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Surface displacements of a PMUT array: Interferometric characterization and mechanical crosstalk evaluation PMUT阵列的表面位移:干涉表征和机械串扰评价
IF 2.9
Open Ceramics Pub Date : 2025-07-06 DOI: 10.1016/j.oceram.2025.100820
S. Udovenko , R. Graham , P. Tipsawat , M. Pineda , S. Trolier-McKinstry
{"title":"Surface displacements of a PMUT array: Interferometric characterization and mechanical crosstalk evaluation","authors":"S. Udovenko ,&nbsp;R. Graham ,&nbsp;P. Tipsawat ,&nbsp;M. Pineda ,&nbsp;S. Trolier-McKinstry","doi":"10.1016/j.oceram.2025.100820","DOIUrl":"10.1016/j.oceram.2025.100820","url":null,"abstract":"<div><div>Piezoelectric micromachined ultrasonic transducers (PMUTs) enable substantial electrically induced strains at low voltages. In this work a combination of Laser Doppler Vibrometry (LDV) and Mapping Single Beam Laser Interferometry (SBLI) was used to characterize PMUT displacement shapes at frequencies of 600 kHz and 1 kHz, respectively. Finite element modeling demonstrated excellent agreement with the displacements, once the device geometry was corrected to measured (rather than nominal) dimensions and appropriate boundary conditions were applied. Mapping SBLI was also used to characterize mechanical crosstalk at low frequencies, which is critical for evaluating PMUT performance. It was also demonstrated that driving one element induces bending of the PMUT substrate over dimensions on the 3 mm scale. The analysis of displacement profiles near the edges of released parts of PMUT structure revealed 150 μm transition regions between clamped and released areas. This reduced the active length (where displacement reaches its maximum values) of the PMUT by ∼4%.</div></div>","PeriodicalId":34140,"journal":{"name":"Open Ceramics","volume":"23 ","pages":"Article 100820"},"PeriodicalIF":2.9,"publicationDate":"2025-07-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144632282","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Review of advances and challenges in alkali-activated materials from dredged sediments 疏浚沉积物碱活性材料研究进展与挑战综述
IF 2.9
Open Ceramics Pub Date : 2025-07-06 DOI: 10.1016/j.oceram.2025.100824
Amine el Mahdi Safhi , Shima Pilehvar , Mahdi Kioumarsi
{"title":"Review of advances and challenges in alkali-activated materials from dredged sediments","authors":"Amine el Mahdi Safhi ,&nbsp;Shima Pilehvar ,&nbsp;Mahdi Kioumarsi","doi":"10.1016/j.oceram.2025.100824","DOIUrl":"10.1016/j.oceram.2025.100824","url":null,"abstract":"<div><div>Dredging worldwide generates over 1 billion m³ of sediments annually, creating disposal and environmental challenges. Alkali-activated materials (AAMs) offer a circular pathway by converting dredged sediments (DS) into sustainable binders and aggregates. This review synthesizes 32 studies on DS-based AAMs, detailing sediments chemistry, pretreatment routes, mix-design strategies, performance, and field cases. Calcination or mechanochemical activation elevates DS reactivity, producing binders that achieve 28-day compressive strengths of 15–40 MPa and durable matrices resistant to sulfate, freeze–thaw, and carbonation. Processed DS sands can fully or partially replace natural fine aggregates while maintaining ≥25 MPa concrete strength. AAM matrices immobilize heavy metals, keeping leachate below inert-waste thresholds. Key knowledge gaps remain in standardized mix design, long-term durability, and regulatory acceptance. The review outlines research and policy priorities to scale DS-AAM technologies for low-carbon infrastructure.</div></div>","PeriodicalId":34140,"journal":{"name":"Open Ceramics","volume":"23 ","pages":"Article 100824"},"PeriodicalIF":2.9,"publicationDate":"2025-07-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144587969","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of mineralizer on the synthesis of (Ni, Mn) co-doping CuFe5O8 pigment and its glazing performance 矿化剂对(Ni, Mn)共掺杂CuFe5O8颜料合成及上光性能的影响
IF 2.9
Open Ceramics Pub Date : 2025-07-05 DOI: 10.1016/j.oceram.2025.100822
Guo Feng , Tiantian Liu , Jun Mu , Feng Jiang , Zhiqi Guo , Liangliang Xiao , Qian Wu , Xiaojun Zhang , Jianmin Liu , Jian Liang
{"title":"Effect of mineralizer on the synthesis of (Ni, Mn) co-doping CuFe5O8 pigment and its glazing performance","authors":"Guo Feng ,&nbsp;Tiantian Liu ,&nbsp;Jun Mu ,&nbsp;Feng Jiang ,&nbsp;Zhiqi Guo ,&nbsp;Liangliang Xiao ,&nbsp;Qian Wu ,&nbsp;Xiaojun Zhang ,&nbsp;Jianmin Liu ,&nbsp;Jian Liang","doi":"10.1016/j.oceram.2025.100822","DOIUrl":"10.1016/j.oceram.2025.100822","url":null,"abstract":"<div><div>Novel Co and Cr free, high-temperature (Ni, Mn) co-doping CuFe<sub>5</sub>O<sub>8</sub> black ceramic pigments were synthesized. The effects of mineralizer type and mineralizer amount on the synthesis and coloration of (Ni, Mn) co-doping CuFe<sub>5</sub>O<sub>8</sub> pigments, as well as the effect of glazing calcination temperature on glaze coloration were systematically investigated using testing and characterization methods such as XRD, FE-SEM, TEM, EDS-mapping, HAADF and colorimeter. The results indicate that compared with H<sub>3</sub>BO<sub>3</sub>, NH<sub>4</sub>F, LiF and NaF mineralizers, the pigment with MgO as the mineralizer is relatively better. The optimized mineralizer MgO amount is 6.25 wt.% (mass ratio relative to the pigment). <em>L</em>*, <em>a</em>* and <em>b</em>* values of corresponding optimized pigment are 21.36, 1.10 and -0.24, respectively. The crystal phase of the pigment is CuFe<sub>5</sub>O<sub>8</sub> (73–2314), and no diffraction peak of the heterophase is detected. The crystal size of the pigments is 0.8–1.5 <em>μ</em>m with excellent dispersivity. The glazing temperatures have little effect on the coloration of the pigments when they are used at 1000 °C, 1150 °C and 1300 °C. The results show that the pigment has excellent high temperature resistance and is expected to be widely used in high-temperature glazing coloration.</div></div>","PeriodicalId":34140,"journal":{"name":"Open Ceramics","volume":"23 ","pages":"Article 100822"},"PeriodicalIF":2.9,"publicationDate":"2025-07-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144579789","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Compositional changes to brushite cements to improve mechanical and antibiotic-delivery properties 改变刷石水泥的成分以改善机械和抗生素的输送性能
IF 2.9
Open Ceramics Pub Date : 2025-07-05 DOI: 10.1016/j.oceram.2025.100823
Claudia Morilla Espino , Louise van der Weerd , Lioe-Fee de Geus-Oei , Jeroen JJP van den Beucken
{"title":"Compositional changes to brushite cements to improve mechanical and antibiotic-delivery properties","authors":"Claudia Morilla Espino ,&nbsp;Louise van der Weerd ,&nbsp;Lioe-Fee de Geus-Oei ,&nbsp;Jeroen JJP van den Beucken","doi":"10.1016/j.oceram.2025.100823","DOIUrl":"10.1016/j.oceram.2025.100823","url":null,"abstract":"<div><div>Brushite calcium phosphate cements (bCPCs) are promising synthetic bone substitutes due to their bioactivity, osteoconductivity, and controlled degradation. However, their clinical use is limited by poor handling, low mechanical strength, and insufficient antimicrobial capability. This study explores the incorporation of α-tricalcium phosphate (α-TCP) and silk fibroin (SF) to enhance bCPC performance and enable localized antibiotic delivery using tetracycline (TC). Adding α-TCP improved compressive strength (up to 2.65 MPa), while SF in liquid or fiber form reinforced the matrix. The inclusion of TC and SF extended setting times (4–7 min initial; 7–30 min final) and maintained injectability (up to 50 %). Drug release studies showed a 10 % burst in the first 24 h, with a sustained release of 77 % over 14 days. These multifunctional bCPCs offer injectable, resorbable, and antibacterial properties, making them suitable for non-load-bearing bone repair applications.</div></div>","PeriodicalId":34140,"journal":{"name":"Open Ceramics","volume":"23 ","pages":"Article 100823"},"PeriodicalIF":2.9,"publicationDate":"2025-07-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144579788","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Comparative study on the color characteristics of sky-green porcelain in the four kilns of a Ru kiln system from the Northern Song Dynasty 北宋汝窑系统四窑天青瓷色彩特征比较研究
IF 2.9
Open Ceramics Pub Date : 2025-07-03 DOI: 10.1016/j.oceram.2025.100821
Zhen Sang , Shuofei Zan , Le Li , Xiangyang Fu , Zhen Liu , Danni Chen , Xiaojuan Yuan , Pei Shi
{"title":"Comparative study on the color characteristics of sky-green porcelain in the four kilns of a Ru kiln system from the Northern Song Dynasty","authors":"Zhen Sang ,&nbsp;Shuofei Zan ,&nbsp;Le Li ,&nbsp;Xiangyang Fu ,&nbsp;Zhen Liu ,&nbsp;Danni Chen ,&nbsp;Xiaojuan Yuan ,&nbsp;Pei Shi","doi":"10.1016/j.oceram.2025.100821","DOIUrl":"10.1016/j.oceram.2025.100821","url":null,"abstract":"<div><div>To comparatively study the coloring mechanism of the celadon glaze of the four kilns in the Ru kiln system (i.e., Qingliangsi, Donggou, Yanhedian, and Duandian), samples obtained from these four kilns were examined. The glazes were analyzed by using chromaticity, XRF, XRD, XPS, and SEM/EDS. The results showed that the Fe<sub>2</sub>O<sub>3</sub> content of the Yanhedian, Donggou, Duandian, and Qingliangsi specimens decreased successively<strong>,</strong> so their brightness successively increased. The presence of small and dense bubbles, more mullite crystals, and Mie scattering produced by the phase-separated structure also increased the brightness of the Qingliangsi glaze, giving it the milkiest texture. The Fe<sup>2+</sup>/Fe<sup>3+</sup> ratio and P<sub>2</sub>O<sub>5</sub> content of the Qingliangsi, Duandian, Donggou, and Yanhedian specimen glazes successively decreased. Therefore, their glaze color changed from greenish-blue to greenish-yellow, and the reducing atmosphere decreased successively. The higher CaO content of the Qingliangsi and Duandian glazes deepened their blue hue.</div></div>","PeriodicalId":34140,"journal":{"name":"Open Ceramics","volume":"23 ","pages":"Article 100821"},"PeriodicalIF":2.9,"publicationDate":"2025-07-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144570041","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Dielectric property measurement of a SiCf/SiC ceramic matrix composite via microwave cavity characterisation 基于微波腔表征的SiCf/SiC陶瓷基复合材料介电性能测量
IF 2.9
Open Ceramics Pub Date : 2025-06-25 DOI: 10.1016/j.oceram.2025.100818
Jordan Stephen , Spencer Jeffs , Heungjae Choi , Adrian Porch
{"title":"Dielectric property measurement of a SiCf/SiC ceramic matrix composite via microwave cavity characterisation","authors":"Jordan Stephen ,&nbsp;Spencer Jeffs ,&nbsp;Heungjae Choi ,&nbsp;Adrian Porch","doi":"10.1016/j.oceram.2025.100818","DOIUrl":"10.1016/j.oceram.2025.100818","url":null,"abstract":"<div><div>Ceramic Matrix Composites (CMCs) are used for high temperature structural engineering applications, such as those found within gas turbine engines. When operating in these environments they can undergo oxidation and damage that may not be easily detectable, emphasising the need for a non-invasive assessment approach that could detect such changes. In this research, we use a single mode microwave cavity for sensitive dielectric property measurement as a method of assessment for Silicon Carbide (SiC) CMC material. We have also used this method to characterise individual bundles of SiC fibres, to develop an understanding of the method. Environmental conditions are then applied to the CMC samples including a high temperature exposure at 800 °C, and humidity exposures followed by two different 800 °C reheat durations. Characterisation was performed on the pre- and post-exposed material to verify the severity of each exposure, both microstructurally and mechanically, to compare these with microwave dielectric property data.</div></div>","PeriodicalId":34140,"journal":{"name":"Open Ceramics","volume":"23 ","pages":"Article 100818"},"PeriodicalIF":2.9,"publicationDate":"2025-06-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144523993","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Innovative fabrication pathways for ultra-high temperature ceramic matrix composites: Progress, properties enhancements and future perspectives 超高温陶瓷基复合材料的创新制造途径:进展、性能增强和未来展望
IF 2.9
Open Ceramics Pub Date : 2025-06-24 DOI: 10.1016/j.oceram.2025.100817
Shah Mohammad Azam Rishad, Md. Ashraful Islam, Dipayan Mondal
{"title":"Innovative fabrication pathways for ultra-high temperature ceramic matrix composites: Progress, properties enhancements and future perspectives","authors":"Shah Mohammad Azam Rishad,&nbsp;Md. Ashraful Islam,&nbsp;Dipayan Mondal","doi":"10.1016/j.oceram.2025.100817","DOIUrl":"10.1016/j.oceram.2025.100817","url":null,"abstract":"<div><div>Ultra-High Temperature Ceramic Matrix Composites (UHTCMCs) stand at the frontier of materials science, offering unparalleled resilience in extreme environments, such as aerospace propulsion, hypersonic vehicles, and advanced nuclear systems. The thermal stability, oxidation resistance, and mechanical durability of UHTCMCs—composed of refractory carbides, borides, and nitrides—are superior to those of conventional ceramics and composites. Recent innovations in fabrication techniques have shown promising results in improving the density, mechanical integrity, oxidation resistance, and uniform microstructures of UHTCMCs. However, challenges like incomplete densification, porosity, and thermal shock limitations still impede their broader application. This review explores the progression of UHTCMC fabrication, focusing on both traditional and hybrid techniques and evaluating their respective advantages and shortcomings. This work also focuses on how little changes in these methods have resulted in complicated multi-phase microstructures, which show a huge improvement in customizing the outstanding performance of UHTCMCs in harsh conditions. The discourse extends to identifying the suitable fabrication methods for meticulous applications and the ongoing efforts to overcome existing challenges in the world.</div></div>","PeriodicalId":34140,"journal":{"name":"Open Ceramics","volume":"23 ","pages":"Article 100817"},"PeriodicalIF":2.9,"publicationDate":"2025-06-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144513847","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Advances and obstacles to unify the concept of “printability” in Ceramics Direct Ink Writing 陶瓷直墨书写中“可印刷性”概念统一的进展与障碍
IF 2.9
Open Ceramics Pub Date : 2025-06-21 DOI: 10.1016/j.oceram.2025.100808
Mathilde Maillard , Sylvain Fournier , Esther García-Tuñón , Edwin-Joffrey Courtial
{"title":"Advances and obstacles to unify the concept of “printability” in Ceramics Direct Ink Writing","authors":"Mathilde Maillard ,&nbsp;Sylvain Fournier ,&nbsp;Esther García-Tuñón ,&nbsp;Edwin-Joffrey Courtial","doi":"10.1016/j.oceram.2025.100808","DOIUrl":"10.1016/j.oceram.2025.100808","url":null,"abstract":"<div><div>In Additive Manufacturing, “printability” describes the ability to shape a functional 3D object from a starting material. This concept is not easy to define because it depends on several factors including material considerations (microstructure and rheological properties), as well as process parameters that cannot be evaluated by a single metric. Some printability criteria have been proposed to classify and map the rheological properties of DIW inks. However, these criteria fail to capture all the relevant rheological aspects, and to consider DIW system technical specifications, processing parameters, and final part properties, while rheological characterisation methods remain inconsistent and lack standardisation. This review tackles this gap in the field by providing an overview of literature investigating the links between rheological properties and printability for ceramics DIW. Based on recent findings, we present an overview of specific rheological tests and parameters that correlate with printing behaviour to achieve high-quality outcomes in ceramic 3D printing.</div></div>","PeriodicalId":34140,"journal":{"name":"Open Ceramics","volume":"23 ","pages":"Article 100808"},"PeriodicalIF":2.9,"publicationDate":"2025-06-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144365147","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Laser assisted joining of SiC/SiC for nuclear applications 核用SiC/SiC激光辅助连接
IF 2.9
Open Ceramics Pub Date : 2025-06-16 DOI: 10.1016/j.oceram.2025.100802
Monica Ferraris , Manuela De Maddis , Dario Basile , Khurshid Aliev , Dario Alidoost , Alessandro Benelli , Stefano De La Pierre , Valentina Casalegno , Marion Herrmann , Shuigen Huang , Jef Vleugels , Christophe Lorrette , Cédric Sauder , Konstantina Lambrinou
{"title":"Laser assisted joining of SiC/SiC for nuclear applications","authors":"Monica Ferraris ,&nbsp;Manuela De Maddis ,&nbsp;Dario Basile ,&nbsp;Khurshid Aliev ,&nbsp;Dario Alidoost ,&nbsp;Alessandro Benelli ,&nbsp;Stefano De La Pierre ,&nbsp;Valentina Casalegno ,&nbsp;Marion Herrmann ,&nbsp;Shuigen Huang ,&nbsp;Jef Vleugels ,&nbsp;Christophe Lorrette ,&nbsp;Cédric Sauder ,&nbsp;Konstantina Lambrinou","doi":"10.1016/j.oceram.2025.100802","DOIUrl":"10.1016/j.oceram.2025.100802","url":null,"abstract":"<div><div>Silicon carbide (SiC) is a high-performance ceramic renowned for its excellent strength, thermal stability, and corrosion resistance, making it highly critical for advanced applications. Yet, achieving reliable joints remains challenging, especially given the need for localized heating rather than bulk heating of an entire SiC component. Laser-assisted joining has emerged as a promising alternative, offering the advantages of localized heating, rapid processing without the need for pressure, and precise energy control that significantly minimizes impact on adjacent materials. This study examines the feasibility of using two different infrared diode lasers for pressure-less, localized joining of SiC/SiC tubes to SiC/SiC end-plugs. The results are compared with those obtained using conventional furnaces. A silica-alumina-yttria-based glass is utilized as the joining material. The morphology, microstructure, and mechanical strength of the joints are analyzed, with strength evaluated through push tests designed to detach the end-plug from the tube.</div></div>","PeriodicalId":34140,"journal":{"name":"Open Ceramics","volume":"23 ","pages":"Article 100802"},"PeriodicalIF":2.9,"publicationDate":"2025-06-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144313098","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Influence of calcium nitrate timing on the structural and textural characteristics of mesoporous SiO2-CaO nanoparticles 硝酸钙时间对介孔SiO2-CaO纳米颗粒结构和结构特性的影响
IF 2.9
Open Ceramics Pub Date : 2025-06-12 DOI: 10.1016/j.oceram.2025.100807
Onat Başak , Fatih Kurtuldu , Jan Ilavský , Martina Vitázková , Ana M. Beltrán , Francisco Muñoz , Yolanda Castro , Martin Michálek , Maria Chromčíková
{"title":"Influence of calcium nitrate timing on the structural and textural characteristics of mesoporous SiO2-CaO nanoparticles","authors":"Onat Başak ,&nbsp;Fatih Kurtuldu ,&nbsp;Jan Ilavský ,&nbsp;Martina Vitázková ,&nbsp;Ana M. Beltrán ,&nbsp;Francisco Muñoz ,&nbsp;Yolanda Castro ,&nbsp;Martin Michálek ,&nbsp;Maria Chromčíková","doi":"10.1016/j.oceram.2025.100807","DOIUrl":"10.1016/j.oceram.2025.100807","url":null,"abstract":"<div><div>Mesoporous bioactive glass nanoparticles (MBGNPs) are promising materials for drug delivery due to their high pore volume and specific surface area. This study investigates how the timing of calcium nitrate addition affects the structural and textural characteristics of MBGNPs synthesized via a microemulsion-assisted sol-gel method. Delayed calcium nitrate addition reduced CaO incorporation from 14.2 to 9.5 mol% and increased particle size from 178 ± 51 nm to 256 ± 30 nm. The specific surface area values increased with the delayed addition of calcium nitrate, as observed through BET and USAXS/SAXS measurements. The proportion of Q<sub>Si</sub><sup>n</sup> units slightly changed, but no cytotoxicity was observed in osteoblast-like cells. These findings provide valuable insights into optimizing MBGNP synthesis for biomedical applications.</div></div>","PeriodicalId":34140,"journal":{"name":"Open Ceramics","volume":"23 ","pages":"Article 100807"},"PeriodicalIF":2.9,"publicationDate":"2025-06-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144270488","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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