{"title":"The effect of shielding gas on weldability of the AISI 420 martensitic stainless steel","authors":"İ. Acar, B. Çevik, B. Gülenç","doi":"10.1515/pm-2021-1000","DOIUrl":"https://doi.org/10.1515/pm-2021-1000","url":null,"abstract":"Abstract Most of weld defects occurring in the welding of martensitic stainless steels are caused by the presence of hydrogen. Thus, the effects of hydrogen in the weld zone need to be well-understood to estimate the quality and service life of martensitic stainless steel joints. In the present study, AISI 420 martensitic stainless steel materials were welded by using different combinations of shielding gas via the gas metal arc welding (GMAW) method. It is known that shielding gases also play a critical role in heat input, cooling rate, microstructure of weld seam, weld defects, and mechanical properties besides drying of molten weld pool. Thus, it is important to investigate the effects of shielding gases and gas combinations on the welding of martensitic stainless steels in the welding process. In the present study, 100 % Ar, 97 % Ar + 3 % H2 and 93 % Ar + 7 % H2 gas combinations were employed. The welded sheets were subjected to the metallographic examination as well as hardness, tensile, and bending tests. The effect of the tests and the combination of shielding gas on the mechanical and microstructural properties of AISI 420 stainless steel was investigated. The results indicated that a noticeable grain coarsening occurred in the microstructure of the weld metal and heat affected zones (HAZs) after the addition of H2 into the Ar gas during the welding process. The highest tensile strength was obtained from the joints with 100 % Ar gas. As a result of the tensile test, rupture occurred in the base metal-HAZ transition zone in all the welded samples. In the joints welded with 97 % Ar + 3 % H2 and 93 % Ar + 7 % H2 gas combinations, fracture occurred in the base metal-HAZ transition zone during the bending test.","PeriodicalId":20360,"journal":{"name":"Practical Metallography","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-01-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"79562448","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
L. Schmies, B. Botsch, Q. Le, A. Yarysh, U. Sonntag, M. Hemmleb, D. Bettge
{"title":"Classification of fracture characteristics and fracture mechanisms using deep learning and topography data","authors":"L. Schmies, B. Botsch, Q. Le, A. Yarysh, U. Sonntag, M. Hemmleb, D. Bettge","doi":"10.1515/pm-2022-1008","DOIUrl":"https://doi.org/10.1515/pm-2022-1008","url":null,"abstract":"Abstract In failure analysis, micro-fractographic analysis of fracture surfaces is usually performed based on practical knowledge which is gained from available studies, own comparative tests, from the literature, as well as online databases. Based on comparisons with already existing images, fracture mechanisms are determined qualitatively. These images are mostly two-dimensional and obtained by light optical and scanning electron imaging techniques. So far, quantitative assessments have been limited to macroscopically determined percentages of fracture types or to the manual measurement of fatigue striations, for example. Recently, more and more approaches relying on computer algorithms have been taken, with algorithms capable of finding and classifying differently structured fracture characteristics. For the Industrial Collective Research (Industrielle Gemeinschaftsforschung, IGF) project “iFrakto” presented in this paper, electron-optical images are obtained, from which topographic information is calculated. This topographic information is analyzed together with the conventional 2D images. Analytical algorithms and deep learning are used to analyze and evaluate fracture characteristics and are linked to information from a fractography database. The most important aim is to provide software aiding in the application of fractography for failure analysis. This paper will present some first results of the project.","PeriodicalId":20360,"journal":{"name":"Practical Metallography","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-01-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"87851987","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Combination of Digital Image Correlation (DIC) and in situ 3D-μ-CT in the analysis of the relationship between strains and porosity under creep loading","authors":"B. Camin, J. Hornig-Klamroth, N. zu Bentheim","doi":"10.1515/pm-2023-0008","DOIUrl":"https://doi.org/10.1515/pm-2023-0008","url":null,"abstract":"Abstract In situ 3D μ-XCT allows the time and space resolved measurement and analysis of material damage in the component volume, whereas the Digital Image Correlation (DIC) is a 2D method for the analysis of deformation measured on the surfaces of components. In situ 3D μ-XCT measurements were performed on cylindrical specimen made of SiC particle reinforced titanium MMC (MMC: Metal Matrix Composite) (15 % SiC particles) during creep load. The formation and evolution of voids were subsequently analyzed. Due to the rotationally symmetric sample geometry, the analysis of the deformation in the interior of the material by DIC using 2D slices is possible and evident. The dot pattern required to calculate the strain using DIC (speckle pattern) is provided by the intrinsic particle reinforcement of the MMCs. Temporally and locally changing and time-variant strain fields in both the tensile as well as the compressive range could be detected correlating with void formation and development area.","PeriodicalId":20360,"journal":{"name":"Practical Metallography","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-01-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"88717857","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Imperfections in Inner Cavity of Row 4 Turbine Blade Caused by Metal-Core Reaction","authors":"A. Neidel, E. Cagliyan, B. Fischer","doi":"10.1515/pm-2023-0009","DOIUrl":"https://doi.org/10.1515/pm-2023-0009","url":null,"abstract":"Abstract When selecting case studies for presentation in this section Failure Analysis of Practical Metallography, the authors of this contribution asked themselves time and again what conditions actually constitute a component failure. Conventional wisdom has it that a failure occurred when a component or assembly lost its function intended by design. The authors readily admit that this is decidedly not the case for the “failure” presented in this contribution. Not only did no failure occur (the component was successfully used in engine service for the intended operating time), but the subject turbine blade did not loose its intended function by any stretch of the imagination. Why is this case study then presented here anyway? Because the evaluation and assessment of severity of indications found upon non-de structive testing of the subject turbine blade was only possible after destructive metallurgical investigation. One could jokingly concede that the blade definitely lost its function after metallographic cut-up. In any case, in the “failure case” presented in this contribution, the engineering department did not dare to release the subject turbine component for renewed engine service after refurbishment, since indications were detected that could not be properly assessed, without destroying the part; hence the subject component was not fit for engine service. The inclined reader may himself decide whether this fact makes it a component failure.","PeriodicalId":20360,"journal":{"name":"Practical Metallography","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-01-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"84618885","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
D. Hohs, S. Klett, R. Löffler, F. Trier, D. Goll, G. Schneider
{"title":"Visualization of magnetization reversal processes by dynamic Kerr microscopy","authors":"D. Hohs, S. Klett, R. Löffler, F. Trier, D. Goll, G. Schneider","doi":"10.1515/pm-2023-0002","DOIUrl":"https://doi.org/10.1515/pm-2023-0002","url":null,"abstract":"Abstract Dynamic Kerr microscopy enables the analysis of structural defects in magnetic materials and their impact on the demagnetization behavior. Using new visualization techniques, it is possible to image the demagnetization process in the microstructure. It has been found that residual stresses and inclusions in soft magnets, for example, will impede magnetization. In permanent magnets, abnormally large grains, for example, will demagnetize first and then cause an accelerated demagnetization of adjacent grains.","PeriodicalId":20360,"journal":{"name":"Practical Metallography","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2022-12-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83155727","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
M. Laub, Björn Bachmann, E. Detemple, F. Scherff, T. Staudt, M. Müller, D. Britz, F. Mücklich, C. Motz
{"title":"Determination of grain size distribution of prior austenite grains through a combination of a modified contrasting method and machine learning","authors":"M. Laub, Björn Bachmann, E. Detemple, F. Scherff, T. Staudt, M. Müller, D. Britz, F. Mücklich, C. Motz","doi":"10.1515/pm-2022-1025","DOIUrl":"https://doi.org/10.1515/pm-2022-1025","url":null,"abstract":"Abstract The prior austenite grain size (PAGS) represents one of the most significant microstructural parameters for steel research and process development. Since the PAGS directly correlates with recrystallisation during rolling in the manufacturing process of steel plates, it has a huge influence on its mechanical properties. Methods to determine the PAGS reliably and reproducibly are in high demand. There are several different approaches, based on different working principles, aiming to measure the PAGS. In this paper, the focus will be held on chemical etching methods because they allow, other than indirect techniques, space-resolved images as output, coupled with a fast application with good statistics and do not necessarily require a pretreatment of the specimen that can alter properties of interest. A parameter study has been conducted to identify unknown influencing variables as well as to tune well known parameters for their application to low-carbon steels. In the scope of this work, a novel and objective way of determining the PAGS is being presented. A reproducible approach has been developed that is able to automatically reconstruct the prior austenite grain boundaries (PAGB) from low-carbon steels and thereby determining the PAGS. Based on an improved etching recipe, a routine could be elaborated using modern methods of machine learning in the field of computer vision that is able to quantitatively analyze optical micrographs. Semantic segmentation is used to detect the PAGB based on correlative EBSD data and expert’s annotations; thus, reconstructing the prior morphological microstructure. Therefore, besides the determination of the average grain size, the distribution of the PAGS and their morphological parameters can be quantified.","PeriodicalId":20360,"journal":{"name":"Practical Metallography","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2022-12-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"87649704","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Ferrite in the HAZ of Dissimilar Temperature Probe Welds","authors":"A. Neidel, M. Giller, S. Riesenbeck","doi":"10.1515/pm-2023-0003","DOIUrl":"https://doi.org/10.1515/pm-2023-0003","url":null,"abstract":"Abstract Protector tubes for temperature sensors were welded onto experimental gas turbine compressor blades. While the blades were made of a high alloy hard-martensitic stainless chromium steel, a high alloy metastable austenitic stainless steel was used for the tiny protector tubes. The dissimilar weld joint was applied using manual GTAW. A large amount of blocky delta ferrite formed in the HAZ immediately adjacent to the fusion line, on the side of the martensitic steel. Delta ferrite in such dissimilar welds might detrimentally affect the mechanical properties of the weld joint. It was therefore recommended not to use the affected experimental blades in test engine service. Even though no failure occurred in this case, one was prevented by declaring the subject instrumented parts unfit for test engine service.","PeriodicalId":20360,"journal":{"name":"Practical Metallography","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2022-12-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"80499989","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Materialographic sample preparation of ancient copper materials","authors":"H. Cloeren","doi":"10.1515/pm-2022-0071","DOIUrl":"https://doi.org/10.1515/pm-2022-0071","url":null,"abstract":"Abstract The metallographic preparation of samples from classical antiquity requires the use of very gentle preparation techniques. On the one hand, this is necessary since the samples provided are often very small and on the other hand, because the remaining sample material can be inserted back into the original object. Both sample preparation and microstructural evaluation may offer insights into the manufacture of the objects, for example whether casting, heat treatment or reshaping had taken place. In addition, corrosion products on the sample surfaces can be characterized. The results of the metallographic preparation of three different ancient copper objects are presented: 1. A bronze vessel from Gordion. 2. Bronze roof tiles from Caligula’s Nemi ships. 3. Roman copper nails from Carnuntum.","PeriodicalId":20360,"journal":{"name":"Practical Metallography","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2022-11-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"86941552","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Metallography on a sickle fragment from the Drassburg/Burgenland hoard find","authors":"R. Haubner, S. Strobl","doi":"10.1515/pm-2022-1005","DOIUrl":"https://doi.org/10.1515/pm-2022-1005","url":null,"abstract":"Abstract The Drassburg Bronze Age hoard find (approx. 25 kg) also comprises some sickles and sickle fragments. One of these sickle fragments was provided for metallographic examinations. A XRF analysis revealed 94.5 wt.% Cu, 4.31 wt.% Sn, 0.61 wt.% Pb, and 0.12 wt.% S in the alloy. It can therefore be attributed to tin bronzes. The material has a uniform dendritic microstructure. Higher concentrations of Sn, S, and Pb were measured in the interdendritic areas. This suggests a precipitation of the phases Pb and Cu2S from the residual melt. Klemm II etching also revealed the dendritic areas which exhibited different orientations. Deformations were observed in thin edge areas of the sickle fragments. They were introduced in the course of mechanical postprocessing of the bronze or during its use. The surface of the sickle exhibits a patina with a layered structure and a thickness of up to 500 μm. The Sn contents measured in the outer layers are somewhat higher than in the inner layers.","PeriodicalId":20360,"journal":{"name":"Practical Metallography","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2022-11-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"87598362","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}