Food Control最新文献

{"title":"Removal of aerosols from the air by seaweed cellulose nanofibers: To improve the authenticity of loop-mediated isothermal amplification for detection of pork adulteration","authors":"Duoduo Zhang,&nbsp;Mohamed Aamer Abubaker,&nbsp;Yang Jiao,&nbsp;Yongfeng Liu","doi":"10.1016/j.foodcont.2025.111205","DOIUrl":"10.1016/j.foodcont.2025.111205","url":null,"abstract":"<div><div>Meat adulteration has attracted more and more attention from consumers. Loop-mediated isothermal amplification (LAMP) is a method that can be used to detect meat adulteration on the spot, quickly and without any instruments. Therefore, in this study, seaweed cellulose and β-CD were used as raw material to prepare aerogel materials capable of adsorbing aerosols, which were used in LAMP and qLAMP detection. LAMP and qLAMP detection were performed with pork-specific primers, the results showed that this material could effectively avoid the problem of false positives. Amplification occurred only with the pork DNA template, and the other four kinds of meat were not amplified. The LAMP and qLAMP assays were performed with different concentrations of the pork DNA template (100 ng/μL-1 fg/μL) to determine its sensitivity, and the results showed that 1 fg/μL of pork could be detected. By testing the experimental adulteration model prepared by mixing different proportions of pork (0.1%–20%) with beef and goat meat, the detection limit of the two methods was determined to be 0.1% pork. The aerogel material prepared in this study effectively prevent the contamination of aerosol in LAMP and qLAMP, ensuring the result accuracy. Based on this material, the detection sensitivity of LAMP and qLAMP is high, with a low detection limit, which has significant application potential in the field of meat adulteration detection.</div></div>","PeriodicalId":319,"journal":{"name":"Food Control","volume":"172 ","pages":"Article 111205"},"PeriodicalIF":5.6,"publicationDate":"2025-02-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143388125","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Application of multivariate analysis and Kohonen Neural Network to discriminate bioactive components and chemical composition of kosovan honey","authors":"Hyrije Koraqi ,&nbsp;Jolanta Wawrzyniak ,&nbsp;Alev Yüksel Aydar ,&nbsp;Ravi Pandiselvam ,&nbsp;Waseem Khalide ,&nbsp;Anka Trajkoska Petkoska ,&nbsp;Ioannis Konstantinos Karabagias ,&nbsp;Seema Ramniwas ,&nbsp;Sarvesh Rustagi","doi":"10.1016/j.foodcont.2024.111072","DOIUrl":"10.1016/j.foodcont.2024.111072","url":null,"abstract":"<div><div>The diversity of botanical origins may influence the composition of honey and thus its recognition as a functional and healthy food. This study examined the standard physicochemical properties, bioactive components and antioxidant activity of Kosovan honeys according to their floral source (monofloral, blossom, acacia, and mountain blossom honey). Then the Kohonen Neural Network (KNN), which transforms complex multivariate data into two-dimensional space, and Principal Component Analysis (PCA) were used to identify and group botanical origin of honey samples based on their component features. Physicochemical characteristics, total phenolic content, and antioxidant activity varied significantly between the individual distinct varieties of honeys. Statistical analysis showed the usefulness of KNN and PCA for dimensionality reduction and detecting the structure and general regularities in the values of variables describing the tested honeys of the same botanical origin. KNNs have proven to be a particularly effective data mining tool, enabling the detection of subtle differences and clearer separation of clusters occurring in honey samples. The developed KNN model revealed proximity between the AC and MBL clusters, as well as between the MF and BL clusters, indicating similarity of their features. The arrangement of honey groups on the matrix map also suggested that the properties of AC and MBL honeys were significantly different from those of MF and BL honeys. The research showed that both methods used could be used as additional statistical tools supporting the recognition of the type of honey according to its chemical composition, mineral content, bioactive components and the antioxidant activity of honey as a functional food.</div></div>","PeriodicalId":319,"journal":{"name":"Food Control","volume":"172 ","pages":"Article 111072"},"PeriodicalIF":5.6,"publicationDate":"2025-02-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143350769","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Target-mediated rolling circle amplification/transcription coupling with double signal amplification of exonuclease III-assisth most of them are low-ed CRISPR/Cas12a-Cas13a for simultaneously ultrasensitive detection of aflatoxin B1 and ochratoxin A","authors":"Yaqi Li ,&nbsp;Qingyue Sun ,&nbsp;Xin Chen ,&nbsp;Yian Jian ,&nbsp;Siye Wei ,&nbsp;Xiang Zuo ,&nbsp;Chang Liu ,&nbsp;Dezhao Kong ,&nbsp;Feng Lin","doi":"10.1016/j.foodcont.2025.111200","DOIUrl":"10.1016/j.foodcont.2025.111200","url":null,"abstract":"<div><div>Aflatoxin B₁ (AFB₁) and ochratoxin A (OTA) are among the more toxic natural carcinogens that threaten human and animal health. Herein, we reported a target-mediated rolling circle amplification/transcription fluorescent aptasensor for the simultaneous ultrasensitive detection of AFB₁ and OTA by hydrothermal synthesis of double emitting CQDs (CQDs) based on dual signal amplification of Exonuclease III (Exo Ⅲ) and CRISPR-Cas12a/Cas13a. CQDs was combined with probes for the signal marker. In the presence of AFB₁, the aptamer (Apt¹) specifically bonded to the target resulting in cDNA¹ detachment, Apt¹ was digested by the addition of Exo Ⅲ and AFB₁ was released to interact with Apt¹-cDNA¹ again, releasing more cDNA¹ to activate the trans-cleavage activity of the Cas12a protein and to digest the fluorescent probe (Probe¹) from cobalt hydroxide nanosheet (CoOOH) surface detachment, leading to fluorescence recovery to achieve AFB₁ detection. The system of crRNA²/cDNA²/Probe²/Cas13a was used for OTA detection with the similar principles and processes. This strategy utilized both enzymatic activities of Exo III without interfering with each other. In addition, the simultaneous cutting of DNA probe and RNA probe was realized by utilizing the difference in the cutting targets of Cas12a and Cas13a proteins. The double sensitization signal amplification could further reduce the detection limit to achieve the ultrasensitive detection. The linear range for AFB₁ determination was 0.01–50 ng mL⁻¹ with a detection limit of 3.1 pg mL⁻¹. The OTA was 0.01–50 ng mL⁻¹ with a detection limit of 3.5 pg mL⁻¹. Finally, this developed method was employed to detect three kinds of real grain flour samples to demonstrate the reliability.</div></div>","PeriodicalId":319,"journal":{"name":"Food Control","volume":"172 ","pages":"Article 111200"},"PeriodicalIF":5.6,"publicationDate":"2025-02-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143394095","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Multiphysics analysis for ultrasound settings that can disinfect food: Inactivation of E. coli in apples","authors":"Daniel Aguilar-Torres ,&nbsp;Omar Jiménez-Ramírez ,&nbsp;Regina Hernández-Gama ,&nbsp;Felipe A. Perdomo-Hurtado ,&nbsp;Rubén Vázquez-Medina","doi":"10.1016/j.foodcont.2025.111191","DOIUrl":"10.1016/j.foodcont.2025.111191","url":null,"abstract":"<div><div>Ultrasonic technology has shown great promise in enhancing food safety and quality through disinfection. This study provides a rigorous multiphysics analysis to identify the ultrasonic pressure and frequency for efficient disinfection of apples, with a specific focus on eliminating <em>E. coli</em>. In this study the Finite Element Method (FEM) was used to solve the wave and heat equations describing the spectral and spatio-temporal behavior of the ultrasonic signals in the proposed disinfection setup, as well as a thermoacoustic analysis of the system. The food disinfection system included a chamber of 20 cm <span><math><mo>×</mo></math></span> 9 cm, two piezoelectric transducers, and a whole apple with an average radius of 7 cm. The spectral analysis was performed from 20 kHz to 100 kHz in order to identify the influential frequencies in the disinfection chamber and in the apple. This analysis revealed that there are spatial patterns of ultrasonic signal intensity in the system that depend on the selected operating frequency. This feature makes it possible to distinguish the greatest ultrasonic influence in the disinfection chamber and in the apple. Spatio-temporal analysis was performed to evaluate the thermal effects generated by the ultrasonic signals in the disinfection chamber and in the apple. Then, the ultrasonic irradiation pressure and time for inactivating <em>E. coli</em> in the apple were determined from the thermoacoustic behavior of the system. Finally, microbial analysis and parameter optimization were performed to determine the inactivation rate of <em>E. coli</em> in the disinfection system analyzed in this work.</div></div>","PeriodicalId":319,"journal":{"name":"Food Control","volume":"172 ","pages":"Article 111191"},"PeriodicalIF":5.6,"publicationDate":"2025-02-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143394855","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Decontamination of deoxynivalenol in Indica rice by cold plasma and the determination of major degradation products","authors":"Shijia Huang ,&nbsp;Ling Li ,&nbsp;Guoxin Zhou ,&nbsp;Xingquan Liu ,&nbsp;Jian Guo","doi":"10.1016/j.foodcont.2025.111180","DOIUrl":"10.1016/j.foodcont.2025.111180","url":null,"abstract":"<div><div>Previous studies offer limited research on the degradation pathway and byproducts of deoxynivalenol (DON) in rice through Cold Plasma (CP) treatment, particularly in the identification of products with smaller molecular weights. This study applies CP to treat DON-contaminated <em>Indica</em> rice, examining its efficacy in degrading DON, the resulting byproducts, and its impact on the rice's primary nutritional components and moisture content. The findings reveal a degradation rate of 62.4%, with minimal nutritional impact and a decreased moisture content. Using Ultra Performance Liquid Chromatography-Time of Flight-Mass Spectrometry (UPLC-TOF-MS), we identified 5 potential degradation pathways for the toxin, along with the chemical structures of the degradation products. These results enhance our understanding of the DON degradation mechanism via cold plasma and serve as a reference for studying the degradation mechanisms of structurally similar compounds.</div></div>","PeriodicalId":319,"journal":{"name":"Food Control","volume":"173 ","pages":"Article 111180"},"PeriodicalIF":5.6,"publicationDate":"2025-02-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143419399","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Comprehensive assessment of bamboo and other bio-based dishes contamination","authors":"Kamila Bechynska ,&nbsp;Vit Kosek ,&nbsp;Leos Uttl ,&nbsp;Vojtech Hrbek ,&nbsp;Claire McKillen ,&nbsp;Emma Bradley ,&nbsp;Monika Tomaniova ,&nbsp;Jana Hajslova","doi":"10.1016/j.foodcont.2025.111188","DOIUrl":"10.1016/j.foodcont.2025.111188","url":null,"abstract":"<div><div>In line with the shifts towards sustainable food production, bio-based food contact materials are becoming more favored than conventional ones. In this study, we collected 33 bamboo and other bio-based dishes from the British, Chinese and Czech markets with the aim to investigate a potential presence of hazardous compounds that may migrate into food. Non-targeted screening by ultra-high-performance liquid chromatography coupled to high-resolution tandem mass spectrometry (UHPLC-HRMS/MS) was employed for analysis of acidified aqueous (3%, w/w, acetic acid), ethanolic and isooctane extracts prepared from disintegrated dishes. Besides melamine detected in 32% of tested samples (mainly bamboo-based), also some pesticide residues and a number of plant secondary metabolites were found. Migration tests performed according to the EURL guideline showed six non-compliant bamboo products exceeding melamine limits set by Commission Regulation (EU) No October 2011. Melamine was also found to migrate in low concentrations into hot lemon tea and orange juice. Targeted screening of 443 pesticides showed the highest number of residues in cereal-based dishes, when only disinfectants were found in bamboo-based dishes.</div></div>","PeriodicalId":319,"journal":{"name":"Food Control","volume":"174 ","pages":"Article 111188"},"PeriodicalIF":5.6,"publicationDate":"2025-02-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143445695","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Controlling Listeria monocytogenes contamination in fresh goat milk cheeses: Dynamic modelling during storage","authors":"Olga María Bonilla-Luque ,&nbsp;Arícia Possas ,&nbsp;Úrsula Gonzales-Barron ,&nbsp;Vasco Cadavez ,&nbsp;Youssef Ezzaky ,&nbsp;Abdelraheem Hussein ,&nbsp;Antonio Valero","doi":"10.1016/j.foodcont.2025.111194","DOIUrl":"10.1016/j.foodcont.2025.111194","url":null,"abstract":"<div><div>Predictive models applied for artisanal fresh goat cheeses are invaluable tools for rapid decision-making in quality and safety management. <em>Listeria monocytogenes</em> is a common foodborne pathogen associated with recent safety alerts in ready-to-eat (RTE) products in Andalucia. Managing artisanal production variables, such as storage conditions and final product features (pH or water activity [a_w]) might be crucial for controlling <em>L. monocytogenes</em> in these traditional products. This study evaluated the time-temperature dependence of <em>L. monocytogenes</em> during shelf-life of fresh goat milk cheese artisanally produced in Andalucía. The effect of storage temperature (4–25 °C) over 5–20 days was tested in lab-scale fresh goat milk cheeses initially inoculated with a three-strain cocktail of the pathogen (ca. 2–3 log cfu/g). The Huang (model A) and Baranyi (model B) models coupled with Ratkowsky were fitted to the collected growth data to describe the relationship between <em>L. monocytogenes</em> concentration, growth rate (<em>μ</em>_max, log cfu/d), storage temperature, and time. The results highlighted the higher variability of growth data at 4 °C, the linear relationship between <em>μ</em>_<em>max</em> and temperature, the inverse correlation between y_<em>max</em> (exceeding 5 log cfu/g at all the temperatures) and <em>ΔY</em> (with a maximum of 4.386 and minimum of 2.461, at 4 and 25 °C, respectively) and a faster decrease of pH at higher temperatures. Model validity, assessed through goodness-of-fit and both internal and external validations (under both isothermal temperatures and a dynamic temperature workflow simulating real production scenario), revealed good model adjustment to <em>L. monocytogenes</em> growth in artisanal commercial cheeses, after determining a correction factor of 1.806 and 1.856, for models A and B, respectively. Predictions indicated that an initially contaminated artisanal fresh goat milk cheese would not meet regulatory limits after 4 days under refrigeration conditions (4 °C), aerobic conditions, or opened packaging. These results highlight the potential public health risk of artisanal fresh goat milk cheeses related to <em>L. monocytogenes</em> transmission if manufacturing and storage conditions are not well controlled, emphasizing the need for stringent microbial control efforts and mitigation measures.</div></div>","PeriodicalId":319,"journal":{"name":"Food Control","volume":"174 ","pages":"Article 111194"},"PeriodicalIF":5.6,"publicationDate":"2025-02-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143464242","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Climate change and campylobacteriosis from chicken meat: The changing risk factors and their importance","authors":"Kevin Queenan,&nbsp;Barbara Häsler","doi":"10.1016/j.foodcont.2025.111193","DOIUrl":"10.1016/j.foodcont.2025.111193","url":null,"abstract":"<div><div>Globally, chicken meat is currently the highest consumed meat per capita, and it continues to rise. Campylobacteriosis is one of the most reported gastrointestinal conditions, typically associated with chicken meat consumption. Cases are seasonal with summer and early autumn peaks. Similar seasonal peaks in <em>Campylobacter</em> prevalence in broilers and in retailed chicken meat have also been shown. Climate change impacts include increased ambient temperatures, rainfall, and humidity, and more frequent extreme weather events. These are likely to impact the risks associated with warmer-season foodborne diseases like campylobacteriosis. A literature review was conducted to identify the chicken related <em>Campylobacter</em> risk factors from farm to fork. Expert opinion was gathered using a modified Delphi survey in two rounds: 1) to identify risk factors whose likelihood of occurring would be impacted by climate change, 2) to determine the likelihood of the proposed change and the impact on campylobacteriosis from chicken meat consumption. Likert scores were used to calculate a mean risk level value. The latter was used together with a respondent agreement cut-off of over 66% to highlight risk factors most likely to change and to impact the risk of campylobacteriosis from chicken meat under climate change. Increasing temperatures and humidity and the extension of summer and early autumn seasons had the overall highest Mean Risk Level value (19/25). The increased prevalence of pests, especially flies had the second highest (16/25), and the highest respondent agreement level (94%). Several water-related risk factors were found likely to increase, including water drinker contamination, use of non-mains water sources, and those associated with water-based broiler house hygiene. Heat stress related risks were also highlighted, including the increased likelihood of on-farm <em>Campylobacter</em> positive animals and recent in-flock mortalities, a high degree of caecal colonisation, and faecal shedding of <em>Campylobacter,</em> and contaminating drinkers and carcase washing water. Other risk factors affected included higher consumption volumes and frequency of chicken meals, and broiler farmers having under 10 years of experience. These findings provide insights on how climate change may affect risk factor occurrence in the future and highlights those risks that decisionmakers should consider more closely in the future.</div></div>","PeriodicalId":319,"journal":{"name":"Food Control","volume":"173 ","pages":"Article 111193"},"PeriodicalIF":5.6,"publicationDate":"2025-02-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143419336","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"A preliminary survey on the presence of ciguatoxins (CTXs) in fishery products sold in Italy: An initial step towards the proper assessment of an emerging EU risk","authors":"Marta Di Maggio ,&nbsp;Christopher R. Loeffler ,&nbsp;Lara Tinacci ,&nbsp;Elena Varinelli ,&nbsp;Sonia Dall’Ara ,&nbsp;Synne T. Frøstrup ,&nbsp;Astrid Spielmeyer ,&nbsp;Alice Giusti ,&nbsp;Andrea Armani","doi":"10.1016/j.foodcont.2025.111202","DOIUrl":"10.1016/j.foodcont.2025.111202","url":null,"abstract":"<div><div>Ciguatera poisoning is a food-borne disease related to the consumption of finfish from areas endemic for ciguatoxins (CTXs). Mislabeling of fishery products can enhance consumer's exposure to this hazard by hiding the presence of CTXs vector species. In this study, we identified the main CTXs vector fish families (CVF) and the FAO areas at CTXs risk. Market products from CVF and sourced from CTXs risk areas were collected in Italy, molecularly authenticated to detect potential mislabeling cases, and then analysed for CTXs using a two-tier detection method (cell-based assay and mass spectrometry). Additionally, the official lists of seafood trade names (OL) from EU countries associated with ciguatera poisoning (CP) outbreaks linked to imported products were evaluated to assess a possible correlation between market species and CP risk. The Italian OL was also included. A total of 24 CVF and four FAO areas were selected. Overall, 51 market products were collected. The availability of CVF products from FAO areas at CTXs risk was limited in the Italian market. Molecular authentication revealed 16 cases of mislabeling (31.4%) in products from Sparidae, Lethrinidae and Epinephelidae. All samples analysed tested negative for CTXs. The OL analysis highlighted that a revision to improve correspondence between trade names and species would be beneficial also in the light of a proper risk assessment. Although no CP outbreaks have been reported in Italy by far, and no CTXs were detected in this study, the implementation of targeted programs to prevent and manage CP risk should be considered. This is particularly important because i) mislabeling remains prevalent in products imported to Italy, and ii) future indigenous outbreaks due to climate changes should be anticipated.</div></div>","PeriodicalId":319,"journal":{"name":"Food Control","volume":"172 ","pages":"Article 111202"},"PeriodicalIF":5.6,"publicationDate":"2025-02-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143388023","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}

{"title":"Establishment and verification of GC-MS/MS method for four fluoroquinolones residues determination based on precolumn derivatization: Application to poultry eggs","authors":"Hao Ding ,&nbsp;Junjie Xu ,&nbsp;Shuyu Liu ,&nbsp;Pengfei Gao ,&nbsp;Yawen Guo ,&nbsp;Yang Cao ,&nbsp;Yiwei Hong ,&nbsp;Xing Xie ,&nbsp;Tao Zhang ,&nbsp;Genxi Zhang ,&nbsp;Xiaodong Guo ,&nbsp;Guojun Dai ,&nbsp;Maoda Pang ,&nbsp;Kaizhou Xie","doi":"10.1016/j.foodcont.2025.111203","DOIUrl":"10.1016/j.foodcont.2025.111203","url":null,"abstract":"<div><div>In this study, liquid‒liquid extraction and solid‒phase extraction were coupled with derivatization to detect 4 types of fluoroquinolones residues in poultry eggs (chicken, duck, goose, and quail eggs) via GC-MS/MS. A 10% trichloroacetic acid‒acetonitrile solution and trimethylsilyl diazomethane (TMSD) were chosen as the extraction and derivatization reagents, respectively. The results revealed that the detection and quantitative limits (LODs, LOQs) were 1.0, 0.2, 0.5, and 1.0 μg/kg and 2.0, 0.4, 1.0, and 2.0 μg/kg, respectively. The peak areas of all the target compounds had a good linear relationship with the corresponding concentrations of the matrix matched standard working solution, with R² values higher than 0.9991. The recoveries of the target compounds were all higher than 78.0%. The RSDs ranged from 2.1% to 8.0%. All the matrices had weak matrix effect. This established method satisfied the requirements of the NY/T 1896–2010 industry standard for veterinary drug residue detection in China, providing a scientific basis for fluoroquinolone residue detection. Furthermore, this method expands the monitoring range, improves the detection efficiency, reduces the cost, and meets the detection needs of different laboratories.</div></div>","PeriodicalId":319,"journal":{"name":"Food Control","volume":"172 ","pages":"Article 111203"},"PeriodicalIF":5.6,"publicationDate":"2025-02-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143394099","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}