Exp: siloxane-methacrylate coating (Si-O) via post immersion in experimental solution followed by heating; Exp-S: silane after Si-O treatment; Exp-A: adhesive after Si-O treatment; and Exp-SA: silane and adhesive after Si-O treatment. The posts were positioned in a mold to allow insertion of a dual-curing resin core, serially sectioned into beams, and subjected to microtensile bond strength (μTSB) testing. The three-point bending test and SEM/EDX analysis were used to assess the mechanical and surface properties of untreated GFPs that were etched with H₂O₂ or treated with Si-O. RESULTS Surface treatments affected the μTSB only for the Exacto GFPs. The highest μTBS (MPa) was observed in Exp-S and Exp-SA groups, whereas H₂O₂ etching resulted in intermediate values. The mechanical properties were not affected by surface treatments. Exacto GFPs had significantly higher flexural strength (σf) and flexural modulus (Ef) than did the White Post DC GFPs, but the latter were significantly stiffer (S) than Exacto, regardless of the surface treatment tested. H₂O₂ promoted morphological changes in post surfaces. The experimental treatment promoted deposition of Si onto the post surface, improving bond strengths of Exacto posts. CONCLUSION The proposed novel coating technique is a viable procedure for fiber post manufacturers to improve the μTSB of resin-based materials.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":"51 1","pages":"49-57"},"PeriodicalIF":0.0,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83677830","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
A. Khan, A. A. A. Al Kheraif, S. Jamaluddin, Mohamad Elsharawy, D. Divakar
{"title":"Recent Trends in Surface Treatment Methods for Bonding Composite Cement to Zirconia: A Reveiw.","authors":"A. Khan, A. A. A. Al Kheraif, S. Jamaluddin, Mohamad Elsharawy, D. Divakar","doi":"10.3290/j.jad.a37720","DOIUrl":"https://doi.org/10.3290/j.jad.a37720","url":null,"abstract":"PURPOSE To evaluate the in vitro studies conducted in the last six years on new zirconia materials to discover and explore current trends in bonding composite cement to zirconia substrate. MATERIALS AND METHODS An in-depth review of the in vitro studies performed between 2010 and 2016 was conducted, focusing on the current trends in surface conditioning methods for zirconia ceramic. PubMed was used for searching the literature. Resin composite bonding to zirconia, zirconia surface coating, and zirconia surface treatment method were the keywords used. Complete scientific articles were reviewed and evaluated for appropriateness. RESULTS The literature survey showed a variety of surface treatment techniques comprising grit blasting (laboratory or chairside) with or without silica-coated alumina particles, the use of materials containing phosphate monomers, different silanes and primers, laser irradiation, Si vapor-phase deposition, and selective infiltration etching. CONCLUSIONS The problem of composite cement bonding to zirconia has yet to be definitively solved. Nevertheless, the application of phosphate monomer on tribochemically silica-coated zirconia surfaces is currently the least complicated and most efficaceous means of bonding composite cement to zirconia. Selective infiltration etching seems to be a promising technique for establishing a durable bond between composite cement and zirconia, and should be studied further.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":"104 1","pages":"7-19"},"PeriodicalIF":0.0,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76117243","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Bond Strengths of Orthodontic Metal Brackets to Tribochemically Silica-coated Zirconia Surfaces Using Different 10-Methacryloyloxydecyl Dihydrogen Phosphate-containing Primers.","authors":"Na-Hyun Kim, Yoon-Ji Kim, Dong-Yul Lee","doi":"10.3290/j.jad.a37724","DOIUrl":"https://doi.org/10.3290/j.jad.a37724","url":null,"abstract":"PURPOSE To evaluate the effects of tribochemical silica coating and different 10-methacryloyloxydecyl dihydrogen phosphate (MDP)-containing primers on the shear bond strength (SBS) of orthodontic metal brackets to yttrium-stabilized tetragonal zirconia polycrystal (Y-TZP) surfaces. MATERIALS AND METHODS One hundred ninety polished Y-TZP specimens were randomly assigned to 19 groups (n = 10): 30 specimens were used for surface analyses after polishing with 600-grit silicon carbide paper, airborneparticle abrasion with 50-μm alumina (A), or tribochemical silica coating (CoJet [C]); 160 specimens were used in SBS testing of orthodontic metal brackets to Y-TZP after alumina airborne-particle abrasion or tribochemical silica coating and application of either ESPE-Sil (S) (ASn, ASa, CSn, CSa), Alloy Primer (AP) (AAPn, AAPa, CAPn, CAPa), Clearfil Ceramic Primer (CP) (ACPn, ACPa, CCPn, CCPa), or Scotchbond Universal (U) (AUn, AUa, CUn, CUa) and either stored in water for 24 h (non-aged, n) or thermocycled 5000 times (aged, a). The surface analyses and SBSs were statistically analyzed with ANOVA and Tukey's tests. RESULTS Both mechanically treated surfaces had significantly greater surface roughness and surface free energy than did the polished surfaces. The type of primer and aging significantly affected the bond strength. Among the thermocycled specimens, the AAPa, AUa, and CCPa groups showed the greatest SBS. CONCLUSION After alumina airborne-particle abrasion, the application of Alloy Primer, Clearfil Ceramic Primer, or Scotchbond Universal provided stable bonding to Y-TZP ceramics. After tribochemical silica coating, however, only Clearfil Ceramic Primer produced a durable bond to Y-TZP ceramics.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":"27 1","pages":"21-29"},"PeriodicalIF":0.0,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"74349682","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
A. F. Montagner, N. Opdam, J. de Munck, M. Cenci, B. Van Meerbeek, M. Huysmans
{"title":"Bonding Efficacy and Fracture Pattern of Adhesives Submitted to Mechanical Aging with the Rub&Roll Device.","authors":"A. F. Montagner, N. Opdam, J. de Munck, M. Cenci, B. Van Meerbeek, M. Huysmans","doi":"10.3290/j.jad.a37721","DOIUrl":"https://doi.org/10.3290/j.jad.a37721","url":null,"abstract":"PURPOSE To evaluate the effect of water storage and cyclic loading on the microtensile bond strength (μTBS) and fracture pattern of adhesives to dentin. MATERIALS AND METHODS Midcoronal dentin surfaces (n = 36) were prepared and composite restorations were built up using two adhesives (self-etch and etch-and-rinse). The specimens were randomly divided into 3 groups according to the aging conditions (n = 6): 1. CONTROL storage in water for 24 h (CO); 2. water storage: storage in water for 6 months (WS); 3. mechanical loading: 750,000 mechanical cycles (ML) using the Rub&Roll loading device. Specimens were sections into beams and the μTBS was tested. Fracture patterns were analyzed using stereomicroscopy and fractographic analysis was performed using SEM. μTBS data (n = 53-72 specimens) were subjected to two-way ANOVA and Tukey's post-hoc test. The chi-squared test was used to compare the distribution of failure modes (p < 0.05). RESULTS Aging conditions and adhesives significantly affected μTBS (p < 0.01). The CO group showed no difference between materials and had highest μTBS. After WS, the self-etch adhesive showed higher μTBS than did the etchand- rinse adhesive. ML resulted in lower μTBS for both adhesives. Materials (p < 0.01) and aging (p < 0.01) significantly influenced the distribution of failure modes. SEM analysis showed that specimens submitted to WS or ML showed features of degradation and fatigue at the fractured interface, depending on the adhesive. CONCLUSION Mechanical loading had a negative effect on the bonding efficacy of both adhesives and influenced the fracture pattern, with specimens presenting a different fracture surface from that observed in water-stored specimens.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":"31 1","pages":"59-68"},"PeriodicalIF":0.0,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"75278267","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Michael Sawalt, S. Paris, U. Blunck, F. Schwendicke
{"title":"Fracture Resistance and Cusp Deflection of Lined or Non-lined Composite and Glass Hybrid Restorations Over Residual Demineralized Dentin.","authors":"Michael Sawalt, S. Paris, U. Blunck, F. Schwendicke","doi":"10.3290/j.jad.a37719","DOIUrl":"https://doi.org/10.3290/j.jad.a37719","url":null,"abstract":"PURPOSE To assess the fracture resistance (FR) and cusp deflection (CD) of lined or non-lined composite (CO) and glass hybrid (GH) restorations over residual demineralized dentin. MATERIALS AND METHODS In 48 extracted human premolars, artificial residual demineralized dentin was induced on pulpo-axial walls of standardized cavities. Various restorations were placed over this demineralized dentin: an experimental GH, a composite restoration (OptiBond FL+Tetric EvoCeram) without lining, or composite restorations with non-setting (Hypocal) or setting (Dycal) calcium hydroxide lining. After thermomechanical cycling, groups (n = 12) were compared regarding their CD and FR. RESULTS CD did not differ significantly between groups. FR was significantly lower in teeth restored with GH (median: 238 N; 25th/75th percentiles: 191/287 N) than in those restored with lined or non-lined composites (median range: 517-569 N; p < 0.05/Mann-Whitney), which did not differ significantly from each other (p > 0.05). CONCLUSION Within the conditions of this in vitro study, CH lining of pulpo-axial walls had only limited impact on CD and FR. GH showed the lowest FR and might not be optimal for restoring deep or extended cavitated lesions.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":"39 1","pages":"77-82"},"PeriodicalIF":0.0,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"80662864","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Ferhan Egilmez, G. Ergun, I. Cekic-Nagas, P. Vallittu, L. Lassila
{"title":"Light Transmission of Novel CAD/CAM Materials and Their Influence on the Degree of Conversion of a Dual-curing Resin Cement.","authors":"Ferhan Egilmez, G. Ergun, I. Cekic-Nagas, P. Vallittu, L. Lassila","doi":"10.3290/j.jad.a37722","DOIUrl":"https://doi.org/10.3290/j.jad.a37722","url":null,"abstract":"PURPOSE To evaluate the light transmission characteristics of different types, shades, and thicknesses of novel CAD/CAM materials and their effect on the degree of conversion (DC) of a dual-curing resin cement. MATERIALS AND METHODS Square specimens (12 × 12 mm2) of three CAD/CAM materials - GC Cerasmart, Lava Ultimate, Vita Enamic - of different thicknesses (1.00, 1.50, and 2.00 mm, n = 5 per thickness) were irradiated with an LED unit. The amount of transmitted light was quantified. Thereafter, the DC% of the dual-curing resin cement (RelyX Ultimate) was recorded after 15 min using Fourier transform infrared spectroscopy. Statistical analysis was performed using two-way ANOVA followed by the Tukey's HSD post-hoc test at a significance level of p < 0.05. Regression analysis was performed to investigate the correlation between the DC and radiant energy, and the DC and thickness. RESULTS Although the type and shade of CAD/CAM material significantly affect transmitted light irradiation (p < 0.0001), degrees of conversion are similar when the CAD/CAM material or material shade were taken into consideration (p > 0.05). Conversely, material thickness significantly affected light transmission (p < 0.0001) and DC (p < 0.0001). Multiple effects of material, shade, and thickness did not significantly affect the evaluated parameters (p = 0.638 for light irradiation; p = 0.637 for DC). Linear regression analysis showed a correlation between delivered energy and DC% results of the Vita Enamic (R² = 0.4169, p < 0.0001). CONCLUSION Reduced light transmission in 2-mm-thick specimens of all CAD/CAM materials indicates that proper curing of the cement beneath CAD/CAM materials should be ensured.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":"44 1","pages":"39-48"},"PeriodicalIF":0.0,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"88161676","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Editorial: Editors are Not Publication Police.","authors":"R. Frankenberger, B. Van Meerbeek","doi":"10.3290/j.jad.a35627","DOIUrl":"https://doi.org/10.3290/j.jad.a35627","url":null,"abstract":"","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":"38 1","pages":"3"},"PeriodicalIF":0.0,"publicationDate":"2016-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83586046","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
S. Soliman, R. Preidl, Sabine Karl, N. Hofmann, G. Krastl, B. Klaiber
{"title":"Influence of Cavity Margin Design and Restorative Material on Marginal Quality and Seal of Extended Class II Resin Composite Restorations In Vitro.","authors":"S. Soliman, R. Preidl, Sabine Karl, N. Hofmann, G. Krastl, B. Klaiber","doi":"10.3290/j.jad.a35520","DOIUrl":"https://doi.org/10.3290/j.jad.a35520","url":null,"abstract":"PURPOSE To investigate the influence of three cavity designs on the marginal seal of large Class II cavities restored with low-shrinkage resin composite limited to the enamel. MATERIALS AND METHODS One hundred twenty (120) intact human molars were randomly divided into 12 groups, with three different cavity designs: 1. undermined enamel, 2. box-shaped, and 3. proximal bevel. The teeth were restored with 1. an extra-low shrinkage (ELS) composite free of diluent monomers, 2. microhybrid composite (Herculite XRV), 3. nanohybrid composite (Filtek Supreme XTE), and 4. silorane-based composite (Filtek Silorane). After artificial aging by thermocycling and storage in physiological saline, epoxy resin replicas were prepared. To determine the integrity of the restorations' approximal margins, two methods were sequentially employed: 1. replicas were made of the 120 specimens and examined using SEM, and 2. the same 120 specimens were immersed in AgNO3 solution, and the dye penetration depth was observed with a light microscope. Statistical analysis was performed using the Kruskal-Wallis and the Dunn-Bonferroni tests. RESULTS After bevel preparation, SEM observations showed that restorations did not exhibit a higher percentage of continuous margin (SEM-analysis; p>0.05), but more leakage was found than with the other cavity designs (p<0.05). The lowest percentage of continuous margin was observed in ELS restorations (p<0.05). More fractured margins were observed in the undermined enamel cavity design groups (p<0.05). CONCLUSION Bevel preparation failed to improve margin quality in large Class II composite restorations and is no longer recommended. However, undermined enamel should be removed to prevent enamel fractures.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":"1 1","pages":"7-16"},"PeriodicalIF":0.0,"publicationDate":"2016-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76062133","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}