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Crystal Structure of N-(4-Chloro-2-hydroxyphenyl)-5-methoxysalicylaldimine N-(4-氯-2-羟基苯基)-5-甲氧基水杨醛二胺的晶体结构
Analytical Sciences: X-ray Structure Analysis Online Pub Date : 2008-01-01 DOI: 10.2116/ANALSCIX.24.X145
A. Tavman
{"title":"Crystal Structure of N-(4-Chloro-2-hydroxyphenyl)-5-methoxysalicylaldimine","authors":"A. Tavman","doi":"10.2116/ANALSCIX.24.X145","DOIUrl":"https://doi.org/10.2116/ANALSCIX.24.X145","url":null,"abstract":"The crystal structure of N-(4-chloro-2-hydroxyphenyl)-5-methoxysalicylaldimine was determined by X-ray diffraction at room temperature. The compound crystallizes in an orthorhombic system, and space group P212121. Unit-cell dimensions are the following: a = 7.3074(5)A, b = 8.3166(7)A, c = 21.782(2)A, V = 1323.7(2)A3, Z = 4. The molecule is non-planar and twisted around a C-N single bond. The molecule has N…H-O type intramolecular hydrogen bonding.","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"13 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"84340685","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Synthesis and Crystal Structure of Cd3(dppz)2(cis-chdc)2(trans-chdc)[dppz = dipyrido[3,2-a:2′,3′-c]phenazine and chdc = 1,4-cyclohexanedicarboxylate] Cd3(dppz)2(顺式-chdc)2(反式-chdc)[dppz =二吡啶[3,2-a:2′，3′-c]吩那嗪和chdc = 1,4-环己二羧酸盐]的合成与晶体结构
Analytical Sciences: X-ray Structure Analysis Online Pub Date : 2008-01-01 DOI: 10.2116/ANALSCIX.24.X221
J. Han, De-li Liu, P. Gao, Ning Li
{"title":"Synthesis and Crystal Structure of Cd3(dppz)2(cis-chdc)2(trans-chdc)[dppz = dipyrido[3,2-a:2′,3′-c]phenazine and chdc = 1,4-cyclohexanedicarboxylate]","authors":"J. Han, De-li Liu, P. Gao, Ning Li","doi":"10.2116/ANALSCIX.24.X221","DOIUrl":"https://doi.org/10.2116/ANALSCIX.24.X221","url":null,"abstract":"The coordination polymer Cd3(dppz)2(cis-chdc)2(trans-chdc) (dppz = dipyrido[3,2-a:2′,3′-c]phenazine and chdc = 1,4-cyclohexanedicarboxylate) (1), with the formula C60H50Cd3N8O12 was synthesized and the crystal structure was determined by single-crystal X-ray diffraction. The complex belongs to a triclinic system, space group P1 with a = 8.6338(17)A, b = 10.774(2)A, c = 14.872(3)A, α = 77.23(3)°, β = 81.77(3)°, γ = 82.80(3)°. The chdc2- carboxylates bridge the Cd(II) cations to form rare trinuclear Cd(II) clusters. The cis-chdc2- ligands are held together by the trinuclear Cd(II) clusters to generate a double-stranded chain. Further, the trans-chdc2- ligands bridge adjacent double-stranded chains to yield an interesting two-dimensional framework.","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"24 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"85536394","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis and crystal structure of 6-p-hydroxyphenyl-5,6-dihydrobenzoimidazo[1,2-c]quinazoline. 6-对羟基苯基-5,6-二氢苯并咪唑[1,2-c]喹唑啉的合成与晶体结构
Analytical Sciences: X-ray Structure Analysis Online Pub Date : 2008-01-01 DOI: 10.2116/ANALSCIX.24.X39
S. Naveen, Rita Bhattacharjee, V. Gayathri, S. Anandalwar, J. S. Prasad
{"title":"Synthesis and crystal structure of 6-p-hydroxyphenyl-5,6-dihydrobenzoimidazo[1,2-c]quinazoline.","authors":"S. Naveen, Rita Bhattacharjee, V. Gayathri, S. Anandalwar, J. S. Prasad","doi":"10.2116/ANALSCIX.24.X39","DOIUrl":"https://doi.org/10.2116/ANALSCIX.24.X39","url":null,"abstract":"The title compound, C20H15N3O, was synthesized and the structure was investigated by X-ray crystallography. The compound crystallizes in the triclinic crystal class in the space group P1 with cell parameters a = 7.724(6)A, b = 9.059(6)A, c = 12.186(1)A, α = 78.588(5)°, β = 73.630(4)°, γ = 70.924(5)° Z = 2. The dihydropyrimidine ring in the quinazoline moiety is in an skew-boat conformation. The structure exhibits intermolecular hydrogen bonds of the type N-H…O and O-H…N.","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"28 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"79508417","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Synthesis and Crystal Structure of Di-p-bromobenezenesulfonyl-macluraxanthone 二对溴苯磺酰基大杉酮的合成及晶体结构
Analytical Sciences: X-ray Structure Analysis Online Pub Date : 2008-01-01 DOI: 10.2116/ANALSCIX.24.X71
N. Boonnak, S. Chantrapromma, Hoong-Kun Fun, Chatchanok Karalai
{"title":"Synthesis and Crystal Structure of Di-p-bromobenezenesulfonyl-macluraxanthone","authors":"N. Boonnak, S. Chantrapromma, Hoong-Kun Fun, Chatchanok Karalai","doi":"10.2116/ANALSCIX.24.X71","DOIUrl":"https://doi.org/10.2116/ANALSCIX.24.X71","url":null,"abstract":"The title compound was synthesized and characterized by single crystal X-ray diffraction. The compound crystallizes in the triclinic space group P1; a = 7.4092(5), b = 13.9154(11), c = 16.9139(11)A, α = 101.576(4), β = 95.892(4) and γ = 99.859(4)°, V = 1666.1(2)A3, Z = 2 and Dx = 1.661 g cm-3. In the molecular structure, the xanthene ring system is essentially planar and the chromene ring adopts a screw boat conformation. The 1,1-dimethyl-2-propenyl substituent is planarly attached to the attached benzene ring whereas the two p-bromobenzenesulfonyl groups are bisectionally and axially attached to the attached benzene ring. O-H…O intramolecular hydrogen bonds were observed in the molecular structure. In the crystal packing, the molecules are linked by weak C-H…O intermolecular interactions forming chains along the c-axis. The crystal structure is stabilized by intramolecular O-H…O hydrogen bond and weak C-H…O intra-and intermolecular interactions.","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"24 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"81777456","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis and Crystal Structure of Tetraethylammonium Tris(1,10-phenanthroline)manganese(II) triperchlorate (Et4N)[Mn(phen)3](ClO4)3 三(1,10-菲罗啉)锰(II)三高氯酸四乙基铵(Et4N)[Mn(phen)3](ClO4)3的合成与晶体结构
Analytical Sciences: X-ray Structure Analysis Online Pub Date : 2008-01-01 DOI: 10.2116/ANALSCIX.24.X33
Cheng-Bing Ma, Changneng Chen, Qiutian Liu
{"title":"Synthesis and Crystal Structure of Tetraethylammonium Tris(1,10-phenanthroline)manganese(II) triperchlorate (Et4N)[Mn(phen)3](ClO4)3","authors":"Cheng-Bing Ma, Changneng Chen, Qiutian Liu","doi":"10.2116/ANALSCIX.24.X33","DOIUrl":"https://doi.org/10.2116/ANALSCIX.24.X33","url":null,"abstract":"The title complex was serendipitously obtained by reacting imidazole-4,5-dicarboxylic acid, tetraethylammonium hydroxide, 1,10-phenanthroline, and manganese(II) perchlorate hexahydrate in ethanol-water mixed solvent. It crystallizes in the monoclinic system, space group Cc with a = 24.8043(6), b = 8.7973(2), c = 24.2475(2)A, β = 118.844(1)°, V = 4634.6(2)A3 and Z = 4. A most noteworthy structural feature is that two counterions, namely Et4N+ and ClO4- cocrystallize in the crystal lattice.","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"72 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83397868","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal Structure of 5-Methyl-2-(phenylazo)pyridine 5-甲基-2-(苯偶氮)吡啶的晶体结构
Analytical Sciences: X-ray Structure Analysis Online Pub Date : 2008-01-01 DOI: 10.2116/ANALSCIX.24.X99
K. Hansongnern, Uraiwan Changsaluk, C. Pakawatchai
{"title":"Crystal Structure of 5-Methyl-2-(phenylazo)pyridine","authors":"K. Hansongnern, Uraiwan Changsaluk, C. Pakawatchai","doi":"10.2116/ANALSCIX.24.X99","DOIUrl":"https://doi.org/10.2116/ANALSCIX.24.X99","url":null,"abstract":"The title compound, C12H11N3, was synthesized and characterized by X-ray diffraction analysis. In the molecule, the substituted pyridine ring is not coplanar with the azo group, and the angle between the pyridine ring and the azo plane is 7.6(2)°. However, the angle between the azo plane and the benzene ring is 9.7(2)°. The N=N distance is 1.228(2)A.","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"26 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"82615007","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Crystal Structure of (S)-1-(4-Chlorobenzoyl)-3-(1-hydroxy-3-phenylpropan-2-yl)thiourea (S)-1-(4-氯苯甲酰基)-3-(1-羟基-3-苯丙基-2-基)硫脲的晶体结构
Analytical Sciences: X-ray Structure Analysis Online Pub Date : 2008-01-01 DOI: 10.2116/ANALSCIX.24.X59
Junke Wang, Zhijin Lu, J. Bai, Yi Pan
{"title":"Crystal Structure of (S)-1-(4-Chlorobenzoyl)-3-(1-hydroxy-3-phenylpropan-2-yl)thiourea","authors":"Junke Wang, Zhijin Lu, J. Bai, Yi Pan","doi":"10.2116/ANALSCIX.24.X59","DOIUrl":"https://doi.org/10.2116/ANALSCIX.24.X59","url":null,"abstract":"(S)-1-(4-Chlorobenzoyl)-3-(1-hydroxy-3-phenylpropan-2-yl)thiourea was synthesized and the crystal structure was determined by single-crystal X-ray diffractometry. The carbonyl and thiocarbonyl moieties are pointing in approximately opposite directions, The unit-cell dimensions are a = 7.2302(13)A, b = 7.4899(15)A, c = 16.265(3)A with α = 93.6190(12)°, β = 90.035(2)°, γ = 90.0520(13)° and V = 879.1(3)A.","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"12 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"82938159","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Crystal Structure of 1,3,6-Tribromocarbazole 1,3,6-三溴咔唑的晶体结构
Analytical Sciences: X-ray Structure Analysis Online Pub Date : 2008-01-01 DOI: 10.2116/ANALSCIX.24.X189
A. Cowley, D. R. Johnston, D. Kays, D. Watkin
{"title":"Crystal Structure of 1,3,6-Tribromocarbazole","authors":"A. Cowley, D. R. Johnston, D. Kays, D. Watkin","doi":"10.2116/ANALSCIX.24.X189","DOIUrl":"https://doi.org/10.2116/ANALSCIX.24.X189","url":null,"abstract":"The crystal structure properties of 1,3,6-tribromocarbazole (1) are: orthorhombic, space group Pna21 with a = 17.3110(3)A, b = 4.5608(2)A, c = 14.9606(2)A, V = 1181.17(6)A3, Z = 4, R1 = 0.0267, wR2 = 0.0594 for the 2677 reflections (I > 3σ(I)). The solid state structure of 1 consists of layers of stacked molecules, with hydrogen bonding between the N-H bonds and the Br atoms of molecules on neighbouring stacks (H…Br distances = 2.840(1)A).","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"25 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"78763247","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis and Crystal Structure of Aqua[(E)-2-(2-((2,3-dimethyl-5-oxo-1-phenyl-2,5-dihydro-1H-pyrazol-4-ylimino)methyl)phenoxy)acetato]-triphenyltin(IV) 水[(E)-2-(2-(2,3-二甲基-5-氧-1-苯基-2,5-二氢- 1h -吡唑-4-酰基)甲基)苯氧基)乙酸]-三苯基锡(IV)的合成及晶体结构
Analytical Sciences: X-ray Structure Analysis Online Pub Date : 2008-01-01 DOI: 10.2116/ANALSCIX.24.X73
Xiao-Niu Fang, Jian-Hong Wu, Meng-Qiang Zhou, Ji-Wu Wen
{"title":"Synthesis and Crystal Structure of Aqua[(E)-2-(2-((2,3-dimethyl-5-oxo-1-phenyl-2,5-dihydro-1H-pyrazol-4-ylimino)methyl)phenoxy)acetato]-triphenyltin(IV)","authors":"Xiao-Niu Fang, Jian-Hong Wu, Meng-Qiang Zhou, Ji-Wu Wen","doi":"10.2116/ANALSCIX.24.X73","DOIUrl":"https://doi.org/10.2116/ANALSCIX.24.X73","url":null,"abstract":"","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"188 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"78829888","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal Structure of Bis(N-ethyl-N-phenyldithiocarbamato-κ2S,S′)-(2-ethyl-2-oxazoline-κ1N)zinc(II) 双(n -乙基- n -苯基二硫代氨基-κ 2s,S ')-(2-乙基-2-恶唑啉-κ 1n)锌(II)的晶体结构
Analytical Sciences: X-ray Structure Analysis Online Pub Date : 2008-01-01 DOI: 10.2116/ANALSCIX.24.X155
Robert A. Gossage, H. Jenkins
{"title":"Crystal Structure of Bis(N-ethyl-N-phenyldithiocarbamato-κ2S,S′)-(2-ethyl-2-oxazoline-κ1N)zinc(II)","authors":"Robert A. Gossage, H. Jenkins","doi":"10.2116/ANALSCIX.24.X155","DOIUrl":"https://doi.org/10.2116/ANALSCIX.24.X155","url":null,"abstract":"The title material was synthesised by the treatment of [Zn{S2CN(Et)(Ph)}2]2 with excess 2-ethyl-2-oxazoline. The crystal system is triclinic (space group P1 and Z = 2). The unit-cell dimensions are a = 10.2310(4)A, b = 11.4701(5)A, c = 12.1981(5)A with α = 85.952(1)°, β = 75.174(1)°, γ = 72.442(1)° and V = 1319.30(9)A3. The final R value is 0.0248 (4641 observed reflections: I > 2σ(I)). The Zn atom coordinates with two chelating dithiocarbamato groups and one N-bound oxazoline.","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"34 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"87405440","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 3
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