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New Cesium-Containing Quartzoid Glasses 新型含铯石英玻璃
IF 0.7 4区 材料科学
Glass Physics and Chemistry Pub Date : 2023-11-16 DOI: 10.1134/S1087659622600417
T. A. Tsyganova, M. A. Girsova, L. N. Kurylenko, L. F. Dikaya, M. V. Staritsyn
{"title":"New Cesium-Containing Quartzoid Glasses","authors":"T. A. Tsyganova,&nbsp;M. A. Girsova,&nbsp;L. N. Kurylenko,&nbsp;L. F. Dikaya,&nbsp;M. V. Staritsyn","doi":"10.1134/S1087659622600417","DOIUrl":"10.1134/S1087659622600417","url":null,"abstract":"<p>Information about new cesium-containing quartzoid glasses (QGs) obtained as a result of the heat treatment of high-silica porous glasses (PGs) impregnated with aqueous solutions of CsNO<sub>3</sub> is presented. Quartzoid glasses have been studied by SEM, X-ray diffraction, flame photometry, and energy-dispersive X‑ray spectroscopy. It has been established that the total content of cesium in the synthesized QGs increases with an increase in the concentration of the impregnating solution of cesium nitrate and an increase in the impregnation time of PGs for the selected synthesis conditions.</p>","PeriodicalId":580,"journal":{"name":"Glass Physics and Chemistry","volume":"49 5","pages":"456 - 462"},"PeriodicalIF":0.7,"publicationDate":"2023-11-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"134796723","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Ion-Beam Synthesis of a Hidden Lead-Silicate Layer in Single-Crystal Silicon 单晶硅中隐藏铅酸盐层的离子束合成
IF 0.7 4区 材料科学
Glass Physics and Chemistry Pub Date : 2023-11-16 DOI: 10.1134/S1087659623600564
E. Yu. Buchin, Yu. I. Denisenko
{"title":"Ion-Beam Synthesis of a Hidden Lead-Silicate Layer in Single-Crystal Silicon","authors":"E. Yu. Buchin,&nbsp;Yu. I. Denisenko","doi":"10.1134/S1087659623600564","DOIUrl":"10.1134/S1087659623600564","url":null,"abstract":"<p>The features of the formation of a hidden lead-silicate insulating layer in silicon substrates are considered. To do this, ions of molecular oxygen and lead are sequentially implanted into them in an atomic ratio of 75 : 1 then annealing is carried out at a temperature of 1150°C in an environment of dry oxygen. The distribution of the implanted ions in the experimental samples is recorded by the method of secondary ion mass spectrometry. It is shown that the latent insulator is formed in the process of the spinodal decomposition of a solid solution of SiO<sub><i>x</i></sub>–PbO<sub><i>x</i></sub> in the form of a three-layer structure. Its middle part is silicon dioxide doped with lead ions and the side parts consist of a lead-silicate phase. A relaxation diffusion model is proposed to analyze the distribution profile of lead.</p>","PeriodicalId":580,"journal":{"name":"Glass Physics and Chemistry","volume":"49 5","pages":"535 - 537"},"PeriodicalIF":0.7,"publicationDate":"2023-11-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"134796904","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Adsorption of Norfloxacin by Titanium-Doped Mesoporous Bioactive Glass: Kinetics, Isotherms, Thermodynamic and Regenerable Studies 掺钛介孔生物活性玻璃吸附诺氟沙星:动力学、等温线、热力学和可再生研究
IF 0.7 4区 材料科学
Glass Physics and Chemistry Pub Date : 2023-11-16 DOI: 10.1134/S1087659623600473
Liying Li, Song Kang, Yanbin Bu, Qingzhe Zhou, Jianhua Feng
{"title":"Adsorption of Norfloxacin by Titanium-Doped Mesoporous Bioactive Glass: Kinetics, Isotherms, Thermodynamic and Regenerable Studies","authors":"Liying Li,&nbsp;Song Kang,&nbsp;Yanbin Bu,&nbsp;Qingzhe Zhou,&nbsp;Jianhua Feng","doi":"10.1134/S1087659623600473","DOIUrl":"10.1134/S1087659623600473","url":null,"abstract":"<p>A series of Titanium-doped mesoporous bioactive glass with different Si-Ca ratios (MBG-Ti-1– MBG-Ti-5) were prepared by the sol-gel method. These materials were used to adsorb Norfloxacin (NOR) pollutant from aqueous solution. The morphology, microstructure and chemical properties of MBG-Ti-3 were characterized by transmission electron microscopy (TEM), scanning electron microscope (SEM), energy dispersive spectrometer (EDS), X-ray diffraction (XRD) and X-ray photoelectron spectroscopy (XPS). The N<sub>2</sub> adsorption-desorption isotherm and pore size distribution of MBG-Ti-3 were investigated by the Brunauer–Emmett–Teller (BET) method and Barret–Joyner–Halenda (BJH) method. The specific surface of MBG-Ti-3 was 126.68 m<sup>2</sup>/g and the pore size was about 15 nm. The effect of time, initial concentration, pH and temperature on the adsorption of NOR were investigated. The maximum adsorption efficiency was 68% at 30°C, pH 8.0. Moreover, adsorption of NOR onto MBG-Ti-3 could be well fitted with the pseudo-first-order model and the pseudo-second-order model. Furthermore, adsorption was spontaneous, exothermic process of reduced entropy by analyzing thermodynamic model. Through the analysis of adsorption model, plausible adsorption mechanism was proposed. MBG-Ti-3 exhibited better adsorption efficiency after recycle 3 times. Additionally, bioactive glass was eco-friendly attribute to biological suitability which could not cause secondly pollution for aquatic environment. As an environmentally friendly adsorbent, Titanium-doped mesoporous bioactive glass showed promising potential application in NOR antibiotics removal from aquatic environment.</p>","PeriodicalId":580,"journal":{"name":"Glass Physics and Chemistry","volume":"49 5","pages":"431 - 441"},"PeriodicalIF":0.7,"publicationDate":"2023-11-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"134796725","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Anisotropy of Thermal Expansion of Oxoborate Warwickite 氧化硼酸盐岩热膨胀的各向异性
IF 0.7 4区 材料科学
Glass Physics and Chemistry Pub Date : 2023-11-16 DOI: 10.1134/S1087659623600503
Y. P. Biryukov, R. S. Bubnova, S. K. Filatov
{"title":"Anisotropy of Thermal Expansion of Oxoborate Warwickite","authors":"Y. P. Biryukov,&nbsp;R. S. Bubnova,&nbsp;S. K. Filatov","doi":"10.1134/S1087659623600503","DOIUrl":"10.1134/S1087659623600503","url":null,"abstract":"<p>In this paper, the transition metal oxoborate warwickite (Fe<sup>2+</sup>,Mg)Fe<sup>3+</sup>(BO<sub>3</sub>)O is studied for the first time by low- and high-temperature X-ray diffraction in the temperature range from 93 to 513 K. The sharply anisotropic nature of its thermal expansion is revealed. A structural interpretation of the expansion mechanism is given both in terms of the contribution of cationic and oxocentered polyhedra.</p>","PeriodicalId":580,"journal":{"name":"Glass Physics and Chemistry","volume":"49 5","pages":"514 - 519"},"PeriodicalIF":0.7,"publicationDate":"2023-11-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"134796902","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Enhancement of Optical and Electrical Properties of Pr3+ Doped Na2O–ZnO–TeO2 Glass Materials Pr3+掺杂Na2O-ZnO-TeO2玻璃材料光学和电学性能的增强
IF 0.7 4区 材料科学
Glass Physics and Chemistry Pub Date : 2023-11-16 DOI: 10.1134/S108765962360045X
J. N. Mirdda, S. Mukhopadhyay, K. R. Sahu, M. N. Goswami
{"title":"Enhancement of Optical and Electrical Properties of Pr3+ Doped Na2O–ZnO–TeO2 Glass Materials","authors":"J. N. Mirdda,&nbsp;S. Mukhopadhyay,&nbsp;K. R. Sahu,&nbsp;M. N. Goswami","doi":"10.1134/S108765962360045X","DOIUrl":"10.1134/S108765962360045X","url":null,"abstract":"<p>Praseodymium incorporated Na<sub>2</sub>O–ZnO–TeO<sub>2</sub> (NZT) glass materials were prepared through usual melt quenching technique. The temperature of glass transition and the melting point were obtained by using thermal analyses. The amorphous and ionic nature of the prepared samples was obtained from the recorded X-ray diffraction pattern and FTIR spectra respectively. The optical band gap energy was calculated using UV-Vis absorption spectra and was observed to be decreased from 2.86 to 2.46 eV due to the increasing concentration of Pr<sup>3+</sup> ions. The peaks of absorption spectra were found. The intense emission was observed from the fluorescence measurement for the emission band of Pr<sup>3+</sup> doped glass materials. The doping of higher concentrations of Pr<sup>3+</sup> ions enhanced the intensity of the emission peaks. The CIE chromaticity coordinates were estimated from fluorescence spectra for pure and Pr<sup>3+</sup> doped glass samples to know the suitability of laser emission of these glass samples. The dielectric constant of the glass materials was observed to be independent of frequency in the large range of frequency (500 Hz to 2 MHz). The variation of conductivity of the glasses was exposed the Arrhenius mechanism of conduction with the temperature.</p>","PeriodicalId":580,"journal":{"name":"Glass Physics and Chemistry","volume":"49 5","pages":"442 - 455"},"PeriodicalIF":0.7,"publicationDate":"2023-11-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"134796987","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of Disorder in the Structure of a Ferroelectric Composite Material xPbSe·(1 – x)PbSeO3 on the Smearing of the Phase Transition 铁电复合材料xPbSe·(1 - x)PbSeO3结构无序对相变涂抹的影响
IF 0.7 4区 材料科学
Glass Physics and Chemistry Pub Date : 2023-08-14 DOI: 10.1134/S1087659623600278
V. V. Tomaev, D. P. Danilovich, S. S. Proshkin
{"title":"Effect of Disorder in the Structure of a Ferroelectric Composite Material xPbSe·(1 – x)PbSeO3 on the Smearing of the Phase Transition","authors":"V. V. Tomaev,&nbsp;D. P. Danilovich,&nbsp;S. S. Proshkin","doi":"10.1134/S1087659623600278","DOIUrl":"10.1134/S1087659623600278","url":null,"abstract":"<p>This paper analyzes the experimental and theoretical studies of the problem of a diffuse phase transition (PTC) in a composite material <i>x</i>PbSe⋅(1 – <i>x</i>)PbSeO<sub>3</sub>, in which <i>x</i> varies from 0 to 1. The decrease in stability in the virtual cubic phase of lead selenide (PbSe) is achieved by oxidizing it with atmospheric oxygen and forming a ferroelectric disordered monoclinic phase of lead selenite (PbSeO<sub>3</sub>). The mechanism of lead selenide oxidation by air oxygen is studied by X-ray diffractometry, optical reflection in the infrared region of the spectrum, X-ray emission analysis (the chemical shift method), nuclear magnetic resonance, studies of AC and DC conductivity, differential scanning calorimetry, and other methods. The reason for the smearing of the phase transition in the <i>x</i>PbSe⋅(1 – <i>x</i>)PbSeO<sub>3</sub> composite, in which <i>x</i> varies from 0 to 1, is analyzed based on the previously obtained experimental results of its detection.</p>","PeriodicalId":580,"journal":{"name":"Glass Physics and Chemistry","volume":"49 4","pages":"364 - 373"},"PeriodicalIF":0.7,"publicationDate":"2023-08-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"4563653","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Formation of Zn0.5Ni0.5Fe2O4 Nanocrystals in Conditions of Solution Combustion: Effect of the Type of Fuel on the Structure and Morphology 溶液燃烧条件下Zn0.5Ni0.5Fe2O4纳米晶的形成:燃料类型对结构和形貌的影响
IF 0.7 4区 材料科学
Glass Physics and Chemistry Pub Date : 2023-08-14 DOI: 10.1134/S108765962360028X
M. A. Gavrilova, D. A. Gavrilova, I. S. Kondrashkova, A. A. Krasilin
{"title":"Formation of Zn0.5Ni0.5Fe2O4 Nanocrystals in Conditions of Solution Combustion: Effect of the Type of Fuel on the Structure and Morphology","authors":"M. A. Gavrilova,&nbsp;D. A. Gavrilova,&nbsp;I. S. Kondrashkova,&nbsp;A. A. Krasilin","doi":"10.1134/S108765962360028X","DOIUrl":"10.1134/S108765962360028X","url":null,"abstract":"<p>Nickel-zinc ferrites, which have pronounced ferrimagnetic and semiconductor properties, can be used as promising magnetically controlled photocatalysts for the purification of aqueous media from organic pollutants. The value of the specific surface area largely affects the photocatalytic properties of the material; therefore, the possibility of its control and variation at the stage of synthesis is of great scientific and technical interest. In this study, nanocrystalline ferrite of the Zn<sub>0.5</sub>Ni<sub>0.5</sub>Fe<sub>2</sub>O<sub>4</sub> composition is obtained under conditions of solution combustion using various types of organic fuel as the main factor affecting the formation of the specific surface area, and subsequent heat treatment in air at a temperature of 500°C for 2 h. The crystal structure, chemical composition, and morphology of Zn<sub>0.5</sub>Ni<sub>0.5</sub>Fe<sub>2</sub>O<sub>4</sub> are studied by methods of X‑ray phase analysis, X-ray spectral microanalysis, and scanning electron microscopy. The values of the specific surface area of the synthesized nanopowders are calculated based on the method of liquid-phase adsorption from a Methylene Blue solution and the low-temperature adsorption-desorption of nitrogen. The results of the X‑ray phase analysis show that a single-phase nanocrystalline product with a spinel structure is formed, where the average crystallite size varies within 11–23 nm and is inversely related to the value of the specific surface area, respectively, after the reaction with succinic acid (39.1 m<sup>2</sup>/g) and with glycine (20.2 m<sup>2</sup>/g). It is established that the choice of the fuel largely affects the formation of nanocrystals and the specific surface area of the samples, and the approach used makes it possible to control its values.</p>","PeriodicalId":580,"journal":{"name":"Glass Physics and Chemistry","volume":"49 4","pages":"394 - 401"},"PeriodicalIF":0.7,"publicationDate":"2023-08-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"4561938","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Relationship of Temperature Dependences of Microhardness and Enthalpy of Glass on the Example of Selenium 以硒为例研究玻璃显微硬度与热焓的温度依赖性
IF 0.7 4区 材料科学
Glass Physics and Chemistry Pub Date : 2023-08-14 DOI: 10.1134/S1087659623600266
Shunbo Wang, Yu. S. Tver’yanovich
{"title":"Relationship of Temperature Dependences of Microhardness and Enthalpy of Glass on the Example of Selenium","authors":"Shunbo Wang,&nbsp;Yu. S. Tver’yanovich","doi":"10.1134/S1087659623600266","DOIUrl":"10.1134/S1087659623600266","url":null,"abstract":"<p>A model is proposed that makes it possible to calculate the temperature dependence of the microhardness of glass over the entire temperature range from the softening temperature to absolute zero. The calculation uses the temperature dependence of the glass enthalpy and the value of its microhardness at the glass transition temperature. The proposed model is tested on the example of glassy selenium. For this, the temperature dependence of the microhardness of selenium on the softening temperature up to 100 K, which is 50 K below its Debye temperature, is measured. Thus, a relationship is established between the strength and thermodynamic properties of glass.</p>","PeriodicalId":580,"journal":{"name":"Glass Physics and Chemistry","volume":"49 4","pages":"336 - 339"},"PeriodicalIF":0.7,"publicationDate":"2023-08-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"4563533","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Thermal Expansion of Fedotovite K2Cu3O(SO4)3 and Piypite K4Cu4O(SO4)4·(Na,Cu)Cl Fedotovite k2cu30o (SO4)3和Piypite k4cu40o (SO4)4·(Na,Cu)Cl的热膨胀
IF 0.7 4区 材料科学
Glass Physics and Chemistry Pub Date : 2023-08-14 DOI: 10.1134/S1087659623600333
A. P. Shablinskii, S. K. Filatov, Y. P. Biryukov, A. A. Yuriev, L. P. Vergasova
{"title":"Thermal Expansion of Fedotovite K2Cu3O(SO4)3 and Piypite K4Cu4O(SO4)4·(Na,Cu)Cl","authors":"A. P. Shablinskii,&nbsp;S. K. Filatov,&nbsp;Y. P. Biryukov,&nbsp;A. A. Yuriev,&nbsp;L. P. Vergasova","doi":"10.1134/S1087659623600333","DOIUrl":"10.1134/S1087659623600333","url":null,"abstract":"<p>This paper presents the results of a study of the thermal behavior of fedotovite K<sub>2</sub>Cu<sub>3</sub>O(SO<sub>4</sub>)<sub>3</sub> and piypite K<sub>4</sub>Cu<sub>4</sub>O(SO<sub>4</sub>)<sub>4</sub>∙(Na,Cu)Cl minerals in a wide temperature range. The crystal structure of the holotype piypite specimen is refined at room temperature. The mechanisms of thermal expansion of minerals depending on the crystal structure are described.</p>","PeriodicalId":580,"journal":{"name":"Glass Physics and Chemistry","volume":"49 4","pages":"386 - 393"},"PeriodicalIF":0.7,"publicationDate":"2023-08-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"4563540","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Thermal Expansion of Ba3Lu(BO3)3 Borate Ba3Lu(BO3)3硼酸盐的热膨胀
IF 0.7 4区 材料科学
Glass Physics and Chemistry Pub Date : 2023-08-14 DOI: 10.1134/S1087659623600291
Y. P. Biryukov, R. S. Bubnova
{"title":"Thermal Expansion of Ba3Lu(BO3)3 Borate","authors":"Y. P. Biryukov,&nbsp;R. S. Bubnova","doi":"10.1134/S1087659623600291","DOIUrl":"10.1134/S1087659623600291","url":null,"abstract":"<p>In this study, Ba<sub>3</sub>Lu(BO<sub>3</sub>)<sub>3</sub> borate obtained by solid-phase synthesis is explored by high-temperature X-ray powder diffraction in the temperature range from 25 to 900°C. At room temperature, the compound expands slightly anisotropically (α<sub>max</sub>/α<sub>min</sub> = 1.2), and with an increase in temperature, the degree of anisotropy increases significantly (α<sub>max</sub>/α<sub>min</sub> = 6.9 at 900°C). The maximum expansion is observed along the crystallographic axis <i>c</i> (α<sub><i>c</i></sub> = 10.45 <i>×</i> 10<sup>–6</sup>°C<sup>–1</sup> at 25°C and 36.34 <i>×</i> 10<sup>–6</sup>°C<sup>–1</sup> at 900°C), perpendicular to which the boron-oxygen triangles [BO<sub>3</sub>] are located, and the minimum is in the plane where the triangles are located.</p>","PeriodicalId":580,"journal":{"name":"Glass Physics and Chemistry","volume":"49 4","pages":"374 - 378"},"PeriodicalIF":0.7,"publicationDate":"2023-08-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"4563539","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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