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PREPARATION, STRUCTURE AND IONIC CONDUCTIVITY OF THE M0.9Y0.1O2–?–BiScO3 (M = Zr, Ce) M0.9Y0.1O2-?-BiScO3（M = Zr、Ce）的制备、结构和离子导性
Steklo i Keramika Pub Date : 2023-06-01 DOI: 10.14489/glc.2023.06.pp.054-059
I. Sudzhanskaya, V. S. Sotnikova
{"title":"PREPARATION, STRUCTURE AND IONIC CONDUCTIVITY OF THE M0.9Y0.1O2–?–BiScO3 (M = Zr, Ce)","authors":"I. Sudzhanskaya, V. S. Sotnikova","doi":"10.14489/glc.2023.06.pp.054-059","DOIUrl":"https://doi.org/10.14489/glc.2023.06.pp.054-059","url":null,"abstract":"Samples of Zr0.9Y0.1O2–?–BiScO3 and Сe0.9Y0.1O2–?–BiScO3 solid solutions were obtained by solid-phase synthesis. X-ray diffraction revealed that the Zr0.9Y0.1O2–?–BiScO3 system corresponds to a tetragonal structure with space symmetry group P42/nmc. The Сe0.9Y0.1O2–?–BiScO3 ceramics is two-phase and is characterized by a cubic structure with space symmetry groups and Ia–3. Using the impedance spectroscopy method, it was found that the Сe0.9Y0.1O2–?–BiScO3 system has the highest electrical conductivity, however, the activation energy is lower in the Zr0.9Y0.1O2–?–BiScO3 ceramics, amounting to 0.3 eV in the temperature range of 300–420 ?С and 0.7 eV in the temperature range 420–680 ?С. The activation energy of the Сe0.9Y0.1O2–?–BiScO3 solid solution is 1.0 eV.","PeriodicalId":445802,"journal":{"name":"Steklo i Keramika","volume":"43 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2023-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139371123","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
INFLUENCE OF CeO2 ON THE FORMATION OF PLASMONIC Au NANOPARTICLES IN GLASSES OF THE ZnO–MgO–Al2O3–SiO2 SYSTEM 二氧化 CeO2 对 ZnO-MgO-Al2O3-SiO2 系统玻璃中形成层状金纳米颗粒的影响
Steklo i Keramika Pub Date : 2023-06-01 DOI: 10.14489/glc.2023.06.pp.003-014
G. Y. Shakhgildyan, V. Durymanov, L. Avakyan, G. N. Atroshenko, M. Vetchinnikov, R. O. Alexeev, E. Ignat'eva, N. V. Golubev, A. A. Zolikova, L. Bugaev, V. Sigaev
{"title":"INFLUENCE OF CeO2 ON THE FORMATION OF PLASMONIC Au NANOPARTICLES IN GLASSES OF THE ZnO–MgO–Al2O3–SiO2 SYSTEM","authors":"G. Y. Shakhgildyan, V. Durymanov, L. Avakyan, G. N. Atroshenko, M. Vetchinnikov, R. O. Alexeev, E. Ignat'eva, N. V. Golubev, A. A. Zolikova, L. Bugaev, V. Sigaev","doi":"10.14489/glc.2023.06.pp.003-014","DOIUrl":"https://doi.org/10.14489/glc.2023.06.pp.003-014","url":null,"abstract":"Using absorption spectroscopy, differential scanning calorimetry, and X-ray powder diffraction, we studied the effect of a small addition of CeO2 on the process of thermally stimulated formation of plasmonic Au nanoparticles in the glass of the ZnO–MgO–Al2O3–SiO2 system containing TiO2 and ZrO2 as nucleating agents. It is shown that when the glass is heated from temperatures slightly above Tg to temperatures in the region of the exothermic peak, the plasmon resonance band of Au nanoparticles undergoes a nonlinear shift; however, the addition of CeO2 significantly expands the the shift to the long wavelength region of the spectrum. We performed the computer simulation of the experimental optical absorption spectra, estimated the sizes of the formed nanoparticles and proposed the mechanism of the effect of the CeO2 addition on the formation of plasmonic Au nanoparticles.","PeriodicalId":445802,"journal":{"name":"Steklo i Keramika","volume":"128 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2023-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139371744","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
LASER FORMATION OF LUMINESCENT TRACKS IN BISMUTH-DOPED NANOPOROUS GLASS 激光在掺铋纳米多孔玻璃中形成发光轨迹
Steklo i Keramika Pub Date : 2023-06-01 DOI: 10.14489/glc.2023.06.pp.015-021
Yu. V. Mikhailov, A. Lipatiev, T. O. Lipatieva, S. Fedotov, M. Ziyatdinova, P. I. Ivanov, V. Sigaev
{"title":"LASER FORMATION OF LUMINESCENT TRACKS IN BISMUTH-DOPED NANOPOROUS GLASS","authors":"Yu. V. Mikhailov, A. Lipatiev, T. O. Lipatieva, S. Fedotov, M. Ziyatdinova, P. I. Ivanov, V. Sigaev","doi":"10.14489/glc.2023.06.pp.015-021","DOIUrl":"https://doi.org/10.14489/glc.2023.06.pp.015-021","url":null,"abstract":"The formation of microtracks in the volume of porous glass samples by femtosecond laser pulses which is of importance for laser writing of active optical waveguides was studied. It was found that impregnation of nanoporous glass in bismuth nitrate solution leads to the appearance of an orange luminescence band under 488 nm light excitation and this luminescence band is enhanced in the laser-wriiten tracks. It is shown that increasing the laser pulse energy to 200 nJ allows increasing the phase contrast of the tracks laser-written in nanoporous glass doped with bismuth compared to the ones formed in nanoporous glass without additives.","PeriodicalId":445802,"journal":{"name":"Steklo i Keramika","volume":"9 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2023-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"139371813","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
SYNTHESIS OF Bi2NiTa2O9 WITH A PYROCHLORE-TYPE STRUCTURE 焦绿石型结构Bi2NiTa2O9的合成
Steklo i Keramika Pub Date : 2022-02-01 DOI: 10.14489/glc.2022.02.pp.040-046
V. Muraviev, B. Makeev, M. Krzhizhanovskaya, R. Korolev, N. Zhuk
{"title":"SYNTHESIS OF Bi2NiTa2O9 WITH A PYROCHLORE-TYPE STRUCTURE","authors":"V. Muraviev, B. Makeev, M. Krzhizhanovskaya, R. Korolev, N. Zhuk","doi":"10.14489/glc.2022.02.pp.040-046","DOIUrl":"https://doi.org/10.14489/glc.2022.02.pp.040-046","url":null,"abstract":"Nickel pyrochlore of the composition Bi2NiTa2O9 was synthesized by the solid-phase reaction method (sp. gr. Fd-3m, a = 10.5238 Å). The process of phase formation of nickel-containing bismuth tantalate Bi2NiTa2O9 with a pyrochlore structure is investigated. The pyrochlore phase synthesis reaction is described by the interaction of orthorhombic bismuth orthotantalate and nickel oxide. Synthesis proceeds mainly at temperatures above 900 °С. The duration of calcination of the preparations leads to the coalescence of grains with the formation of larger particles. \u0000The calcination temperature did not significantly affect the microstructure of the samples. The samples are characterized by a porous dendritic microstructure with a grain size of 0.5 – 1.0 µm. The optimal conditions for obtaining pure pyrochlore can be considered a temperature of 1050 °С and calcination time of 15 hours.","PeriodicalId":445802,"journal":{"name":"Steklo i Keramika","volume":"20 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-02-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"133556025","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
OXIDE-CONTAINING MINERAL FIBERS: TYPES, METHODS OF PRODUCTION, APPLICATION AND MANUFACTURERS (REVIEW) 含氧化物矿物纤维:类型、生产方法、应用及生产厂家(综述)
Steklo i Keramika Pub Date : 2022-01-01 DOI: 10.14489/glc.2022.01.pp.039-050
B. L. Krasniy, K. Ikonnikov, D. Lemeshev, A. Sizova
{"title":"OXIDE-CONTAINING MINERAL FIBERS: TYPES, METHODS OF PRODUCTION, APPLICATION AND MANUFACTURERS (REVIEW)","authors":"B. L. Krasniy, K. Ikonnikov, D. Lemeshev, A. Sizova","doi":"10.14489/glc.2022.01.pp.039-050","DOIUrl":"https://doi.org/10.14489/glc.2022.01.pp.039-050","url":null,"abstract":"The article provides an overview of mineral oxide fibers of various chemical composition: aluminosilicate, alumina, silica, bio-soluble, zirconium oxide fibers and others. Methods for producing discrete and continuous fibers, such as spinning fibers from melts, sol-gel technology, spinning from solutions of metal salts, etc., are described. filtration for alumino-silicate and bio-soluble fibers; thermal insulation up to 1600 or 2000 C and reinforcement of composites used in the aerospace and defense industries for alumina fibers and fibers based on zirconium dioxide, etc. Producers of mineral oxide-containing fibers and products based on them abroad and in Russia are represented.","PeriodicalId":445802,"journal":{"name":"Steklo i Keramika","volume":"39 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"121003726","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
THE STRUCTURE FORMATION OF CuO/ZnO/?-Al2O3 CATALYST FOR THE METHANOL SYNTHESIS PROCESS DURING MECHANOCHEMICAL SYNTHESIS CuO/ZnO/?机械化学合成过程中甲醇合成过程的氧化铝催化剂
Steklo i Keramika Pub Date : 2022-01-01 DOI: 10.14489/glc.2022.01.pp.051-058
D. V. Smirnov, D. A. Prozorov, R. Rumyantsev, A. V. Afineevsky, K. A. Nikitin, A. Meledin, A. A. Kurnikova
{"title":"THE STRUCTURE FORMATION OF CuO/ZnO/?-Al2O3 CATALYST FOR THE METHANOL SYNTHESIS PROCESS DURING MECHANOCHEMICAL SYNTHESIS","authors":"D. V. Smirnov, D. A. Prozorov, R. Rumyantsev, A. V. Afineevsky, K. A. Nikitin, A. Meledin, A. A. Kurnikova","doi":"10.14489/glc.2022.01.pp.051-058","DOIUrl":"https://doi.org/10.14489/glc.2022.01.pp.051-058","url":null,"abstract":"The article discusses the mechanochemical synthesis of a catalyst for the synthesis of methanol. Comparative mechanical activation of both individual components of the catalyst (copper oxide, zinc oxide, and aluminum oxide) and their various mixtures under different conditions has been carried out. The article discusses the structural characteristics of the catalyst for the synthesis of methanol, obtained using X-ray phase analysis, scanning microscopy and low-temperature adsorption of nitrogen.","PeriodicalId":445802,"journal":{"name":"Steklo i Keramika","volume":"73 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"123994997","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
PREPARATION OF NIOBIUM (V) OXIDE WITH CONTROLLED DISPERSITY AND MORPHOLOGY 制备分散性和形貌可控的氧化铌
Steklo i Keramika Pub Date : 2022-01-01 DOI: 10.14489/glc.2022.01.pp.031-038
N. K. Golubeva, D. Danilovich, D. D. Nesmelov, I. D. Shabalkin
{"title":"PREPARATION OF NIOBIUM (V) OXIDE WITH CONTROLLED DISPERSITY AND MORPHOLOGY","authors":"N. K. Golubeva, D. Danilovich, D. D. Nesmelov, I. D. Shabalkin","doi":"10.14489/glc.2022.01.pp.031-038","DOIUrl":"https://doi.org/10.14489/glc.2022.01.pp.031-038","url":null,"abstract":"In this work, the effect of the annealing temperature and the chemical history of the precipitate on the morphology and phase composition of the Nb2O5 powder was studied. Nb2O5nH2O precipitate and gel-like niobium citrate were obtained by solution methods. The synthesis of niobium oxide was carried out at temperatures of 600, 1000, and 1200 °C, the synthesis products were analyzed using X-ray diffraction, scanning electron microscopy, X-ray microscopy, and differential thermal and thermogravimetric analysis. Annealing of niobium citrate at a temperature of 600 °C makes it possible to obtain niobium oxide particles with an average size of about 70 nm, which is 4 – 6 times smaller than Nb2O5 obtained from the Nb2O5nH2O precipitate.","PeriodicalId":445802,"journal":{"name":"Steklo i Keramika","volume":"1 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"128295695","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
CREATION AND PROPERTIES OF CERAMICS FROM NICKEL OXIDE NANOPOWDER 纳米氧化镍粉体陶瓷的制备及性能研究
Steklo i Keramika Pub Date : 2022-01-01 DOI: 10.14489/glc.2022.01.pp.012-014
V. Lysenko
{"title":"CREATION AND PROPERTIES OF CERAMICS FROM NICKEL OXIDE NANOPOWDER","authors":"V. Lysenko","doi":"10.14489/glc.2022.01.pp.012-014","DOIUrl":"https://doi.org/10.14489/glc.2022.01.pp.012-014","url":null,"abstract":"By means of the method of the spark plasma sintering (SPS) on the basis of nanodimensional powder of nickel oxide (with an average particle size of about 100 nm), the fine-grained (of 250 – 500 nanometers approximately), dense (5.93 g/cm3), strong ceramics with the high microhardness Hv = 8.2 GPa, ultimate compressive strength ?B = 0.4 GPa and Young?s modulus of elasticity E = 140 GPa is created. The obtained ceramic sample was nickel oxide NiO (73-1519) with cubic structure, space group Fm3m (No. 225) and lattice size a = 4.168 ?.","PeriodicalId":445802,"journal":{"name":"Steklo i Keramika","volume":"36 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"125147200","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
RESULTS OF COMPARATIVE STUDIES ON THE DURABILITY OF CUTTING CERAMIC PLATES WHEN TURNING HARDENED STEEL BLANKS 车削淬硬钢坯料时陶瓷板切削耐久性的对比研究结果
Steklo i Keramika Pub Date : 2022-01-01 DOI: 10.14489/glc.2022.01.pp.015-020
V. V. Mylnikov, A. I. Pronin, S. Veselov, D. Valko
{"title":"RESULTS OF COMPARATIVE STUDIES ON THE DURABILITY OF CUTTING CERAMIC PLATES WHEN TURNING HARDENED STEEL BLANKS","authors":"V. V. Mylnikov, A. I. Pronin, S. Veselov, D. Valko","doi":"10.14489/glc.2022.01.pp.015-020","DOIUrl":"https://doi.org/10.14489/glc.2022.01.pp.015-020","url":null,"abstract":"The paper presents the results of a study on the durability of cutting ceramics: a replaceable polyhedral plate developed at NSTU and cutting ceramics WOK-60 when processing hardened steel blanks made of 40X (45HRC) steel. As a result of the tests carried out, it was found that with the use of cutting modes developed at KNAU, the durability of SMP from cutting ceramics created at NSTU is more than 1.7 times higher than the performance of plates based on the WOK-60 material. At the same time, the roughness of the treated surface of the work piece was Ra = 0.35 ? 0.05 microns when using SMP from the developed ceramics Ra = 0.55 ? 0.05 microns when using WOK-60 plates. The stages of destruction of cutting ceramic plates are revealed, taking into account the hierarchy of structural scales.","PeriodicalId":445802,"journal":{"name":"Steklo i Keramika","volume":"40 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"133405072","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
EFFECT OF FEATURES IN GRAIN STRUCTURE ON THE THERMOELECTRIC PROPERTIES OF COMPOUNDS BASED ON BISMUTH TELLURIDE 晶粒结构特征对碲化铋基化合物热电性能的影响
Steklo i Keramika Pub Date : 2022-01-01 DOI: 10.14489/glc.2022.01.pp.003-011
O. Ivanov, M. Yaprintsev, A. Vasil'ev, E. P. Dan’shina
{"title":"EFFECT OF FEATURES IN GRAIN STRUCTURE ON THE THERMOELECTRIC PROPERTIES OF COMPOUNDS BASED ON BISMUTH TELLURIDE","authors":"O. Ivanov, M. Yaprintsev, A. Vasil'ev, E. P. Dan’shina","doi":"10.14489/glc.2022.01.pp.003-011","DOIUrl":"https://doi.org/10.14489/glc.2022.01.pp.003-011","url":null,"abstract":"Specific mechanisms of grain structure effect on the thermoelectric properties (specific electrical resistivity and total thermal conductivity) of the Bi1.9Gd0.1Te3 compound have been analyzed. These mechanisms are as follows: 1) forming the surface Te vacancies at grain boundaries acting as donor centres; 2) changing the elemental composition of the grains at high-temperature Te evaporation under thermal treatment of material to prepare the samples with desired average grain size.","PeriodicalId":445802,"journal":{"name":"Steklo i Keramika","volume":"100 8","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"134412512","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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