{"title":"N-(4-氯-2-羟基苯基)-5-甲氧基水杨醛二胺的晶体结构","authors":"A. Tavman","doi":"10.2116/ANALSCIX.24.X145","DOIUrl":null,"url":null,"abstract":"The crystal structure of N-(4-chloro-2-hydroxyphenyl)-5-methoxysalicylaldimine was determined by X-ray diffraction at room temperature. The compound crystallizes in an orthorhombic system, and space group P212121. Unit-cell dimensions are the following: a = 7.3074(5)A, b = 8.3166(7)A, c = 21.782(2)A, V = 1323.7(2)A3, Z = 4. The molecule is non-planar and twisted around a C-N single bond. The molecule has N…H-O type intramolecular hydrogen bonding.","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"13 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Crystal Structure of N-(4-Chloro-2-hydroxyphenyl)-5-methoxysalicylaldimine\",\"authors\":\"A. Tavman\",\"doi\":\"10.2116/ANALSCIX.24.X145\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The crystal structure of N-(4-chloro-2-hydroxyphenyl)-5-methoxysalicylaldimine was determined by X-ray diffraction at room temperature. The compound crystallizes in an orthorhombic system, and space group P212121. Unit-cell dimensions are the following: a = 7.3074(5)A, b = 8.3166(7)A, c = 21.782(2)A, V = 1323.7(2)A3, Z = 4. The molecule is non-planar and twisted around a C-N single bond. The molecule has N…H-O type intramolecular hydrogen bonding.\",\"PeriodicalId\":7796,\"journal\":{\"name\":\"Analytical Sciences: X-ray Structure Analysis Online\",\"volume\":\"13 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2008-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Analytical Sciences: X-ray Structure Analysis Online\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.2116/ANALSCIX.24.X145\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Analytical Sciences: X-ray Structure Analysis Online","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2116/ANALSCIX.24.X145","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 1
摘要
采用室温x射线衍射法测定了N-(4-氯-2-羟基苯基)-5-甲氧基水杨醛二胺的晶体结构。该化合物结晶为正交晶系，空间群为P212121。单元格尺寸如下:a = 7.3074(5) a, b = 8.3166(7) a, c = 21.782(2) a, V = 1323.7(2)A3, Z = 4。这种分子是非平面的，绕着一个碳氮单键旋转。该分子具有N…H-O型分子内氢键。
Crystal Structure of N-(4-Chloro-2-hydroxyphenyl)-5-methoxysalicylaldimine
The crystal structure of N-(4-chloro-2-hydroxyphenyl)-5-methoxysalicylaldimine was determined by X-ray diffraction at room temperature. The compound crystallizes in an orthorhombic system, and space group P212121. Unit-cell dimensions are the following: a = 7.3074(5)A, b = 8.3166(7)A, c = 21.782(2)A, V = 1323.7(2)A3, Z = 4. The molecule is non-planar and twisted around a C-N single bond. The molecule has N…H-O type intramolecular hydrogen bonding.
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