Journal of Food Measurement and Characterization最新文献

{"title":"Application of active packaging materials based on chitosan-baneh loaded with wormwood extract in oxidative, microbial, and sensory properties of cocktail sausage","authors":"Hana Khosravi,&nbsp;Abbas Khoshhal,&nbsp;Elahesadat Hosseini","doi":"10.1007/s11694-025-03117-9","DOIUrl":"10.1007/s11694-025-03117-9","url":null,"abstract":"<div><p>The shelf-life of cocktail sausage can be affected by lipid oxidation and microbial contamination. Utilizing natural antioxidant and antimicrobial agents such as plant extracts could potentially provide a solution to this issue. The objective of this research was to create an edible film using chitosan-baneh included encapsulated microemulsion <i>Artemisia absinthium L</i> (wormwood), and to examine the impact of the film on the preservation of cocktail sausage over 45 days under refrigerated storage conditions. GC/MS analysis of wormwood extract showed that Phenol, 2,3,5,6-tetramethyl, and Caryophyllene are the major compounds with frequency of 24.61% and 22.65%, respectively. The films incorporating encapsulated extract exhibited increased thickness compared to those containing non-encapsulated extract. In contrast, the solubility displayed a contrasting pattern. Notably, the coating film with a high concentration of wormwood extract (1.5%) exhibited the lowest water vapor permeability (WVP). Conversely, the film lacking extract demonstrated higher tensile strength (TS), a property that decreased upon the addition of encapsulated extract. Additionally, the extract’s effect on the amount of Elongation at break (EB) followed an inverse relationship. The smallest rise in pH, peroxide value (PV), thiobarbituric acid (TBA), and total microorganism count (TC) was seen in cocktail sausage with encapsulated film (1.5% wormwood extract) in comparison to the sample lacking extract. The samples that had a coating film with the encapsulated extract were rated the highest in sensory evaluation. Based on the results, the sample containing 1.5% encapsulated wormwood extract was recognized as the superior sample.</p></div>","PeriodicalId":631,"journal":{"name":"Journal of Food Measurement and Characterization","volume":"19 4","pages":"2383 - 2394"},"PeriodicalIF":2.9,"publicationDate":"2025-02-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143706891","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Authenticity assessment of honeydew honey based on phytochemical profile","authors":"Marko Jović,&nbsp;Petar Ristivojević,&nbsp;Dražen Lušić,&nbsp;Dušanka Milojković-Opsenica,&nbsp;Jelena Trifković","doi":"10.1007/s11694-025-03123-x","DOIUrl":"10.1007/s11694-025-03123-x","url":null,"abstract":"<div><p>Considering the health-beneficial properties of honeydew honey and difficulties in its authenticity assessment, a high-performance thin-layer chromatography (HPTLC) fingerprint method in combination with multivariate analysis was developed, in order to relate phenolic profiles of selected honey samples to their verified botanical origin and biological activity. The HPTLC chromatograms were obtained using two derivatization reagents, vanillin-sulfuric acid and 2,2-diphenyl-1-picrylhydrazyl (DPPH) solution. Phenolic profiles of samples indicated the uniformity within each honey variety, but also variability among different botanical origin. Chemometric evaluation, including principal component analysis and partial least squares discriminant analysis, hyphenated with chromatographic method provided a discriminative and predictive methodology for classification of Hungarian oak, Evergreen oak, Montpellier maple and Silver fir honey samples. The analysis highlighted the significance of specific phenolic compounds (e.g., <i>R</i>_<i>F</i> = 0.31, 0.41, 0.51) for distinguishing the samples, underscoring the potential for accurate botanical authentication of samples, particularly Hungarian oak honey, based on its chemical profile. The HPTLC-DPPH method demonstrated a high potential for differentiating samples based on antioxidant activity, offering an efficient alternative to other techniques for antioxidant activity determination. PLS-DA models successfully predicted the botanical origin of <i>Quercus</i> spp., Evergreen oak and Hungarian oak. This approach can be useful for ensuring the quality control of honeydew honey products, providing an efficient and resource-saving alternative to more advanced analytical techniques. Additionally, caffeic acid emerged as the most potent antioxidant across the selected honeydew honey varieties. This highlights the potential of caffeic acid as a key bioactive compound contributing to the health-promoting properties of honeydew honey.</p></div>","PeriodicalId":631,"journal":{"name":"Journal of Food Measurement and Characterization","volume":"19 4","pages":"2449 - 2460"},"PeriodicalIF":2.9,"publicationDate":"2025-02-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143706895","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Recovery of valuable compounds from apricot concentrate production waste using supercritical carbon dioxide extraction as a green separation method","authors":"Mehmet Emin Argun,&nbsp;Mustafa Şamil Argun","doi":"10.1007/s11694-025-03118-8","DOIUrl":"10.1007/s11694-025-03118-8","url":null,"abstract":"<div><p>Apricot concentrate production wastewater (APW), which contains significant amounts of phenolic compounds and exhibits antioxidant activity, is also a major environmental pollutant. This study aimed to recover valuable compounds from APW and mitigate its environmental impact using the supercritical carbon dioxide (SC–CO₂) extraction method. Pressure and temperature variables were studied within the ranges of 8.5–31.5 MPa and 38.5–61.5 °C, respectively. A five–level central composite design (CCD) was applied to statistically analyze the interaction between experimental conditions and results. As a result of the extraction, up to 25% yield and 3.3% total phenolic content (TPC) recovery were achieved, along with a functional extract containing over 2000 mg GAE/L phenolic substances, antioxidant activity exceeding 3000 µM TE, and a significant amount of polyunsaturated fatty acids. Using response surface methodology, the optimum conditions for SC–CO₂ extraction were determined to be 60 °C and 10 MPa. Toxicity values across three trophic levels, along with selected pollution parameters, were assessed before and after the extraction. Notably, following the extraction process, the toxic classification of the wastewater, as determined by the <i>Daphnia magna</i> toxicity test, improved from the very toxic category (Class IV) to the toxic category (Class III).</p></div>","PeriodicalId":631,"journal":{"name":"Journal of Food Measurement and Characterization","volume":"19 4","pages":"2395 - 2408"},"PeriodicalIF":2.9,"publicationDate":"2025-02-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://link.springer.com/content/pdf/10.1007/s11694-025-03118-8.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143706892","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Co-encapsulation of catechin and L-lysine in water-in-oil-in-water (W1/O/W2) double emulsion using membrane emulsification process: application in carrot based infant-purée","authors":"Eya Soussi,&nbsp;Nayrouz Yahyaoui,&nbsp;Moncef Chouaibi,&nbsp;Salem Hamdi","doi":"10.1007/s11694-025-03128-6","DOIUrl":"10.1007/s11694-025-03128-6","url":null,"abstract":"<div><p>This present study is aimed to encapsulate L-lysine and catechin in a double emulsion using a membrane process. Therefore, the obtained data revealed that the encapsulation efficiency, mean average droplet, globule sizes, and polydispersity index ranged from 67.3 to 93.12%, 260 to 149.40 nm, 10.20 to 12.80 µm, and 0.13 to 0.164, respectively. Moreover, the pasteurization exhibits an insignificant decrease in encapsulation efficiency (EE), and a low increase in the mean diameter of globules, and polydispersity index (PDI) (<i>p</i> &gt; 0.05). In addition, pea protein isolate and chitosan in the external water phase notably exhibits the lowest degradation rate constant (k). Also, the results demonstrated that an increase of the volume fraction of the globules (Φ_g), from 10 to 70 wt%, decreases the released L-lysine and catechin contents. Likewise, the effect of added catechin-lysine double emulsion, ranging from 0 to 10% (w/w), assisted with pasteurization on quality attributes of carrot purée samples was also investigated. Lys-Cat-double emulsion preserved the color of carrot purée samples and exhibited microbiological counts below the limit level during 90 days of refrigerated storage (4 °C). Furthermore, the rheological properties of the carrot purée samples showed that they are non-Newtonian liquids with pseudoplastic or shear-thinning behavior with a predominance of viscous modulus (G″) through the frequency range. Finally, these findings revealed a possible use of Lys-Cat-double emulsion, to promote the inhibition of microbial proliferation and enzymatic activities, improve the nutritional and functional properties, and preserve the quality attributes of carrot purée.</p></div>","PeriodicalId":631,"journal":{"name":"Journal of Food Measurement and Characterization","volume":"19 4","pages":"2505 - 2531"},"PeriodicalIF":2.9,"publicationDate":"2025-02-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143706867","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Effect of microwave-vacuum drying on some nutritional and quality characteristics of rosehips","authors":"Mahir Cin,&nbsp;T. Koray Palazoğlu","doi":"10.1007/s11694-025-03105-z","DOIUrl":"10.1007/s11694-025-03105-z","url":null,"abstract":"<div><p>Microwave-vacuum drying of rosehips (<i>Rosa canina</i>) was investigated and the effect of microwave power and vacuum level on some nutritional and quality characteristics was determined. Microwave-vacuum drying experiments were carried out at three microwave power levels (50, 100, and 150 W) and three pressure levels (4, 7.5, and 11 kPa (abs)). Rosehips were dried also by hot air (60 °C) and freeze-drying methods for comparison. Experiments were conducted until a moisture content of less than 10% by weight was achieved. Dried samples were subjected to some physical and chemical analyses. The final product obtained by microwave-vacuum drying was superior to the hot-air dried and comparable to the freeze-dried sample. Microwave-vacuum drying treatments were completed 75–195 min whereas 960 min was needed for hot air drying. It was shown that good quality dried rosehips with 75–90% of the initial vitamin C content can be manufactured by microwave-vacuum drying method.</p></div>","PeriodicalId":631,"journal":{"name":"Journal of Food Measurement and Characterization","volume":"19 4","pages":"2233 - 2251"},"PeriodicalIF":2.9,"publicationDate":"2025-02-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://link.springer.com/content/pdf/10.1007/s11694-025-03105-z.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143706881","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Formulation and optimization of plant based organic coating with citrus peel extract for enhancing shelf life and quality of postharvest litchi fruit","authors":"Shubham Patidar,&nbsp;Purnima Kumari,&nbsp;Anupama Singh,&nbsp;N. C. Shahi,&nbsp;Khan Chand,&nbsp;Afzal Hussain,&nbsp;Waseem Ahmad,&nbsp;U. C. Lohani,&nbsp;Sanjay Kumar","doi":"10.1007/s11694-025-03115-x","DOIUrl":"10.1007/s11694-025-03115-x","url":null,"abstract":"<div><p>Edible coatings have become a promising solution to reduce post-harvest losses, extend shelf life, and preserve the quality of fresh produce. Given the perishability of fruits like Litchi and the substantial post-harvest losses they face, developing sustainable, plant-based coatings offers a promising alternative to conventional preservation methods, which often involve synthetic materials or chemicals. The objective of the present investigation was to formulate and optimize a plant based organic coating powder (OCP) using potato peel starch, gum arabic, and Kinnow peel extract, and to evaluate its effectiveness in enhancing the postharvest storage life and quality attributes of Litchi Fruit. A total 17 experimental runs were carried out by using Box–Behnken design with process parameters, i.e., starch-to-gum ratio (1:1, 2:1, and 3:1), peel extract (0.2%, 0.3%, and 0.4%), and particle size (300 µ, 450 µ, and 600 µ). Design Expert software (ver. 13.0.1) was employed for numerical optimization of the experimental results. The optimized values for OCP were found to be starch-to-gum ratio (1:1), peel extract (0.4%), and particle size (300 µ). The optimized parameters were used to develop the OCP and its effectiveness on Litchi fruit was analysed during 6 day of storage study. Coated litchi fruit experienced minimal weight loss and microbial load compared to the control sample, and its color attributes were better preserved. This study demonstrates the potential of using a sustainable, plant-based coating to extend the shelf life of perishable fruits, offering a safer and eco-friendly alternative for postharvest management in the food industry.</p></div>","PeriodicalId":631,"journal":{"name":"Journal of Food Measurement and Characterization","volume":"19 4","pages":"2350 - 2365"},"PeriodicalIF":2.9,"publicationDate":"2025-02-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143707123","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Rapid GC-FID-based analysis of fatty acid content, nutritional indices, and quality assessment of Rana chensinensis ovum","authors":"Miao Chen,&nbsp;Yuezhen Wang,&nbsp;Yue Zhou,&nbsp;Kexin Zhang,&nbsp;Shihan Wang,&nbsp;Changli Zhang,&nbsp;Min Gao,&nbsp;Zhihan Wang,&nbsp;Yongsheng Wang","doi":"10.1007/s11694-025-03119-7","DOIUrl":"10.1007/s11694-025-03119-7","url":null,"abstract":"<div><p>To assess the nutritional value of <i>Rana chensinensis</i> ovum (RCO), fatty acid fingerprinting using gas chromatography (GC) in conjunction with quantitative analysis of multiple components using a single marker (QAMS) was applied. Through analysis of the standard fingerprint of thirteen RCO samples from Northeast China, eleven common peaks were identified, including palmitic acid (C16:0), palmitoleic acid (C16:1), stearic acid (C18:0), oleic acid (OA, C18:1n9c), linoleic acid (LA, C18:2n6), α-linolenic acid (ALA, C18:3n3), paullinic acid (C20:1), eicosadienoic acid (C20:2), arachidonic acid (ARA, C20:4n6), eicosapentaenoic acid (EPA, C20:5n3) and docosahexaenoic acid (DHA, C22:6n3). In QAMS, methyl oleate served as the internal reference, and relative correction factors were calculated for the remaining ten components. Compared with internal standard method, this QAMS method is feasible (RSD &lt; 4%, <i>p</i> &gt; 0.05, cos θ &gt; 0.9999) and is more advantageous in terms of speed and cost-effectiveness. The RCO samples were categorized into four groups using hierarchical cluster analysis (HCA) and principal component analysis (PCA). Additionally, partial least squares-discriminant analysis (PLS-DA) was used to identify four important categorical variables: ALA, C16:0, LA, and ARA. In this work, a useful framework for quality control is provided by the effective application of GC fingerprinting and QAMS in the qualitative and quantitative evaluation of RCO.</p></div>","PeriodicalId":631,"journal":{"name":"Journal of Food Measurement and Characterization","volume":"19 4","pages":"2409 - 2424"},"PeriodicalIF":2.9,"publicationDate":"2025-02-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143707125","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Development and characterization of biodegradable polyvinyl alcohol/carboxymethyl cellulose composite films","authors":"Karanjit Kapila,&nbsp;Sushen Kirtania","doi":"10.1007/s11694-025-03121-z","DOIUrl":"10.1007/s11694-025-03121-z","url":null,"abstract":"<div><p>The objective of the present work was to investigate the effect of CMC biopolymer on the physicochemical, mechanical, thermal, barrier, and biodegradation properties of PVA-based films. The polymeric films were developed using solution casting method, incorporating CMC at concentrations ranging from 0.5 to 1.5%. With the addition of CMC, the tensile strength (TS) of the hybrid films was reduced from 1.40 ± 0.02 MPa to 1.99 ± 0.02 MPa. However, there was a significant improvement in the elongation at break (EAB) up to 49.29% compared to PVA film. The addition of CMC resulted in substantial improvements in water vapor permeability (WVP) and moisture retention capacity (MRC), showcasing a 38.73% improvement in WVP and a satisfactory MRC of 78.374% at 0.5% CMC concentration. The hybrid films also exhibit enhanced light absorbance at UV wavelength with opacity ranging from 0.301 to 1.413. TGA analysis showed a notable enhancement in the decomposition temperature of the hybrid PVA/CMC films, resulting in reduced mass loss compared to the PVA film. FTIR spectra confirmed that blending CMC with PVA led to the formation of strong hydrogen bonds within the polymer blend, significantly affecting the intermolecular forces inside the cellulose matrix. Moreover, with the addition of CMC, the degradation rate of the PVA/CMC film was increased approximately to 40% on the 30th day of soil burial. The films also exhibit effective microbial degradation against <i>Pseudomonas putida and Bacillus subtilis</i> bacteria strains as compared to commercial plastics. Overall, the obtained results validate the use of CMC biopolymer for blending of single polymer system as well as scaling down the extensive use of petroleum-based polymers in the field of packaging.</p></div>","PeriodicalId":631,"journal":{"name":"Journal of Food Measurement and Characterization","volume":"19 4","pages":"2425 - 2437"},"PeriodicalIF":2.9,"publicationDate":"2025-02-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143707071","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Advancing aflatoxin analytical techniques: harnessing next-generation technologies and industrial innovations for precision quantification and qualitative profiling—a prospective approach toward public health safeguarding","authors":"Ishrat Perveen,&nbsp;Muhammad Yaqoob,&nbsp;Sajid Hameed,&nbsp;Nazia Koser,&nbsp;Samia Nawab,&nbsp;Usama Amjad,&nbsp;Hina Younis,&nbsp;Sumbal Nazir,&nbsp;Akash John,&nbsp;Tallat Anwar Faridi,&nbsp;Naaz Abbas,&nbsp;Yasar Saleem,&nbsp;Shaista Nawaz,&nbsp;Sania Mazhar,&nbsp;Ayesha Kiran,&nbsp;Fatima Akram,&nbsp;Quratulain Syed,&nbsp;Syed Hussain Imam Abidi","doi":"10.1007/s11694-025-03109-9","DOIUrl":"10.1007/s11694-025-03109-9","url":null,"abstract":"<div><p>Aflatoxins (AFs), carcinogenic mycotoxins produced by <i>Aspergillus parasiticus</i> and <i>Aspergillus flavus</i>, frequently contaminate food commodities, posing global health risks. This study evaluates recent advancements in aflatoxin detection using next-generation technologies like mass spectrometry, high-performance liquid chromatography (HPLC), and immunoaffinity chromatography, to enhancing improved accuracy, sensitivity, and efficiency. The innovations in the food processing, agriculture, and pharmaceutical sectors have been explored in the study, focusing on improved detection and mitigation strategies. These developments offer greater precision in both quantification and qualitative profiling of aflatoxins, addressing global food safety challenges. High-Performance Liquid Chromatography (HPLC) with fluorescence detection (FL) has achieved a limit of detection (LOD) as low as 0.05 ng/mL, improving sensitivity by 15%. Immunoaffinity chromatography has increased AFs recovery rates by 30%, offering greater accuracy in high-fat matrices like nuts and oils. Electrochemical immunosensors have shown a 20% increase in detection accuracy. Liquid–liquid microextraction (LLME) has reduced solvent use by 20%, promoting more sustainable testing. HPLC coupled with mass spectrometry (LC–MS) has improved detection accuracy by 25%, enabling simultaneous detection of multiple AFs, including AFB1, AFB2, AFG1, and AFG2, with a LOD of 0.03–2.23 μg/kg. These advancements have led to a worldwide reduction in AF levels, driven by precise, rapid, and specific detection techniques. This review critically assesses these methods, highlights their advantages and limitations, and emphasizes the need for harmonized testing protocols and regulatory compliance. By advancing aflatoxin analytical techniques, this study contributes to a prospective approach toward safeguarding public health and ensuring global food safety.</p><h3>Graphical abstract</h3>\u0000<div><figure><div><div><picture><source><img></source></picture></div></div></figure></div></div>","PeriodicalId":631,"journal":{"name":"Journal of Food Measurement and Characterization","volume":"19 4","pages":"2155 - 2171"},"PeriodicalIF":2.9,"publicationDate":"2025-02-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143707120","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Enhancing the black truffle polysaccharide extraction efficiency using a combination of natural deep eutectic solvents and ultrasound-assisted techniques","authors":"Yi Wu,&nbsp;Hui Hu,&nbsp;Guangzhen Yang,&nbsp;Yifan Chen,&nbsp;Xiaoyu Zhong,&nbsp;Shanshan Li,&nbsp;Ming Pan,&nbsp;Yuanbin Li,&nbsp;Jiaheng Zhang","doi":"10.1007/s11694-024-03073-w","DOIUrl":"10.1007/s11694-024-03073-w","url":null,"abstract":"<div><p>Natural deep eutectic solvents (NaDESs) with ultrasound-assisted (UAE) method was used to improve the extraction efficiency of polysaccharide from black truffles, which can overcome the limitations of conventional methods. It demonstrated that the extraction efficiency of polysaccharide by six NaDESs with UAE were better than those of conventional solvents. Among the NaDESs, betaine-citric acid (BetCi) NaDES showed the best performance, achieving a remarkable extraction yield of 9.38%, outperforming water, ethanol, and 1,3-butanediol by 0.4, 11.5 and 11.0 times, respectively. Moreover, the polysaccharide yield was further optimized by response surface method, based on three influence factors (NaDES concentration, liquid-to-solid, and ultrasonic time). Scanning electron microscopy images showed that compared to the traditional extraction methods, the plate-like structure fractured into smaller pieces of black truffles treated by BetCi NaDES with UAE, indicating deeper interactions between NaDES and black truffles. Furthermore, the skin penetration as well as antioxidant and anti-wrinkle properties of the black truffle polysaccharide extract were evaluated, revealing promising bioactivity. Overall, this study represents a comprehensive exploration of novel extraction methods, highlighting efficient polysaccharide extraction and its potential applications.</p></div>","PeriodicalId":631,"journal":{"name":"Journal of Food Measurement and Characterization","volume":"19 4","pages":"2208 - 2219"},"PeriodicalIF":2.9,"publicationDate":"2025-02-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143707027","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}