Dwinna Rahmi, R. Yunilawati, I. Setiawati, Irwinanita Irwinanita, B. N. Jati, A. Riyanto, Yemirta Yemirta, N. N. Aidha
{"title":"ANTIOXIDANT ACTIVITY, SKIN IRRITAION POTENTIAL AND CHEMICAL COMPOSITION OF CLOVE LEAF OIL FROM WEST JAVA INDONESIA","authors":"Dwinna Rahmi, R. Yunilawati, I. Setiawati, Irwinanita Irwinanita, B. N. Jati, A. Riyanto, Yemirta Yemirta, N. N. Aidha","doi":"10.17146/jsmi.2021.23.1.6398","DOIUrl":"https://doi.org/10.17146/jsmi.2021.23.1.6398","url":null,"abstract":"ANTIOXIDANT ACTIVITY, SKIN IRRITATON POTENTIAL, AND CHEMICAL COMPOSITION OF CLOVE LEAF OIL FROM WEST JAVA INDONESIA. Essential oils with specific chemical compositions have the potential as a source of antioxidants in cosmetics, however, in general, essential oils are not safe because of the potential for skin irritation. This study aims is to perform fractionation to obtain clove oil with a chemical composition that is safe on the skin and does not reduce its antioxidant activity. Fractionation was performed at a temperature of 100 – 285 oC. Chemical composition was determined by Mass Chromatography Spectrometry (GC-MS), antioxidant activity by DPPH method, and irritation potential by in-vivo patch test. The results showed chemical components of clove oil were eugenol, copaene, beta caryophyllene, iso-eugenol, alpha caryophyllene, cadinene, caryophyllene oxide, caryophylla and beta caryophylla. Fractions with chemical compositions of eugenol and beta caryophyllene as the main components and copaene, iso-eugenol, alpha caryophyllene, cadinene as secondary components have very light erythema and no potential irritation to the skin. The fraction produced from the fractionation of crude clove oil at a temperature of 235 – 260 oC has the highest antioxidant activity of 10.17 mg/L.","PeriodicalId":365391,"journal":{"name":"Jurnal Sains Materi Indonesia","volume":"34 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2021-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"129653800","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
M. Hasbi, M. R. Wida'atullah, F. Citrawati, S. Chandra, L. Suhaemi
{"title":"IDENTIFICATION OF BAINITE IN A MULTI-PHASE MICROSTRUCTURE OF AN AUSTEMPERED STEEL ALLOY: A METALLOGRAPHY APPROACH","authors":"M. Hasbi, M. R. Wida'atullah, F. Citrawati, S. Chandra, L. Suhaemi","doi":"10.17146/jsmi.2021.23.1.6401","DOIUrl":"https://doi.org/10.17146/jsmi.2021.23.1.6401","url":null,"abstract":"IDENTIFICATION OF BAINITE IN A MULTI-PHASE MICROSTRUCTURE OF AN AUSTEMPERED STEEL ALLOY: A METALLOGRAPHY APPROACH. Structural characterization of a multi-phase steel has become an exciting issue in various studies to date. This relates to the difficulty in distinguishing phases with similar morphology, i.e. bainite and martensite, through chemical etching. This study discusses a method to observe bainite phase through a metallographic approach on FeNi steel using color etching. Variations in the use of etching in this research include 2% nital, 4% picral, and 15% sodium metabisulphite (SMB). First, the samples were austenized then austempered at either 400 °C or 500 °C, for 60 min followed by quenching in either water or brine solution. Based on optical microscope observations, SMB color etching provides more explicit information on the visualization of bainite and martensite phases because they have different color appearances. The bainite phase is shown in bluish color, while the martensite phase is shown in brownish color. Furthermore, the influence of variation in austempering temperature and quench media on microstructure morphology was also discussed. In addition, the calculation of the lattice parameters of the X-Ray Diffraction (XRD) pattern was also carried out in this study to identify the crystal structure formed.","PeriodicalId":365391,"journal":{"name":"Jurnal Sains Materi Indonesia","volume":"5 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2021-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"128749900","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Satrio Herbirowo, M. Harimurti, S. Chandra, Dedi Pria Utama, F. M. Ridlo, Y. M. Zulaida, B. Adjiantoro
{"title":"STUDY ON THE EFFECT OF COMPOSITION AND VARIATION OF Sn/Zn COOLING MEDIA ON NICKEL ALLOY STEEL THROUGH HOT FORGING AND AUSTEMPERING","authors":"Satrio Herbirowo, M. Harimurti, S. Chandra, Dedi Pria Utama, F. M. Ridlo, Y. M. Zulaida, B. Adjiantoro","doi":"10.17146/jsmi.2021.23.1.6374","DOIUrl":"https://doi.org/10.17146/jsmi.2021.23.1.6374","url":null,"abstract":"STUDY ON THE EFFECT OF COMPOSITION AND VARIATION OF Sn/Zn COOLING MEDIA ON NICKEL ALLOY STEEL THROUGH HOT FORGING AND AUSTEMPERING. Laterite steel with nickel content is expected to be a solution to overcome the lack of domestic steel availability and dependence on imports. This research was conducted to develop Nickel-Chromium-Molybdenum alloy steel used Grinding ball for cement industrial applications. Grinding ball is the one of imported steel products needed to be crushing and size reduction the ores or cement. In addition to import issues, grinding balls have a significant problem: their mechanical properties that do not meet SNI 1049 require the material to have a minimum hardness value of 45 HRC. In this study, the characteristics of Nickel alloy steel were investigated further through heat treatment of forgings heated at the austenitizing temperature of 950 °C and austempering with variations in the cooling medium of Sn/Zn solution. The cooling medium was chosen because it has a melting temperature in the phase diagram area to form the bainite microstructure with complex and challenging characteristics, both of which are required in material for grinding ball applications. In particular, the hardness value that passed the SNI 1069 standard was the use of samples with a Cr-Mo alloy of 1%-wt with a hardness value of 45.92 HRC for Sn Austemper and 48.07 HRC for Zn austemper.","PeriodicalId":365391,"journal":{"name":"Jurnal Sains Materi Indonesia","volume":"218 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2021-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"133797074","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"ANNEALING TEMPERATURES’ EFFECTS ON MICROSTRUCTURE AND OPTICAL PROPERTIES OF Ba0.95Sr0.05TiO3 FILMS","authors":"Y. Iriani, F. Nurosyid, Ratna Mayasari, D. Sandi","doi":"10.17146/jsmi.2021.23.1.6338","DOIUrl":"https://doi.org/10.17146/jsmi.2021.23.1.6338","url":null,"abstract":"ANNEALING TEMPERATURES’ EFFECTS ON MICROSTRUCTURE AND OPTICAL PROPERTIES OF Ba0.95Sr0.05TiO3 FILMS. Ferroelectric materials, one of which is Barium Strontium Titanate (BST), can be applied for photovoltaic. Ferroelectric films function as the P-type semiconductor in the P-N junction. BST (Ba0.95Sr0.05TiO3) films have been deposited on Pt/Si (111) and quartz substrates via the CSD method prepared by spin coater. The films were annealed at various temperatures of 800 °C, 900 °C, and 1000 °C to observe the annealing temperatures' effects on the microstructure and optical properties of the BST films. From the XRD results, the intensity of diffraction peaks gets higher along with the higher annealing temperature. It thus causes the level of crystallization and the crystal size of the Ba0.95Sr0.05TiO3 films to increase. The morphology results reveal that the grains size of the Ba0.95Sr0.05TiO3 films is getting larger with the higher annealing temperature. The optical properties examined in the Ba0.95Sr0.05TiO3 films include absorbance and bandgap energy values. Values of bandgap energy show a decrease with increasing sintering temperature. The smallest bandgap energy of the Ba0.95Sr0.05TiO3 film is achieved at 1000 °C of 3.20 eV. BST films were annealed at temperature 1000 °C attained from this study can be considered as candidate for a photovoltaic ferroelectric material.","PeriodicalId":365391,"journal":{"name":"Jurnal Sains Materi Indonesia","volume":"1 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2021-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"126305963","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
V. Saraswaty, R. C. Nissa, B. Firdiana, A. H. Abdullah
{"title":"THE PHYSICOCHEMICAL CHARACTERISTICS OF RECYCLED-PLASTIC PELLETS OBTAINED FROM DISPOSABLE FACE MASK WASTES","authors":"V. Saraswaty, R. C. Nissa, B. Firdiana, A. H. Abdullah","doi":"10.17146/jsmi.2021.23.1.6336","DOIUrl":"https://doi.org/10.17146/jsmi.2021.23.1.6336","url":null,"abstract":"THE PHYSICOCHEMICAL CHARACTERISTICS OF RECYCLED-PLASTIC PELLETS OBTAINED FROM DISPOSABLE FACE MASK WASTES. The government policy to wear a face mask during the COVID-19 pandemic has increased disposable face mask wastes. Thus, to reduce such wastes, it is necessary to evaluate the physicochemical characteristics of disposable face masks wastes before the recycling process and the recycled products. In this study, physicochemical characterization of the 3-ply disposable face masks and the recycled plastic pellets after disinfection using 0.5% v/v sodium hypochlorite were evaluated. A set of parameters including the characterization of surface morphology by a scanning electron microscope (SEM), functional groups properties by a fourier transform infra-red spectroscopy (FT-IR), thermal behavior by a differential scanning calorimetry (DSC), tensile strength and elongation at break were evaluated. The surface morphological of each layer 3-ply disposable face mask showed that the layers were composed of non-woven fibers. The FT-IR evaluation revealed that 3-ply disposable face mask was made from a polypropylene. At the same time, the DSC analysis found that the polypropylene was in the form of homopolymer. The SEM analysis showed that the recycled plastic pellets showed a rough and uneven surface. The FT-IR, tensile strength and elongation at break of the recycled plastic pellets showed similarity with a virgin PP type CP442XP and a recycled PP from secondary recycling PP (COPLAST COMPANY). In summary, recycling 3-ply disposable face mask wastes to become plastic pellets is recommended for handling disposable face mask wastes problem.","PeriodicalId":365391,"journal":{"name":"Jurnal Sains Materi Indonesia","volume":"73 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2021-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"131260989","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"THE STRUCTURAL, IMPEDANCE AND DIELECTRIC A FERRITE CORE OF IRON MANGANITE AND ITS COMPOSITE","authors":"Y. E. Gunanto, H. Sitompul, M. Izaak, W. A. Adi","doi":"10.17146/jsmi.2021.23.1.6303","DOIUrl":"https://doi.org/10.17146/jsmi.2021.23.1.6303","url":null,"abstract":"THE STRUCTURAL, IMPEDANCE AND DIELECTRIC A FERRITE CORE OF IRON MANGANITE AND ITS COMPOSITE. Samples with single-phase MnFeO3 and multiphase MnFeO3/ZnFe2O4 (30/70), and MnFeO3/ZnFe2O4/LaMnO3 (30/40/30) have been successfully prepared as ferrite cores by the solid-state reaction method using high energy milling. Crystal structure, surface morphology, impedance, AC-conductivity and dielectric quantities, such as dielectric constant and dielectric loss have been studied. The crystalline structures for MnFeO3, ZnFe2O4, and LaMnO3 are hexagonal, cubic and monoclinic, The Rietveld program used for XRD analysis resulted in the composition fractions of single phase MnFeO3, multiphase MnFeO3/ZnFe2O4 (31/69), and MnFeO3/ZnFe2O4/LaMnO3 (31/40/29). The morphology of all samples has a heterogeneous shape and size with low porosity. The single-phase impedance of MnFeO3 is higher than the multiphase sample. The conductivity of the three samples has the same pattern, which is relatively constant at low frequencies and begins to increase at frequencies above 10 kHz. The dielectric constant and dielectric loss (tan 𝜕) have high values at low frequencies, decrease exponentially with increasing frequency and are relatively fixed at high frequencies.","PeriodicalId":365391,"journal":{"name":"Jurnal Sains Materi Indonesia","volume":"5 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2021-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"126470994","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
R. C. Nissa, D. Sumiarsa, W. Kosasih, B. Firdiana, A. H. Abdullah
{"title":"SYNTHESIS L-LACTIC ACID FROM FERMENTATION OF CASSAVA PULP BY USING TEMPEH INOCULUM","authors":"R. C. Nissa, D. Sumiarsa, W. Kosasih, B. Firdiana, A. H. Abdullah","doi":"10.17146/jsmi.2021.23.1.6265","DOIUrl":"https://doi.org/10.17146/jsmi.2021.23.1.6265","url":null,"abstract":"SYNTHESIS L-LACTIC ACID FROM FERMENTATION OF CASSAVA PULP BY USING TEMPEH INOCULUM. This study used cassava waste pulp as a fermentation substrate to produce lactic acid using a tempeh inoculum. Tempeh inoculum is a mixed culture of Rhizopus with Rhizopus oligosporus as the primary fungus. Lactic acid is an organic acid most widely used in the food, pharmaceutical, cosmetic and chemical industries. One of the important uses of lactic acid is as a raw material for producing Polylactic Acid (PLA) biopolymers, namely polymers that can decompose naturally in a relatively fast time. The analysis was performed using the Response Surface Methodology (RSM) method and the Box Behnken Design (BBD) experimental design with substrate concentration parameters, inoculum concentration, and incubation time on lactic acid. The fermentation process is carried out using a flask shaker at a temperature of 30 ºC, pH 6.0, and a rotational speed of 150 rpm. The optimum yield for lactic acid is 6.65 g/L. It was acquired at substrate 20 g/L, inoculum concentration 0.30 % (w/v) at an incubation time of 72 hours.","PeriodicalId":365391,"journal":{"name":"Jurnal Sains Materi Indonesia","volume":"48 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2021-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"133456477","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"SYNTHESIS AND CHARACTERIZATION: COMPOSITE OF GRAPHENE OXIDE BASED PALM KERNEL SHELL WASTE WITH FE3O4","authors":"Bernadeta Ayu Widyaningrum, Dita Apriani, Putri Amanda, I. Ismadi, Sutanto Sutanto","doi":"10.17146/jsmi.2021.22.3.6310","DOIUrl":"https://doi.org/10.17146/jsmi.2021.22.3.6310","url":null,"abstract":"SYNTHESIS AND CHARACTERIZATION: COMPOSITE OF GRAPHENE OXIDE BASED PALM KERNEL SHELL WASTE WITH Fe3O4. In this study, GO-Fe3O4 were fabricated by co-precipitation technique and the graphene oxide (GO) were synthesized from an agricultural biomass, palm kernel shell, via Hummer’s method. Field Emission Scanning Electron Microscopy and Energy Dispersive Spectrum (FESEM-EDS), Fourier Transform Infra-Red (FT-IR) spectroscopy, X-Ray Diffractometer (XRD), and Raman spectroscopy were used to analysis the successful attachment of Fe3O4 onto the surface of GO. Morphology observation showed that Fe3O4 were heterogeneously deposited on the surface of GO. FT-IR spectra shows peak that incorporated to oxygenated functional groups and sharp peak at 586 cm-1 confirmed to lattice absorption of Fe3O4. The percentage of composition of GO-Fe3O4 was characterized by energy dispersive spectroscopy and the results also confirmed in XRD exhibits similar properties with JCPDS 19-0629 for magnetite more dominant than GO. From Raman spectroscopy analysis shows that 1343.82 cm-1 (D-band) and 1584.62 cm-1 (G-band) and 2698 cm-1 (2D-band) indicates GO and GO-Fe3O4 were successfully synthesized.","PeriodicalId":365391,"journal":{"name":"Jurnal Sains Materi Indonesia","volume":"20 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2021-08-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"130524360","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
P. Amanda, S. Nabila, I. Ismadi, D. Purnomo, N. Masruchin
{"title":"PICKERING EMULSION TECHNOLOGY IN FABRICATE CELLULOSE FOAM FROM OIL PALM EMPTY FRUIT BUNCH WASTE","authors":"P. Amanda, S. Nabila, I. Ismadi, D. Purnomo, N. Masruchin","doi":"10.17146/jsmi.2021.22.3.6255","DOIUrl":"https://doi.org/10.17146/jsmi.2021.22.3.6255","url":null,"abstract":"PICKERING EMULSION TECHNOLOGY IN FABRICATE CELLULOSE FOAM FROM OILPALM EMPTY FRUIT BUNCH WASTE. Cellulose from the oil palm empty fruit bunch (OPEFB) waste can make a porous material. This study aims to make cellulose foam with Pickering emulsion technology used cellulose nanofiber as a Pickering agent. The mechanism of Pickering emulsion is learned from foamability and stability of foam in the presence of various concentrations of surfactant. The result showed that using Pickering emulsion technology only needed surfactant with a small concentration to improve foamability and stability. The addition of CNF indeed improved the stability and foamability with the Pickering effect. The stability test shows that the foam stabilized with CNF appeared to be relatively stable. In contrast to the CNF free system, the foams were collapse in three days tested. Structures of foam was characterized using an optical microscope and showed that the foam was composed into two- or three dimensional microstructures formed by gas bubble of wet foam in random orientations. This process generated the lightweight Cellulose foam from OPEFB waste, with a density of 0.07 g/cm3. Using Pickering emulsion technology to make cellulose foam can be one way to overcome OPEFB waste and this foam is potential for various applications.","PeriodicalId":365391,"journal":{"name":"Jurnal Sains Materi Indonesia","volume":"41 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2021-08-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"121844815","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"EFFECT OF TREATMENT SOLUTION ON THE MICROSTRUCTURE AND MICROHARDNESS OF TERNARY Ni-Al-Nb ALLOY DOPED WITH TITANIUM","authors":"H. Nugraha, Pradoto Ambardi, D. Prajitno","doi":"10.17146/JSMI.2020.22.1.5526","DOIUrl":"https://doi.org/10.17146/JSMI.2020.22.1.5526","url":null,"abstract":"EFFECT OF TREATMENT SOLUTION ON THE MICROSTRUCTURE AND MICROHARDNES OF TERNARY Ni-Al-Nb ALLOY DOPED WITH TITANIUM. Nickel-based superalloys have been widely used in various applications, which require high strength at high temperatures. Most types of these superalloys is age-hardenable because they have γ’ particles' chemical composition Ni3(Al, Ti) in γ’-phase matrix. This research will be used alloy Ni-Al-Nb added alloying elements Ti. This research was conducted to study the mechanical properties, microstructure conditions in some alloys Ni-Al-Nb added distinction Titanium element (0,5% and 1% Ti) using the method of aging temperature variation performed at a temperature of 650 °C,700 °C and 750 °C with a holding time 4 hours and air cooling. Tests were conducted to determine the characterization of the specimen includes testing metallographic optical microscope, Rockwell hardness C and SEM- EDS,XRD. Results obtained from this research that addition of titanium element affecting the hardness values as well as the results of the cast, solution treatment and aging process results. The 1% Titanium content can affect the gamma prime coarsening and make the grain on the microstructure result smooth.","PeriodicalId":365391,"journal":{"name":"Jurnal Sains Materi Indonesia","volume":"15 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2021-05-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"130120896","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}